ATOMER Analysis Tests Consulting

ATOMER
ANALYSIS - TESTS
CONSULTING IN MATERIALS
& CHEMISTRY
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contact@atomer.fr
contact@atomer.fr ATOMER ©
The analysis engineering division
Analysis in all its forms

The entire range of the latest technology as more
conventional situations in the most diverse
♦ Analysis satisfying standards ASTM, ISO, DIN, ...
♦ Reverse engineering
♦ Find a contaminant or additive
♦ Analysis for expertise in litigation

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contact@atomer.fr
Performance analysis
♦ Appropriate and effective solutions
♦ Personalized support
♦ Timeliness of customer
♦ Total confidentiality
♦ Rates very competitive

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contact@atomer.fr
Equipment performance and skills

in sampling and interpretation
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contact@atomer.fr
The methods available to the analyst are :
• Separative methods for sample preparation : filtration,

precipitation,, fractionation
precipitation fractionation,, various chromatographies
• Spectroscopic methods : multinuclear NMR, FTIR,

UV--visible
UV visible,, Raman, MS, RX, ESCA, ...
• Colorimetric assays and various tests
• Electrochemical methods
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contact@atomer.fr
CHROMATOGRAPHY :
Thin Layer Chromatography (HPTLC)
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contact@atomer.fr
VACCUM FILTRATION POLYMERS
PRECIPITATION
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ROTATIVE EVAPORATION
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SOXHLET EXTRACTION
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SPECTROSCOPY :
FTIR with many accessories
PERKIN-ELMER FTIR spectrometer vertical ATR with variable angle

KRS-5 crystal
49 €/spectrum
Diamond ATR Specular reflexion

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contact@atomer.fr
SPECTROSCOPY :
UV-VISIBLE (Additives research & quantification)
www.atomer.fr Spectrophotometer UV-visible LAMBDA 35

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QUANTITATIVE COLORIMETRY :
• Precision spectrocolorimetry designed for the measurement

of liquid and transparent colored plastics ...
• Standards methods : Iodine index, Gardner, Hazen (Pt Pt--Co

Co))
Klett,, Saybolt
Klett Saybolt,, ASTM D-
D-1500, Lovibond
Lovibond,, Ly
Ly,, Lr
Lr,, (Tx
(Tx,,Ty
Ty,,Tz
Tz))
(X,Y,Z), Lab
Lab**-CIE, …
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contact@atomer.fr
QUALITATIVES COLORIMETRIC TESTS
White cloud
polyurethane
Filter paper
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contact@atomer.fr
QUALITATIVES COLORIMETRIC TESTS
Violet : 1,5-NDI
Specific reactive
Red-brown :
2,4 & 2,6-TDI
2,4-TDI dimerized
Yellow : 4,4’-MDI
Red : TMP & TDI

addition products
Uncolored :
aliphatic
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isocyanates
contact@atomer.fr
Physical and mechcanical tests :
• Thermal & thermo

thermo--mechanical methods : DSC, TMA, ATG,
DMA, HDT, …
• Mechanical tests : Tensile

Tensile,, flexion, compression
• Rheological methods : viscosimeters

viscosimeters,, rheometers
rheometers,, …
• Fire - Smoke tests
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contact@atomer.fr
Heat Deflection Temperature (HDT)
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contact@atomer.fr
Melt Fluid Index (MFI)
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contact@atomer.fr
MECHANICAL TESTS :
TENSILE-COMPRESSION-FLEXION
TENSILE &
COMPRESSION
TESTS
45 € / 5 pieces
www.atomer.fr Extensometer ZWICK 1455

contact@atomer.fr
MECHANICAL TESTS :
TENSILE-COMPRESSION-FLEXION
Extensometer INSTRON 5867. Extensometer INSTRON 5544.

www.atomer.fr
contact@atomer.fr
MECHANICAL TESTS :
TESTS STANDARDS OFF - MAKING PIECES
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contact@atomer.fr
RESILIENT TESTS
1 Joule / 4 J / 7,5 J
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contact@atomer.fr
HARDNESS
Persoz
Shore A & D
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HARDNESS
Vickers
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contact@atomer.fr
Testing of nano-indentation with the Nano indenter XP
Measuring the hardness and modulus of elasticity (including dynamic modules)
The measurement by nano-indentation is to implement and monitor expenses as low as a

few tens of micro-Newtons (μN) and up to several hundred Millinewton (mN) with an
accuracy μN
The advantage of the instrument of nano-indentation is its ability to measure with

nanometer resolution, depth of penetration up to a few tens of nm with an accuracy <nm
Field of paints, lacquers, varnishes, eye layers (sol-gel),

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microelectronics, cosmetics films
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ABRASION RESISTANCE
Linear Taber
Circular Taber
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RHEOLOGY :
RHEOMETER
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RHEOLOGY :
BROOKFIELD VISCOSIMETER
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KINETIC RHEOLOGY :
PENDULAR VISCOSIMETER
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contact@atomer.fr
POLYMERS THERMAL ANALYSIS
(DIFFERENTIAL SCANNING CALORIMETRY)
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contact@atomer.fr
Some applications of thermal analysis by differential scanning calorimetry in
the field of plastics and polymers :
* Identify the softening point of a material ;

* Compare the effects of additives on the material ;
* Determine the glass transition temperature (Tg) ;
* Determine the degree of crystallinity and melting temperature (Tm ) ;
* Determine the minimum temperature in the manufacturing process of a material ;
* Determine the amount of energy needed to melt the material ;
* Quantify the material specific heat (Cp) ;
* Run a test of stability in oxygen, OIT: Oxidation Induction Time ;
* Understand and quantify the kinetics of reaction of thermosetting material during its
cooking ;
* Compare the doneness of a material relative to another ;
* Characterize material when it reacts under ultraviolet light ;
* Characterize material at its cooking temperature ;
* Determine the crystallization temperature (Tc) during cooling.
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contact@atomer.fr
Thermogram of a thermoset polymer and measure its
glass transition temperature (Tg)
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contact@atomer.fr
Thermogram of the reaction of a mixture of monomers
(thermosetting) and partial and total integration of the exothermic
reaction of polymerization (crosslinking)
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contact@atomer.fr
OIT : Oxidation Induction Time
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contact@atomer.fr
(THERMOGRAVIMETRIC ANALYSIS)
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contact@atomer.fr
(THERMOGRAVIMETRIC ANALYSIS)
Some applications of the TGA in plastics are
listed below :
* Determine the amount of filler material in weight percent ;
* Determine the amount of ash material in weight percent ;
* Characterize the mass loss of a material over a range of temperature ;
* Characterize the mass loss vs material. time at a given temperature ;
* Quantifying the loss of water, solvent, or plasticizer or additive in a certain

range of temperature ;
* Examine the properties of flame retardant material ;
* Examine the combustion properties of a material.

www.atomer.fr
contact@atomer.fr
ACCELERATED PHOTOAGEING
(Q-UV + Spray)
Simulation of energy rays of the solar spectrum. Programming

condensation temperature cycles (simulation of the morning dew) and
UV, water spray to test the degradation produced by rain, perfectly
simulates the thermal shock
www.atomer.fr
contact@atomer.fr
ACCELERETED PHOTOAGEING
(SUNTEST)
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contact@atomer.fr
DETERMINATION OF LIQUIDS MOISTURE
(KARL FISCHER COULOMETRY)
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contact@atomer.fr
FIRE – SMOCK TESTS
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contact@atomer.fr
METALLOGRAPHY
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contact@atomer.fr
Website : www.atomer.fr
www.atomer.fr
contact@atomer.fr

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ATOMER

Analysis in all its forms

♦ Analysis satisfying standards ASTM, ISO, DIN, ...

♦ Find a contaminant or additive

♦ Analysis for expertise in litigation

♦ Appropriate and effective solutions

♦ Rates very competitive

Equipment performance and skills

• Separative methods for sample preparation : filtration,

• Spectroscopic methods : multinuclear NMR, FTIR,

• Colorimetric assays and various tests

PERKIN-ELMER FTIR spectrometer vertical ATR with variable angle

Diamond ATR Specular reflexion

www.atomer.fr Spectrophotometer UV-visible LAMBDA 35

• Precision spectrocolorimetry designed for the measurement

• Standards methods : Iodine index, Gardner, Hazen (Pt Pt--Co

Red : TMP & TDI

• Thermal & thermo

• Mechanical tests : Tensile

• Rheological methods : viscosimeters

• Fire - Smoke tests

www.atomer.fr Extensometer ZWICK 1455

Extensometer INSTRON 5867. Extensometer INSTRON 5544.

The measurement by nano-indentation is to implement and monitor expenses as low as a

The advantage of the instrument of nano-indentation is its ability to measure with

Field of paints, lacquers, varnishes, eye layers (sol-gel),

* Identify the softening point of a material ;

* Determine the amount of filler material in weight percent ;

* Determine the amount of ash material in weight percent ;

* Characterize the mass loss of a material over a range of temperature ;

* Characterize the mass loss vs material. time at a given temperature ;

* Quantifying the loss of water, solvent, or plasticizer or additive in a certain

* Examine the properties of flame retardant material ;

* Examine the combustion properties of a material.

Simulation of energy rays of the solar spectrum. Programming

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