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Ultrasonic Measurement

of Multiphase Flow Erosion


N. R. Kesana
Department of Mechanical Engineering,
Patterns in a Standard Elbow
University of Tuisa, Solid particle erosion is a mechanical process in which material is removed from a sur-
Tuisa, OK 74104 face due to impacts of solid particles transported within a fluid. It is a common problem
e-mail: nrk301@utulsa.edu faced by the petroleum industry, as solid particles are also produced along with oil and
gas. The erosion not only causes economic losses resulting from repairs and decreased
S. A. Grubb production but also causes safety and environmental concerns. Therefore, the metal
ConocoPhillips - Technology, losses occurring in different multiphase flow regimes need to be studied and understood
600 North Dairy Ashford, in order to develop protective guidelines for oil and gas production equipment. In the
Houston, TX 77079-1175 current study, a novel noninvasive ultrasonic (UT) device has been developed and imple-
e-mail: scott.a.grubbiSconooophlilips.com mented to measure the metal loss at 16 different locations inside an elbow. Initially,
experiments were performed with a single-phase carrier fluid (gas-sand) moving in the
pipeline, and the erosion magnitudes are compared with computational fluid dynamics
B. S. McLaury (CFD) results and found to be in good agreement. Next, experiments were extended to
e-maii: brenton-mciaury@utulsa.edu the multiphase slug flow regime. Influence of particle diameter and liquid viscosity were
also studied. Two different particle sizes (150 and 300 ¡xm sand) were used for performing
S. A. Shirazi tests. The shapes of the sand are also different with the 300 um sand being sharper than
e-mail: siamack-shirazi@jtulsa.edu the 150 ßm sand. Three different liquid viscosities were used for the present study (1 cP,
10 cP, and 40 cP). While performing the UT experiments, simultaneous metal loss meas-
Department of Mechanicai Engineering, urements were also made using an intrusive electrical resistance (ER) probe in a section
University of Tuisa, of straight pipe. The probe in the straight pipe is an angle-head probe which protrudes
Tuisa, OK 74104 into the flow with the face placed in the center of the pipe. The UT erosion measurements
in a bend are also compared with experimental data obtained placing an intrusive flat
head ER probe flush in a bend, and the results were found to be in good agreement.
Finally, the noninvasive nano UT permanent placement temperature compensated ultra-
sonic wall thickness device developed for this work has the capability of measuring metal
loss at many locations and also identifying the maximum erosive location on the pipe
bend. [DOI: 10.1115/1.4023331]

Introduction tion such as elbows, tees, and sudden expansion and contraction
zones. Since erosion depends on multiple factors, developing a
In oil and gas production, sand creates many problems, ranging predictive tool for erosion is a challenging task.
from accumulation of the sand in perforation tunnels, damage to
The severity of erosion can be clearly emphasized by the pic-
pumps, well tubing, and fittings. Sand screens or gravel packs are
ture shown below. Figure 1 shows the location of a through wall
commonly installed in open hole well bores to avoid the passage
failure caused by erosion in a stainless steel elbow. This location
of sand along with the reservoir fluids. However, this sand control
of failure supports the statement already made that erosion
approach may fail due to plugging of the screens with smaller
particles causing an increase in the local fiuid velocity at other
portions of the screen causing damage. Sand in production fluids
repeatedly impacts pipe walls removing material gradually. The
mechanism of material loss depends on the type of pipe wall
material. For example, the erosion of ductile materials is caused
by localized metal deformation resulting in cutting action due to
severe particle impacts. Other types of failure mechanisms include
plowing, fatigue, and brittle fracture.
Prediction of solid particle erosion is difficult because erosion
depends on many factors. The important factors are flow pattern,
sand distribution, flow geometry, fiuid flow rates, and particle
properties such as size, shape, and hardness. The complexity of
erosion is increased in multiphase flow because different flow
patterns can occur under different operating conditions. The flow
pattern affects the sand particle impact characteristics and causes
different amounts of erosion. The geometries, which are more
susceptible to erosion, are the ones which change the flow direc-

Contributed by the Petroleum Division of ASME for publication in the JOURNAL


OF ENERGY RESOURCES TECHNOLOOY. Manuscript received June 19, 2012; final
manuscript received December 6, 2012; published online May 24, 2013. Assoc. Fig. 1 Stainless steel elbow failure as the result of erosion in
Editor; Christopher J. Wajnikonis. muitiphase fiow

Journal of Energy Resources Technology Copyright ©2013 by ASME SEPTEMBER 2013, Vol. 135 / 032905-1
failures commonly occur in locations where the flow direction body), slug body length, slug liquid holdup, and velocity of gas
changes. This failure was observed after conducting experiments bubbles entrained inside the liquid slug body.
in a laboratory for approximately 3 months. There is a vast amount of literature available on studies of
slug characteristics as they tend to be important in models, which
predict pressure drop. Several experimental techniques have
evolved in the recent past to study details of slug flow such as
Slug Flow—^Literature Survey its structure, length distribution, and void fraction. Some of
the instruments used by researchers are conductance probes,
The major focus is to conduct slug flow experiments with sand
nuclear-densitometers, fiber-optic sensors, wire mesh sensors,
and measure the erosion. So, a brief description of slug flow is
piezo-electric sensors, hot-film anemometers, and tomography
given in this section.
techniques. Slug length measurements suggest that the slug body
The study of intermittent flow has received considerable atten- length is not constant and it follows a log normal distribution
tion for the past 30 years due to its most complex flow structure. [3-8]. This suggests that the volume of liquid inside the slug body
In horizontal pipelines, two intermittent flow patterns are ofren is continuously changing and over a certain period of time there
seen: plug flow and slug flow. Plug flow is characterized by liquid will be stable, decaying and growing slugs passing by a particular
plugs without gas entrainment, moving between the stratiñed zone cross-section inside the pipe which would be sufficiently far from
of the gas bubble and the liquid fllm regions. Plug flow occurs at the inlet of the pipe. Also, several correlations have been devel-
lower gas rates. If the gas rate is increased while maintaining a oped for the calculation of the mean slug length based on pipe
constant liquid rate, a three-dimensional mixing zone is observed diameter and orientation of the pipe. Recently, Sarica et al. [9]
at the front of the plug. This three-dimensional mixing zone conducted a sensitivity analysis on the influence of slug length
results in entrainment of the gas bubbles inside the liquid plugs, correlations on frequently used mechanistic models in the litera-
creating aerated plugs. The aerated plugs are commonly referred ture which are used to predict the pressure drop in the slug flow
to as slugs. regime. They found that the influence of slug length correlations
Slug flow is characterized by slugs moving at a velocity approx- is relatively small in the calculations of pressure drop and liquid
imately equal to the mixture velocity (mixture velocity is deflned holdup.
as the sum of superñcial liquid and gas velocities) between the
stratiñed gas and liquid film region. In the stratifled zone, gas Slug liquid holdup and translational velocity measurements
moves on top and the liquid film flows beneath it. The gas bubble have also been conducted by many investigators. There are many
seen in the stratifled region is usually called the Taylor bubble. slug liquid holdup correlations available in the literature. Gomez
The combination of liquid slug body and the Taylor bubble region et al. [10] is a commonly used slug liquid holdup correlation as it
is called the slug unit. The various components of the slug flow is applicable to all inclination angles. Also, Zhang et al. [11]
are shown in Fig. 2 developed a unifled mechanistic model which predicts slug liquid
holdup by equating the kinetic energy possessed by the slug body
Pseudo slug flow is a type of intermittent flow pattern which is
to the surface free energy of the entrained spherical gas bubbles.
seldom described in literature. In this type of flow pattern there is
Pereyra et al. [12] gathered huge data sets on slug liquid holdup
entrainment of liquid droplets inside the Taylor bubble within the
from literature and compared the data with the published correla-
stratifled region, in addition to the entrainment of the gas bubbles
tions. They improved the slug liquid holdup correlations by tuning
in the liquid slug region.
them to the available data and finding new constant values for the
Many researchers have focused on the flow rates which result correlations.
in the transition from stratifled flow to slug flow. Two different
approaches were followed by researchers. The first approach is to Slug flow characteristics are important for understanding and
use classical linear stability analysis and the other is to examine predicting erosion. Despite the literature available on slug flow, it
the stability of the slugs travelling over the liquid layer. Duckler is currently an active research area due to its vast appearance in
and Hubbard [1] flrst proposed the concept of a stable slug. They many areas and enormous complexity.
said that a fast moving liquid slug picks up slow moving liquid
inside a liquid film and accelerates the liquid to the slug velocity.
It then sheds the liquid back into the liquid film region. For a Sand Distribution and Transport
steady state slug flow, the rate of liquid picked up by the slug front In addition to the multiphase flow characteristics, sand distribu-
is equal to the rate of the liquid shed at the slug back. Taitel and tion and transportation characteristics also directly influence the
Bamea [2] developed a comprehensive model for slug flow by erosion behavior and magnitudes. So, a general overview on the
applying the momentum balance on the liquid film region. The influence of the sand characteristics on erosion is explained
final output of this model is to determine the pressure drop across below.
the slug unit, where the slug unit is defined as the combination of Hill [13] examined the behavior of sand flowing in horizontal
slug body and the liquid fllm region. This model takes into consid- pipes and determined critical transport velocity. He observed
eration four types of closure relationships: translational velocity the effects of particle concentration (0.01%, 0.1%, 1% by vol-
(interface velocity between Taylor bubble and the liquid slug ume), particle diameter (20/¿m, 150/¿m, 300 ^m), liquid viscosity

Flow
Taylor Bubble

—^ -—^
Liquid Film

Fig. 2 Schematic of the siug unit (note: figure is not to scaie)

032905-2 / Vol. 135, SEPTEMBER 2013 Transactions of the ASME


(lcP, lOcP), and the pipe diameter (50.8 mm, 101.6mm) on the acoustic monitors and ER probes in slug flow. ER probes are in-
critical flow rates for particle transport. Experiments were per- trusive instruments which relate the metal loss to the change in
formed under single-phase (liquid and sand) and multiphase (liq- electrical resistance between sample and reference elements
uid, gas and sand) conditions. Hill found increasing particle where the sample element is exposed to the flow, whereas the
concentration, particle diameter, liquid viscosity or pipe diameter reference element is protected from the flow. He concluded that
increased the fluid flow requirements for particle transport. So, for ER probes are successful in detecting metal loss in the slug flow
similar particle size and the fluid flow characteristics, the erosion regime, and acoustic monitor output can be useful in detecting the
for smaller pipe sizes may be higher than larger one. sand rates. He also stated that acoustic monitor raw output
Al-lababidi et al. [14] studied the influence of pipe angle increases by increasing the particle size and these monitors are
(-1-5 deg inclined) on the solid particle transport for single-phase ineffective in detecting particle impacts of 20 fim particles i.e.,
water flow and air-water flow regimes. They conducted experi- finer particle sizes. Odigie [18] extended the acoustic monitor
ments using an average sand size of 200 ;um and varied the study to detect the threshold sand rate for annular, slug, and strati-
particle volume concentrations. In the inclined pipe, the efficient fied flow regimes.
means of particle transport was found to be in pseudo slug flow. It Rodriguez [19] developed a one-dimensional mechanistic
was found that the number of particles entrained in the pseudo model for erosion in slug flow using a stagnation length concept
slugs is higher, because of the increase in turbulence energy at the developed by Shirazi et al. [20]. In this approach, stagnation
front of the liquid slug body. This result has a direct influence length is the distance away from the wall where viscous effects
on erosion, since increasing the number of particle impacts at a are important. He calculated particle impact velocities by applying
specified location in the pipe increases the metal loss. Also, the a force balance on the particle which is used to compute erosion.
particles entrained in the liquid slug body possess high kinetic Finally, he compared the predictions of the model with the experi-
energy causing severe impacts with the pipe wall. Al-lababidi mental data and found good agreement with larger particle sizes.
et al. also mentioned that the change in gas throughput influences The model under predicted the erosion data collected using
the minimum transport condition of the particle. The authors smaller particles.
attributed this behavior to the change in turbulent intensities in the Throneberry [21] conducted measurements with smaller par-
liquid by increasing the gas velocity. They have also emphasized
ticles using ER probes installed on a bend and in a section of
that the change in the particle concentration has a significant
straight pipe. He extended the Rodriguez's model to two dimen-
impact on the particle transportation characteristics which is in
sions thereby considering both normal and tangential impacts of
agreement with the findings of Hill. Recently, Zeinali et al. [15]
the particles at the wall.
studied the influence of near wall turbulent structures on particle
removal from a deposited sand bed. They found with increase in The prior erosion measurements under the slug flow regime
time, the concentration of the finer particles on the pipe bottom were made at a maximum of two locations inside the bend due to
was increased, thereby coarser particles were removed by turbu- the size constraints associated with the ER probes. Therefore,
lent structures. The range of particle sizes they studied was from there is a need for a new measurement technology which enabled
0.1 ßm to 50fim. However, these experiments were performed in erosion inside the bend to be characterized in more detail.
a single-phase liquid flow, and the influence of gas-liquid on the
particle removal was not studied.
Objectives
As mentioned earlier, sand distribution characteristics in
Thus, it is clear that the experimental data is limited in the area
multiphase flows along with the transport characteristics influen-
of erosion in multiphase slug flow despite considerable studies
ces erosion. However, unlike the sand transportation data, the
being done on slug flow behavior. So, the objectives of the current
sand distribution data in the pipelines operating under multiphase
study are as follows:
flow regimes is extremely limited. McLaury et al. [16] studied the
influence of the distribution of sand particles in horizontal and the • Measure erosion inside a standard bend using the nonintru-
vertical annular flow on erosion. They said that the distributions sive state-of-the art UT at sixteen different locations in
of the particles and liquid are relatively uniform for the vertical single-phase (gas) flow with sand and multiphase air-water
pipe compared to the horizontal orientation. They found that the slug flow in horizontal pipes.
amount of liquid and sand collected at the centerline of the pipe • Study the influence of viscosity on erosion inside the bend.
increased by increasing the gas velocity. Particles travel in the gas • Predict erosion using a CFD for the gas-solid flows and com-
core at higher velocities, so more particles near the centerline pare to the measurements made.
cause more erosion. The nonuniform distribution of the particles • Conduct measurements using the flat head ER probe mounted
in the horizontal pipes was attributed to gravity. Also, they found at 45 deg to the bend and the angle-head probe mounted in a
that for a similar sand throughput the metal loss in the vertical straight pipe section.
pipe is higher than that for horizontal pipe which was attributed to • Also, compare UT erosion measurements around the 45 deg
the distribution of the particles. Entrainment of liquid and par- location in the bend to meastirements made using a flat head
ticles is less in horizontal flow, so more particles are in the slower ER probe.
moving liquid film than the gas core. Authors also tried to relate
the liquid film thickness to erosion magnitude, stating that the
increase in the liquid-film thickness in horizontal flow decreases Experimental Facility
erosion. However, the sand distribution behavior needs to be veri- The large scale tower boom loop at the University of Tulsa's
fied for the slug flow regime for which the sand transport charac- North campus is used for conducting erosion experiments. Figure 3
teristics are very different than other multiphase flow patterns. shows a schematic of the experimental facility. It has the potential
to generate a wide variety of flow patterns, and the test section
can be oriented at any angle between 0 and 90 deg. The major
Slug Flow Erosion-Previous Studies components of the loop are compressors, slurry tank, liquid injec-
The complexity in understanding erosion in slug flow is even tion port, gas injection port, test sections, and the collecting tank.
more complicated than slug flow alone as the additional phase The gas required in the test section is supplied by two independent
(solid) is introduced to the liquid and gas phases. There are very Ingersol Rand diesel compressors each with a capacity of 400
few studies in the literature studying erosion in slug flow. standard cubic feet per minute. The boom loop is also equipped
Gundameedi [17] conducted erosion experiments using an ER with a Caterpillar Sullair 375H air compressor rated with capacity
probes installed at a bend and in a straight pipe section in the slug of 375 cubic feet per minute to drive one set of the pumps (2.1
flow regime. His main objective was to study the performance of and 2.2) shown in Fig. 3. Pumps 2.1 and 2.2 are Ingersoll Rand

Journal of Energy Resources Technology SEPTEMBER2013, Vol. 135 / 032905-3


Boom Flat Head
ER Probe

Gas and ,,
Liquid

Acoustic
Gas I Sand
Monitor

Diesel Compressors Pump 2.1) Pump 2.2)

Fig. 3 Schematic of the experimental faciiity

ARO 3 "outlet metallic double diaphragm pumps, these are bigger Once the required superficial gas velocity is achieved, the pumps
pumps which provide a greater amount of liquid inside the test which supply the liquid to the test section are started. The flow
section. The other set of pumps (1.1 and 1.2) are used when lesser rate of the pumping liquid is calculated by measuring the drop in
amounts of liquid are needed inside the flow loop. The slurry tank the liquid level over a period of time. The desired liquid flow rate
has a capacity to hold 230 gallons of liquid, and it is equipped is achieved by adjusting the pressure supplied to the pneumatic
with a '/2 horsepower mixer. The mixer creates a homogeneous pumps.
slurry inside the tank keeping particles from settling at the bottom As this paper also shows measurements in single-phase (gas)
of the tank while conducting experiments. The boom tower is flow, the experimental procedure for generating gas-solid flows is
18 m long and is equipped with two pipe mountings to hold two explained as follows. First, the gas required inside the test section
different sized pipe sections. Another important component of the is achieved by adjusting the valves. Once the gas velocity required
loop is the collecting tank which separates gas from the flowing inside the test section is achieved, sand is injected via a port which
mixture. Gas is allowed to exhaust from the top of the collecting is downstream of the gas flow adjusting valve. Sand is initially
tank, whereas the liquid/solid mixture is pumped back into the filled in a graduated cylinder, and it is allowed to flow with the
slurry tank to conduct recirculating experiments. If once-through help of gravity. The valve at the bottom of the graduated cylinder
experiments were needed, the liquid/solid mixture was pumped to is used to adjust the sand flow rate. Gas moving at very high
a tank which is connected to a drain. The sand particles were velocity inside the pipeline will carry the particles which subse-
filtered using filter bags inside the tank before allowing the liquid quently erode the pipe bend. The gas and sand particles finally
to enter the drain. travel to the collecting tank where gas exhausts from the top of
The experimental procedure for generating the multiphase slug the tank, and the sand particles are deposited at the bottom of the
flow in the test section is explained as follows. The slurry mixture tank. These deposited particles were removed after finishing the
is prepared after ensuring all the valves are closed. The amount of erosion experiments by sending liquid into the collecting tank and
slurry mixture depends on the kind of flow pattern required inside pumping the slurry out of the collecting tank.
the test section. As the experiments presented in this paper are
for the slug flow regime, a large amount of liquid is needed as
compared to other flow regimes. Also in this paper, measurements
for different viscosities are shown. Particles Used in Erosion Experiments
To vary the viscosity, different amounts of carboxlmethyl cellu- Two different abrasive sand particles were used for the erosion
lose (CMC) are added. CMC is a polymer which is commonly measurements. California 60 mesh is the biggest sized particle.
used in the food industry as an additive. Adding CMC to the liquid The mean diameter (Dp) of the particle is 300 ßm. Figure 4 shows
will not alter its density significantly while changing the viscosity. the microscopic image of the California 60 mesh sand particles
It is highly advised to prepare the CMC solution in batches in a showing sharp edges.
separate container using a mortar mixer drill. These CMC solution The other sand particle size used in the experiments is Okla-
batches were dumped into the slurry tank until the desired quan- homa #1. The mean particle size of these particles is around
tity of liquid solution with predetermined viscosity is achieved. 150/¿m. Oklahoma #1 sand has rounded edges in comparison to
The viscosity of the liquid solution is measured using a Hydramo- the California 60 mesh sand. It is considered to be semirounded
tion Viscolite 700 portable viscometer. After the slurry prepara- sand, and Fig. 5 shows an image of the Oklahoma #1 sand.
tion process, the gas is injected into the test section. The valves In all the experiments, the initial sand concentration was kept
are adjusted to achieve the desired gas flow rate in the test section. constant irrespective of its size or shape. Concentration by weight

032905-4 / Vol. 135, SEPTEMBER 2013 Transactions of the ASME


Transntter

DebyLlne

Acoustic Baniw

Fig. 6 Component view of duai eiement ultrasonic transducer

ments at multiple locations on the bend. Also, the technique is


nondestructive, not disturbing the flow inside the elbow. The
ultrasonic wave speed inside the elbow is linear in the normal
200|im—I temperature range, so the thickness can be compensated for the
Fig. 4 Scanning electron microscopic image of California 60 temperature mathematically. The thickness of the pipe wall at the
sand particies location of interest can be determined by multiplying the velocity
of the sound wave in that particular material and the time required
to travel through that thickness. The transducers which perform
the dual role of sending and receiving are called dual element
transducers. In the present study, the pulse/echo technique is
implemented, and therefore dual element transducers are used.
The two elements (sending and receiving) of the dual element
transducer are separated by an acoustic barrier; therefore, the
elements are acoustically separated. Accommodating both ele-
ments in the same body has an advantage of avoiding the ring
down effect. Ring down effect occurs when an element receives
the ultrasonic energy while it is transmitting. This can be observed
when a single element is used in the probe body. Also, the ele-
ments in the dual element transducer are arranged at different
angles avoiding interference between the incoming and outgoing
waves. Figure 6 shows a schematic of a dual element transducer.

UT Data Acquisition Procedure


Long period experiments were not possible in the experimental
Oklahoma-« 220x setting for the erosion measurements. Compressors which provide
the necessary amount of gas into the test section can only operate
Fig. 5 Scanning electron microscopic image of the Okla- for a period of 6-8 h when started with a full tank of diesel.
homa#1 sand particles Hence experimental runtime is limited to 6-8 h. For the gas-sand
experiments, this time period is sufficient as it is highly erosive.
of the sand particles was maintained at 1% (i.e., around 9 kg of Maximum wall loss rates can be observed in real-time without
sand in 870.61 liters (230 gallons) of liquid). further analysis of raw data. This further analysis consists of
applying the temperature-compensated post processor algorithm
to the raw data. The temperature compensated post processor
Ultrasonic Testing for Measuring Erosion requires the appropriate temperature profile of the wall with nec-
A standard 76.2 mm (3-in.) elbow has been equipped with 16 essary variation, so as to provide reasonable metal loss results.
transducers at different locations mounted on the elbow. This ena- The temperature of the wall is measured from outside of the bend
bles the erosion pattern under different operating conditions to be by flush mounting 4 resistance temperature detectors (RTDs)
determined. The elbow test section can be removed from the against the outer elbow wall which are strapped tightly using
boom loop. This enables data acquisition to be performed before thin copper wires. The temperature changes significantly during the
and after the slug flow experiments. Before introducing the fluids experiments. A pseudo steady-state temperature profile is observed
inside the test section, the elbow is transported from an indoor to be acceptable for the temperature compensation post processor.
conditioned space and bolted to the flanges in position on the So the data collected during the pseudo steady state period is used
boom loop. Additional anchoring to the elbow is provided by for calculating the metal loss at the wall. The data gathered with
strapping the elbow tightly with belt and pipe holders. This is very high temperature gradients are excluded from the analysis.
necessary as slug flow is associated with vibrations in the loop, Time required to reach the pseudo steady state period is approxi-
and these vibrations may remove the elbow from the boom loop if mately 45 min for the gas-sand experiments during the experimen-
the necessary anchoring is not provided. tal run time. However, for the slug flow experiments, achieving the
pseudo steady-state during the experimental time period is not pos-
Transducers utilized in this work are manufactured by Olympus
sible due to the intermittent nature of the slug flow regime which
NDT, and the frequency of the transducers used is 10 MHz. The
significantly influences the temperature measurements. Figures 7
size of the transducers used in this work (approximately 6.35 mm
and 8 show the temperature profile of three different gas-sand and
(1/4 in.)) enables a relatively high sensor density on the outside of
multiphase slug flow experiments conducted during three different
the elbow. The high sensor density allows thickness measure-

Journal of Energy Resources Technology SEPTEMBER2013, Vol. 135 / 032905-5


S H Only Temperature ProMe

0 0.5 1 1.6 2 2.5 3 3.5 4 4.5 5 5.5 G 6.5

Fig. 7 Temperature profiles for single-phase (gas-sand) ero- Fig. 9 Picture showing the location of the transducers on the
sion experiments standard 3-in. elbow when attached to the testing section

Slug TeoiperaMire Profll«


Table 1 Operating conditions for the experiments performed
for the single-phase (gas-sand) flow pattern
Experiment VQ Observed Experiment Sand rate Sand size
no. (ft/s) flow pattern run time (h) (g/min) (jum)

1 110 Single-phase 4 68 150


2 108 Single-phase 3.75 69 150
3 95 Single-phase 3 69.6 150

UT Test Results
0 0.5 1 1.5 2 2.5 3 3.5 4 4.5 S 5.5 The elbow is equipped with 16 transducers, and the locations of
the transducers are shown in Fig. 9. The arrow showing the fiow
direction indicates the order of the transducers when placed in the
Fig. 8 Temperature profiles for multiphase slug (gas-liquid- testing section. The erosion patterns are presented for single-
sand) erosion experiments phase (gas) flow and multiphase slug flow regimes with sand.
Effects of particle size and viscosity on erosion are studied.
dates. These figures have the horizontal axis as the experimental
run-time and vertical axis as average surface temperature from the Single-Phase (Gas-Sand Flow). Initially, the experiments
mounted 4 RTDs. It is clear from the single-phase (gas-sand) were perfonned using gas (single-phase fiow) and sand. The
experiments that a pseudo steady-state temperature profile is experimental conditions are shown in Table 1. One reason for test-
achieved. But for the slug flow experiments, the temperature profile ing with 150 jum sand is the relative ease in dry sand injection.
is changing even after 4 h of experimental run-time. Temperature Typically, dry sand injection is much more difficult than injecting
profiles like these cannot be used for the temperature compensated sand along with liquid. The 150 ^m sand is more rounded and
post processor algorithm. In order to analyze the slug flow experi- flows through the sand injection device more easily than angular
mental data in real time, either the experiments need to be con- sand. Erosion in mm per year (mm/y) is reported by dividing the
ducted for longer periods or the temperature of the outside large metal loss by the experimental runtime. It is assumed that the
scale boom loop needs to be controlled. Both of the mentioned sol- metal loss rate is constant.
utions were not possible as experimental run-time is constrained by Figure 10 shows the erosion results in mm/y for a gas velocity
the diesel availability to the compressors and temperature control to of 33.5m/s (llOft/s) and a sand rate of 68g/min using 150/im
such a large scale loop is cost prohibitive. Instead, a simple before sand particles. The experimental run time for this test was 4h.
and after data capture is implemented. Before and after the experi- The location of the maximum erosion can be identified, and also
ment, data are gathered from the ultrasonic transducers where the the erosion pattern on the bend can be clearly seen. The maximum
elbow is moved indoors and is covered with insulation. Also, erosion location inside the bend is around 45 deg to the flow direc-
changing the direction of wall temperature gradient across the tion in the straight pipe. The repeatability of the single-phase flow
elbow wall is avoided by circulating warm air inside the elbow. experiment is tested by performing the same experiment with
This process always allows the heat transfer from inside the elbow more or less the same operating conditions.
to the outside room and also achieves a uniform temperature distri-
Figure 11 shows the erosion results for a superficial gas velocity
bution across the elbow. The components needed for the warm air
of 32.9 m/s (108 ft/s), sand rate of 69 g/min using 150/¡m particle
circulator are two sections of metÉil duct, a metal tee, a small heat
size and an experiment run time of 3 h and 45 min. Operating con-
source and an in-line vent blower. Air recirculates in a closed loop
ditions of this experiment are close to the conditions for Fig. 10.
across the heat source gaining heat and losing that heat gradually
The erosion pattern of Fig. 11 is similar to Fig. 10. The location of
until reaching the heat source again for more energy. Finally, metal
maximum erosion was clearly repeated. However, the magnitudes
loss is calculated from the temperature compensated post processor
of the erosion were not repeated. Still, the erosion magnitudes are
by inputting the file containing data of both before and after testing.
similar considering that erosion is a complex phenomenon and
More details on the temperature compensated post processor algo-
variations in results are anticipated. The possible reasons for the
rithm are provided by Grubb [22].
variation in the magnitude of erosion are as follows:

032905-6 / Vol. 135, SEPTEMBER 2013 Transactions of the ASME


Fig. 10 Erosion shown in mm per year (mm/y) for a single Fig. 12 Erosion shown in mm per year (mm/y) for a single
phase (gas + sand) experiment using 150/im sand at a gas ve- phase (gas + sand) experiment using 150/<m sand at a gas ve-
locity of 33.5 m/s and sand rate of 68 g/min for an experimental locity of 28.9 m/s and sand rate of 69.6 g/min for an experimental
runtime of 4 h runtime of 3 h

However, the location of maximum erosion did not change. This


implies that for gas-sand flows the location of maximum erosion
occurs at 45 deg in a standard bend.

Comparison of UT Single-Phase Erosion Results With CFD


Erosion Predictions. Past studies have shown good agreement
between experimental erosion rates and predicted erosion rates
using CFD for sand traveling in gas. So to gain confidence in the
erosion measurements for single-phase (gas) flows with sand
conducted using the ultrasonic technique, erosion results were
compared to CFD erosion predictions. This was done to achieve
assurance of the ultrasonic technology to continue the measure-
ments in the multiphase slug flow regime which is the prime focus
of this paper. Structured grid with regular sweep meshing was
used for the geometry of a horizontal straight pipe followed by a
standard elbow and a straight pipe of similar length connected at
the exit of the elbow. Grid independence was evaluated by exam-
Fig. 11 Erosion shown in mm per year (mm/y) for a single ining erosion values. 570,000 number of cell volumes are used for
phase (gas + sand) experiment using 150/(m sand at a gas ve- the current study. The boundary conditions were velocity inlet,
locity of 32.9 m/s and sand rate of 69 g/min for an experimental pressure outlet, and wall on the solid surfaces, ANSYS FLUENT Reyn-
runtime of 3 h 45 min olds stress 7 equation model was used for simulating turbulence
inside the flow domain. Discrete phase model was used to track
particles and the erosion/corrosion research center (E/CRC) ero-
sion equation was utilized to compute the magnitudes of the metal
• These experiments were conducted on different days, and the loss inside the bend. More details about the solution approach is
difference in humidity may affect the erosion results. For not mentioned here as CFD is not the focus of this paper.
higher humidity's, more moisture is present in the test section Figure 13 shows the comparison between CFD predictions and
which can cause particles to stick to the pipe walls. In severe the UT measurements for the gas-sand flows. The horizontal axis
cases, the particles may form a protective barrier on the bend shows the gas velocity in m/s and vertical axis shows the erosion
preventing subsequent erosion. This kind of phenomenon is rate in mm per year (mm/y). The bars in the plot show the CFD
also observed by the low liquid loading experiments con- predicted erosion rates and the maximum measured erosion rates.
ducted by Fan [23]. From this plot, it is clear that the predicted and the measured ero-
• There may be a little variation in sand flow rate into the test sion magnitudes were in good agreement.
section. The sand may become clogged in the sand injection
device. This mishap will prevent the sand from flowing until
it is cleaned. However, this effect can be limited by monitor- Multiphase Slug Flow Tests
ing the experiments closely.
The next set of experiments was conducted with slug flow. The
After examining the repeatability of the tests, erosion experi- erosion results in a standard 76.2 mm (3-in.) bend caused by
ments proceeded to the next step. The gas flow rate in the test sec- 150/im sand particles with 1 cP liquid viscosity are shown in
tion was reduced to observe the effect of gas velocity on the Figs. 14 and 15. Figure 14 shows the erosion pattern in a standard
erosion magnitude. Figure 12 shows the erosion pattern for the 76.2 mm (3-in.) bend with superficial gas and liquid velocities of
single-phase (gas) experiment with sand conducted at a gas veloc- 35.6 m/s (117 ft/s) and 0.7 m/s (2.4 ft/s), and the experiment is
ity of 28.9 m/s (95 ft/s) with sand flow rate of 69.5 g/min using conducted for a period of 5.4 hs. Figure 15 shows the erosion
150/im sand particles. As expected, this experiment demonstrates pattern for similar operating conditions as in Fig. 14 but with a
that decreasing the gas velocity decreases the erosion magnitude. superficial liquid velocity of 0.8 m/s (2.5 ft/s). Observing these

Journal of Energy Resources Technology SEPTEMBER2013, Vol. 135 / 032905-7


• CFD Erosion
s Measured Erosion

28.9 32.9 33.5


Gas Velocity [m/s]

Fig. 13 Comparison of CFD erosion predictions to the UT


measurements for gas-sand fiows
Fig. 15 Erosion pattern for 150 //m particle size with superficiai
gas and liquid velocities of 35.6 m/s and 0.8 m/s and iiquid vis-
cosity of 1 cP with an experimental run time of 5.4 h (erosion is
shown in mm/y, exp date: Juiy 29, 2011)

Fig. 14 Erosion pattern for 150 fim particie size with superficial
gas and liquid velocities of 35.6 m/s and 0.7 m/s and liquid vis-
cosity of 1 cP with an expérimentai run time of 5.4 h (erosion is
shown in mm/y, exp date: Aug. 2, 2011)

6 7 9 10 12
two figures, the location of highest erosion is similar for
these two different experiments. However, there is a difference Channel
in the magnitudes of erosion. To understand the amount of varia-
tion in erosion magnitudes, both sets of results are plotted Fig. 16 Comparing magnitudes of erosion measured by trans-
ducers numbered 4, 6, 7, 9,10, and 12 for the experiments con-
together. ducted Juiy 29, 2011 and Aug. 2, 2011 (neariy simiiar operating
Figure 16 shows the comparison of these two erosion experi- conditions in siug fiow)
ments. The magnitudes of erosion measured by transducers 4, 6,
7, 9, 10, and 12 were only considered for the comparison. These
locations experienced the most severe erosion in the slug flow
regime compared to the other locations. From Fig. 16, it can be Influence of particle size on erosion was also studied by
said that the location of maximum erosion is similar for the conducting experiments with 300//m particles. Figure 17 shows
experiments and the experimental magnitudes are comparable. the erosion experimental results with superficial gas and liquid
The percentage difference of erosion magnitude between experi- velocities of 33.5m/s (llOft/s) and 0.9m/s (3ft/s) using 1 cP
ments for transducers 4, 6, 7, 9, 10, and 12 are 30.8, 26.7, 31.8, liquid viscosity. This experiment was conducted for a period of
1.74, 52.8, and 31, respectively. For erosion experiments, these 5 h. It is noticed that the location of highest erosion did not shift
differences are considered to be acceptable. despite increasing the particle size. Definitely, the erosion magni-
tude increased since 300/¿m particles are sharper than the 150/¿m
Definitely for the slug fiow condition, the erosion pattern is sig-
sand particles. Also, the erosion is spread over a larger area as
nificantly different from the single-phase (gas-sand) flow. The dif-
compared to the 150^m experiments. It is shown that the majority
ferences observed in the erosion between these two flow patterns
of the transducers, other than the transducers lying at the bottom
are shown below:
of the elbow, measure erosion greater than 2.54 mm/y. The lower
• The location of highest erosion is slightly above of what was erosion at the bottom of the bend can be explained by the presence
observed for the gas-sand flows. of a slow moving liquid film that provides the bend some protec-
• The erosion magnitudes are significantly lower than for the tion. As with the experiments using 150/im sand particles, a simi-
gas-sand flow. This is due to the different particle behavior in lar study was done to examine the repeatability of the 300 ßm
the slug flow compared to the gas flow. slug flow experiment and found the results were in good

032905-8 / Vol. 135, SEPTEMBER 2013 Transactions of the ASME


Fig. 17 Erosion pattern for 300 ,/m particie size with superficiai pig. 19 Erosion pattern for 300 fim particie size with superficiai
gas and liquid veiocities of 33.5 m/s and 0.9 m/s and iiquid vis- ^„^ |¡ ¡^ veiocities of 35 m/s and 0.7 m/s and iiquid viscos-
cosity of 1 cP for experimental run time of 5 h (erosion is shown ¡ty ,,, 40 g ^p ^^^ expérimentai run time of 6.5 h (erosion is
Shown in mm/y)

1 10
Viscosity [cP]
Fig. 18 Erosion pattern for 300 /im particie size with superf iciai
gas and iiquid velocities of 35.6 m/s and 0.7 m/s and liquid vis- Fig. 20 Liquid viscosity effect on erosion in slug flow
cosity of 10 cP for expérimentai run time of 6.5 h (erosion is
shown in mm/y)
unknown). As performed for previous experimental conditions,
the experiment for the 10 cP liquid viscosity was conducted again
agreement. The difference in the maximum erosion values to observe the repeatability and the results were agreeable. The
between these two experiments was 8.3%. difference in the maximum erosion values obtained for 10 cP liq-
The effect of liquid viscosity was studied after studying the uid viscosity experiments was 16.8%. To further investigate the
influence of particle size on the erosion pattern. For this study, behavior of erosion as a function of viscosity, experiments were
liquid with viscosities of 10 cP and 40 cP were considered. conducted with a liquid viscosity of 40 cP. It should be mentioned
Figures 18 and 19 show the erosion magnitude patterns for similar that conducting experiments with higher liquid viscosity, in this
superficial velocities with liquid viscosities of 10 cP and 40 cP. case 40 cP, is extremely challenging. The particles tend to stick to
Figure 18 shows the erosion magnitude pattern for superficial gas the surface of the slurry tank even though a powerful mixer is in
and liquid velocities of 35.6 m/s (117 ft/s) and 0.7 m/s (2.4 ft/s) use to keep the sand particles suspended. To alleviate this issue,
with liquid viscosity of 10 cP and particle size of 300/im for an hand stirring was also implemented. Figure 19 shows the erosion
experimental run time of 6.5 h. The location of the highest erosion magnitude plot for the superficial gas and liquid velocities of
is similar to the other slug flow tests even with the change in liq- 35 m/s (115 ft/s) and 0.7 m/s (2.3 ft/s) using 300 ßm sand particles
uid viscosity. Also, interestingly it is observed that the erosion with liquid viscosity of 40 cP and an experimental run time of
magnitudes measured by the transducers were slightly higher than 6.5 h. This plot implies that the location of the highest erosion did
that measured for the viscosity of 1 cP. The reason behind this not change by changing the viscosity of the liquid for the operat-
behavior is still unidentified. A possible reason for this behavior ing conditions examined. However, the magnitude of highest ero-
may be more gas entrainment in the liquid slug body. Similar to sion dropped by approximately three times compared with 1 cP
the previous experimental results, the transducers mounted at the and 10 cP experiments. It seems that there are very few locations
bottom of the pipe bend measure minimal or no metal loss due to inside the bend that experience severe erosion under these
the movement of the slow moving liquid fllm (note: some of the viscosities.
transducers of the bend shown in red in Figs. 14, 15, 18, and 19 Erosion rate as a function of viscosity is shown in Fig. 20. Hori-
provided surprising results. The reason for these results is still zontal axis shows the viscosity in centipoise, and the vertical axis

Journal of Energy Resources Technology SEPTEMBER2013, Vol. 135 / 032905-9


• ER@45 Anglehead
• UT@45 • UT Maximum

UJ

35.7 28.0 32.9 33.5 25.9 35.7 35.7 28.0 32.9 33.5 25.9 35.7 33.5
0.7 0.4 0.7 0.7 0.8 0.7 0.7 0.4 0.7 0.7 0.8 0.7 0.7 Vsu[m/s]
1 1 10 1 1 10 1 1 10 1 1 10 40 JJ[CP]
150 150 150 300 300 300 Size [Mm] 150 150 150 300 300 300 300 Size [pm]

Fig. 21 Comparison of erosion magnitudes at variety of oper- Fig. 22 Erosion magnitudes comparison between UT maxi-
ating conditions in a slug flow regime using a flat head ER mum erosion and the erosion measured using the angle-head
probe and the ultrasonic transducer mounted at 45 deg to the probe mounted in the straight pipe section in slug flow regime
bend under variety of operating conditions and particle sizes

shows the averaged erosion rate at transducer number 6 in mm/y


(note: this transducer measures the highest erosion). The location between highest erosion measured for the elbow using the ultra-
of highest erosion in the slug fiow regime is independent of vis- sonic instrument and the erosion measured using the angle-head ER
cosity but the magnitude depends on fluid viscosity. The averaged probe. The bars in Fig. 22 show the erosion magnitudes measured
erosion rate at transducer 6 for the 10 cP viscous fluid is slightly using ultrasonic transducers and the fiat head angle-head probe.
higher than 1 cP. However, the averaged erosion rate at transducer From the data comparison, irrespective of the operating conditions,
6 for the 40 cP viscous fluid is significantly lower than 1 and it is evident that the angle-head measurements were higher than the
10 cP liquid viscosities. The reason is that the slugs for the 40 cP highest erosion measured for the bend. One explanation of the
liquid viscosity are not as energetic compared with 1 cP or 10 cP. results is the blockage provided by the probe. The 25.4mm (1-in.)
The turbulence associated with 40 cP liquid slugs are lower than diameter angle-head probe is inserted into a 76.2 mm (3-in.) diame-
the other lower viscosities, thereby reducing the particle impact- ter pipe thereby increasing the local fluid velocity resulting in
ing velocities at the wall and subsequently causes decreased higher velocity particle impacts. These higher velocity particle
metal loss. However, as explained previously the reason for the impacts cause higher measured metal loss using the angle-head
unexpected behavior of erosion magnitudes for the 10 cP liquid probe compared to the maximum metal loss occurring inside the
viscosity is an unknown. The exploration of this behavior is bend. Therefore, the measurements from the angle-head probe are
planned for future research. conservative when using these results as a guide for erosion in
bends.

Comparison of Nonintrusive UT Data for Slug Flow


to the Intrusive ER Prohe Data Conclusions
Slug flow erosion data collected using the ultrasonic transducer Erosion experiments were performed implementing the ultra-
mounted on the outside wall around 45 deg to the flow direction sonic technique in a 76.2 mm (3-in.) diameter pipe on a standard
was compared to the data gathered using the flat head ER probe elbow. Several conclusions were drawn from the current study
mounted flush to the inside elbow wall mounted at 45 deg. and they are stated as follows:
ER probe experiments were performed separately on a different • Novel noninvasive nano UT permanent placement tempera-
stainless steel elbow equipped with the probe. Necessary precau- ture compensated ultrasonic wall thickness device was devel-
tions were taken to conduct erosion experiments using ER probes oped for this work. It was successful identifying the erosion
by generating similar operating conditions in the test section com- pattern on a standard bend.
pared to the ultrasonic experiments. Figure 21 shows that compar- • Location of highest erosion for the single-phase (gas) fiow
ison with horizontal axis as superficial liquid velocity, superficial was identified around 45 deg to the bend whereas the location
gas velocity, dynamic viscosity and the particle size. The vertical of highest erosion in slug flow was identified at the top of the
axis is erosion rate in mm/y. The bars in Fig. 21 show the erosion bend.
magnitudes measured using ultrasonic transducers and the flush • Erosion measurements in the single-phase fiow were com-
mounted electrical resistance probes. It is evident that the data pared to the CFD predictions and the results were reasonably
collected with these two instruments are agreeable irrespective of agreeable.
the operating condition or particle size. After the comparison • Under the slug flow regime, transducers mounted at the bot-
between the instruments, the maximum erosion obtained through tom of the elbow measured very low erosion as the bottom of
the measurements using the UT instrument were compared to the the elbow is protected by a slow moving liquid film.
erosion data collected using the angle-head ER probe mounted • Erosion measurements were obtained using 150 ^im and
inside the straight pipe section. This was done as oil and gas pro- 300/im particle sizes. Increasing the particle size increased
ducers tend to measure erosion by inserting the probe in the the metal loss. The location of maximum erosion was unal-
straight section due to accessibility. For the current measurements tered by increasing the particle size in the slug flow regime.
with the angle-head probe, the probe is inserted from the top of It should be noted the 300 ßm particles were sharper than the
the pipe until the center of the head of the probe reached the cen- 150/im particles.
terline of the pipe section. The diameter of the angle-head probe
• In the slug flow regime erosion measurements, there is a
used was 25.4 mm (1-in.). Figure 22 shows the comparison
slight increase in erosion magnitude in a bend for 10 cP

032905-10 / Vol. 135, SEPTEMBER 2013 Transactions of the ASME


viscous liquid compared to 1 cP. However, there is a signifi- [5] Nydal, O. J., Pintus, S., and Andreussi, P., 1992, "Statistical Characterization of
Slug Flow in Horizontal Pipes," Int. J. Multiphase Flow, 18, pp. 439-453.
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This material is based upon work supported by the E/CRC [11] Zhang, H.-Q., Wang, Q., Sarica, C , and Brill, J. P., 2003, "A Unified Mechanis-
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[12] Pereyra, E., Arismendi, R., Gomez, L. E., Mohan, R. S., Shoham, O., and
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Production Assurance Technology group at the ConocoPhillips p. 023001.
Bartlesville Technology Center in Bartlesville, Oklahoma. Thanks [13] Hill, A. L., 2011. "Determining the Critical Flow Rates for Low-Concentration
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[14] Al-lababidi, S., Yan, W., and Yeung, H., 2012, "Sand Transportations and Dep-
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[15] Zeinali, H., Toma, P., and Kuru, E., 2012, "Effect of Near-Wall Turbulence
cP = centipoise on Selective Removal of Particles From Sand Beds Deposited in Pipelines,"
CMC = carboxymethyl cellulose ASME J. Energy Resourc. Technol., 134(2), p. 021003.
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Journal of Energy Resources Technology SEPTEMBER2013, Vol. 135 / 032905-11


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