UTHM Lab Manual - Pressure Measurement

FACULTY : ENGINEERING 1
EDITION:
TECHNOLOGY
LABORATORY: CHEMICAL 1
REVISION NO:
ENGINEERING TECHNOLOGY
16 MAY
EFFECTIVE DATE:
EXPERIMENT: PRESSURE 2016
MEASUREMENT AMENDMENT
DATE:
FACULTY OF ENGINEERING TECHNOLOGY
DEPARTMENT OF CHEMICAL ENGINEERING TECHNOLOGY
PROCESS INSTRUMENTATION LABORATORY

LABORATORY INSTRUCTION SHEETS
COURSE CODE BNQ 30203

EXPERIMENT NO. EXPERIMENT 1
EXPERIMENT TITLE PRESSURE MEASUREMENT
DATE
GROUP NO.
1) Engr. Dr. Nasrul Fikry Che Pa
LECTURER/INSTRUCTOR/TUTOR
2) Mr Mohd Syazwan Mohd Ghazali
DATE OF REPORT SUBMISSION
ATTENDANCE/PARTICIPATION/DISIPLINE: /5%
INTRODUCTION: /5%
PROCEDURE: /5%
RESULTS& CALCULATIONS /15%
ANALYSIS /15%
DISTRIBUTION OF MARKS FOR DISCUSSIONS: /20%
LABORATORY REPORT: ADDITIONAL QUESTIONS /15%
CONCLUSION /10%
SUGGESTIONS& RECOMENDATIONS /5%
REFERENCES: /5%
TOTAL: /100%
EXAMINER COMMENTS: RECEIVED DATE AND STAMP:

EDITION:
TECHNOLOGY
REVISION NO:
16 MAY
EFFECTIVE DATE:
DATE:
STUDENT CODE OF ETHICS
DEPARTMENT OF CHEMICAL ENGINEERING TECHNOLOGY
FACULTY OF ENGINEERING TECHNOLOGY
I hereby declare that I have prepared this report with my own efforts. I also admit to
not accept or provide any assistance in preparing this report and anything
that is in it is true.
1) Group Leader: ………………………………………….. (Signature)

Name : __________________________________
Matrix No. : __________________________________
2) Group Member 1: ………………………………………. (Signature)

Name : __________________________________
Matrix No : __________________________________
3) Group Member 2:……………………………………….. (Signature)

Name :__________________________________
Matrix No. : __________________________________
EDITION:
TECHNOLOGY
REVISION NO:
16 MAY
EFFECTIVE DATE:
DATE:
1.0 OBJECTIVES
a) To study the difference of pressure measurement by using different types of
pressure instrument.
b) To compare the accuracy of instrument involved in the measurement of
pressure.
2.0 LEARNING OUTCOMES

At the end of the study, student will be able to:
a) To be familiar with the basic steps of machine from start-up to shut-down
with proper handling and setting.
b) To examine the obtained data of pressure measurement by using different
types of pressure instrument.
3.0 INTRODUCTION
The experiment serve as a continuity for the previous experiment on
identifying and recognizing the function of various equipment, instrumentation
and process involved in chemical and analytical process control system. For this
experiment, the activities focus on examining the data that obtained from
different types of pressure instrument in order to compare the accuracy of the
device.
4.0 INSTRUMENTS /APPARATUS / CHEMICAL / REAGENTS

4.1 Chemicals / Reagents
a) Water
4.2 Apparatus
a) The schematic diagram is shown in Figure 1.
EDITION:
TECHNOLOGY
REVISION NO:
16 MAY
EFFECTIVE DATE:
DATE:
Figure 1: Schematic diagram of Pressure Measurement System

EDITION:
TECHNOLOGY
REVISION NO:
16 MAY
EFFECTIVE DATE:
DATE:
5.0 PROCEDURE
1 Plant Start-up Procedures
1. Switch ON the main power supply. The switch is at the front of the
panel/cubicle.
2. Check that all the manual valves including the vent (V) and bottom drain
(D) valves are shut.
3. Open the manual valve MV3 at the Pressure Gauge (PG). Check the reading
at Pressure Gauge (PG). If the Pressure Gauge (PG) shows some value of
pressure in Tank TI, open the Vent (V) or bottom drain (D) valves to release
the pressure in tank. This is done until the Pressure Gauge (PG) shows a
‘zero’ reading.
4. Connect the Manometer (AMETEK JOFRA CPC-200 INDG) properly to the

Tester Tapping Point, MV 8.
1.2 Experiment 1 (Measurement)
1. Check that the main power supply at the front panel is switched ON.
2. Open manual valves MV1 connected to PT1, MV2 connected to PT2 and
MV3 connected PG. Check that all other manual valves are fully shut.
3. Check that the AFR is at the set pressure of 30 psig.
4. Open manual valve MV6 next to AFR to fill up the Pressure Tank, T1.
5. Check that the Manometer is properly connected to the tester tapping point,
MV8. Open fully the manual valve, MV8.
6. Check the readings at the Manometer and Pressure Gauge (PG). Once the
pressure readings in both the instruments are stabilized, manual valve MV6
is shut fully.
7. Run the experiment

 Suggested pressure: 30 psig
 Check the readings at the Manometer and Pressure Gauge (PG). Once
the pressures readings in both the instruments are stabilized shut the
vent (V) valve and record the data in Table 1.
 Open the Vent (V) valve to release the pressure to the next suggested
pressure.
 Continue measure the pressure from 25 psig until 0 psig.
1.3 Experiment 2 (PT1 Site Calibration)

EDITION:
TECHNOLOGY
REVISION NO:
16 MAY
EFFECTIVE DATE:
DATE:
2. Shut MV1 valve to isolate PT1 from the plant.
3. Remove the tubing connected to the transmitter.
4. Then, fix a vacuum pump (AMETEK MODEL T-750) to the transmitter to
obtain a pressure. FIGURE 1.1
5. Connect the Manometer properly to PT1. FIGURE 1.1
6. Once this is done, a Multimeter (GW MODEL GDM-391A) is connected to
PT1 to obtain the output signal from the transmitter for all the tested site
calibration ranges. FIGURE 1.2
7. Configuration of PT1 can be carried out to access information of the
transmitter.
1.4 Experiment 3 (PT2 Site Calibration)
2. Shut MV2 valve to isolate PT2 from the plant.
3. Remove the tubing connected to the transmitter.
4. Then, fix a vacuum pump (AMETEK MODEL T-750) to the transmitter to
obtain a pressure.
5. Connect the Manometer properly to PT2.
6. Once this is done, a Multimeter (GW MODEL GDM-391A) is connected to
PT2 to obtain the output signal from the transmitter for all the tested site
calibration ranges.
7. Configuration of PT2 can be carried out to access information of the
transmitter.
Plant Shut-down
1. Make sure that the remaining air in pressure tank, T1 is released with vent
(V) valve fully open.
2. Shut the manual valve MV6 next to AFR and all other manual valves fully.
3. Reconnect the original tubing of both PT1 and PT2.
4. Switch OFF the main power supply to the plant at the front of the panel/
cubical.
EDITION:
TECHNOLOGY
REVISION NO:
16 MAY
EFFECTIVE DATE:
DATE:
6.0 RESULTS & CALCULATIONS
TABLE 1: Pressure Measurement

RUN I SET 1 SET 2 Average
A Suggested Pressure, psig 30.00 30.00 30.00
B Actual Gauge Pressure, psig
C Gauge Pressure, psig
D Gauge Pressure, psig
E Absolute Pressure, psia
F=B+ 14.70 Calculated Absolute Pressure, psia
G1 = | B — C |
At Pressure Gauge
Gauge Pressure
G2 = | B — D Deviation, psig At Pressure
| Indicator,
P12
H=|F—E| Absolute Pressure Deviation, psia
RUN II SET 1 SET 2 Average

G1 = lB — Cl At Pressure
Gauge pressure Gauge
Deviation, psig At Pressure
G2 = lB — Dl
Indicator, P12
H = IF — El Absolute Pressure Deviation, psia
EDITION:
TECHNOLOGY
REVISION NO:
16 MAY
EFFECTIVE DATE:
DATE:
RUN III SET 1 SET 2 Average

Gauge pressure Gauge
G2 = lB — Dl Deviation, psig At Pressure
Indicator, P12
RUN IV SET 1 SET 2 Average

Gauge Pressure Gauge
Indicator, P12
EDITION:
TECHNOLOGY
REVISION NO:
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EFFECTIVE DATE:
DATE:
RUN V SET 1 SET 2 Average

Indicator, P12
RUN VII SET 1 SET 2 Average

Indicator, P12
EDITION:
TECHNOLOGY
REVISION NO:
16 MAY
EFFECTIVE DATE:
DATE:
RUN VI SET 1 SET 2 Average

Indicator, P12
Remarks:
B: Read from the Manometer (AMETEK JOFRA CPC-200 INDG).

C: Read from the Pressure Gauge (PG).
D: Read from the Pressure Indicator (PI2) on the front panel.
E: Read from the Pressure Indicator (PI1) on the front panel.
EDITION:
TECHNOLOGY
REVISION NO:
16 MAY
EFFECTIVE DATE:
DATE:
7.0 ANALYSIS OF THE RESULTS
Analysed critically each results obtain in section 6.0 by referring to the

theory/introduction parts. Find reasons (suggested reasons) on each
occurrence shown in the results.
8.0 DISCUSSIONS
Discuss the overall experiment on data obtain based on your understanding.
Discussion should relate reasons for the phenomena/results obtained,
theoretical parts, suggested reasons (if necessary but back with sound
theoretical knowledge) and your overview understanding.
9.0 ADDITIONAL QUESTIONS

i. State whether the pressure is higher/lower/equal at the bottom of a tank
filled with a gas than at the top.
ii. Differentiate absolute pressure and gauge pressure.
iii. If the contents of a tank holding 20m3 of gas are transferred to a tank
with twice as much volume and all other factors remain unchanged, what
will happen to gas pressure?
iv. If the gas in a tank heated and all other factors remain unchanged, what
will happen to the gas pressure?
v. What is the pressure measuring instrument used in this plant?
vi. Discuss briefly the possible errors affecting the accuracy in pressure
measurement as observed in the experiment.
10.0 CONCLUSION
Conclusion is merely a summary of the important findings already reported
in the discussion section. It also relates to the objectives stated earlier.
EDITION:
TECHNOLOGY
REVISION NO:
16 MAY
EFFECTIVE DATE:
DATE:
11.0 SUGGESTIONS & RECOMMENDATIONS
Your ideas of suggestion & recommendation to improve the learning process
for this experiment or anything related to the experimental procedure etc.
12.0 REFERENCES
Minimum of at least 5 references (with 3 of them are paper/book/chapter
based)
Prepared by/Disediakan oleh : Approved by/Disahkan oleh :
Signature/Tandatangan : Signature/Tandatangan :
Name/Nama : DR. NASRUL FIKRY BIN CHE PA Name/Nama : PROF. MADYA DR. ISHAK BABA
Date/Tarikh : Date/Tarikh :

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FACULTY : ENGINEERING 1

PROCESS INSTRUMENTATION LABORATORY

COURSE CODE BNQ 30203

EXPERIMENT TITLE PRESSURE MEASUREMENT

EXAMINER COMMENTS: RECEIVED DATE AND STAMP:

STUDENT CODE OF ETHICS

DEPARTMENT OF CHEMICAL ENGINEERING TECHNOLOGY

FACULTY OF ENGINEERING TECHNOLOGY

1) Group Leader: ………………………………………….. (Signature)

2) Group Member 1: ………………………………………. (Signature)

3) Group Member 2:……………………………………….. (Signature)

2.0 LEARNING OUTCOMES

4.0 INSTRUMENTS /APPARATUS / CHEMICAL / REAGENTS

Figure 1: Schematic diagram of Pressure Measurement System

4. Connect the Manometer (AMETEK JOFRA CPC-200 INDG) properly to the

1.2 Experiment 1 (Measurement)

3. Check that the AFR is at the set pressure of 30 psig.

7. Run the experiment

1.3 Experiment 2 (PT1 Site Calibration)

1.4 Experiment 3 (PT2 Site Calibration)

TABLE 1: Pressure Measurement

RUN II SET 1 SET 2 Average

RUN III SET 1 SET 2 Average

RUN IV SET 1 SET 2 Average

RUN V SET 1 SET 2 Average

RUN VII SET 1 SET 2 Average

RUN VI SET 1 SET 2 Average

B: Read from the Manometer (AMETEK JOFRA CPC-200 INDG).

Analysed critically each results obtain in section 6.0 by referring to the

9.0 ADDITIONAL QUESTIONS

ii. Differentiate absolute pressure and gauge pressure.

v. What is the pressure measuring instrument used in this plant?

Prepared by/Disediakan oleh : Approved by/Disahkan oleh :

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