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This test method is not for resale.

Copyright © 2012 American Association of Textile Chemists and Colorists


AATCC Test Method 8-2007

Colorfastness to Crocking: Crockmeter Method


Developed in 1936 by AATCC Commit- for information purposes only. The pre- tant to avoid incorrect test results where
tee RA38; revised 1937, 1952, 1957, cautions are ancillary to the testing proce- abnormal crock images can result and in-
1961, 1969, 1972, 1985, 1988, 1996, dures and are not intended to be all inclu- fluence the rating process.
2004, 2005, 2007; reaffirmed 1945; sive. It is the user’s responsibility to use 6.2 Use the Crockmeter Verification
1989; editorially revised and reaffirmed safe and proper techniques in handling Cloth or in-house poor crocking fabric
1968, 1974, 1977, 1981, 1995, 2001; materials in this test method. Manufac- with known behavior and conduct three
editorially revised 1986, 2002, 2008 turers MUST be consulted for specific dry and wet crock tests.
(with title change), 2009, 2010, 2011. details such as material safety data sheets 6.2.1 A poor circular image with un-
Partly equivalent to ISO 105-X12. and other manufacturer’s recommenda- even dye pick-up may indicate the crock-
tions. All OSHA standards and rules ing finger needs resurfacing (see 13.7).
must also be consulted and followed. 6.2.2 A double, elongated image may
1. Purpose and Scope 4.1 Good laboratory practices should indicate a loose clip (see 13.7).
be followed. Wear safety glasses in all 6.2.3 A stretched and streaked crock
1.1 This test method is designed to de- laboratory areas. image may be due to mounting the crock
termine the amount of color transferred square diagonally.
from the surface of colored textile materi-
als to other surfaces by rubbing. It is ap-
5. Apparatus and Materials (see 13.1) 6.2.4 Scuff marks to the sides of the
plicable to textiles made from all fibers in specimen indicate the loops to the wire
5.1 Crockmeter (see 13.3, 13.4 and
the form of yarn or fabric whether dyed, clips are positioned downwards and are
Fig. 1).
printed or otherwise colored. It is not rec- not high enough to prevent rubbing the
5.2 Crockmeter Test Cloth, cut in 50
ommended for use for carpets or for specimen surface.
mm squares (see 13.5).
prints where the singling out of areas may 5.3 AATCC Chromatic Transference 6.2.5 A streak in the center of the crock
be too small using this method (see 13.2 Scale (see 13.6). cloth image and in the direction of rub-
and 13.3). 5.4 Gray Scale for Staining (see 13.6). bing may mean the top of the metal base
1.2 Test procedures employing white is warped and not flat. This will require a
5.5 White AATCC Textile Blotting
test cloth squares, both dry and wet with brace insert to square up the tester base.
Paper (see 13.6).
water, are given. 5.6 Specimen Holder for crockmeter 6.2.6 If specimen holders are used,
1.3 As washing, drycleaning, shrink- (see 13.4). place the holder over the specimen on the
age, ironing, finishing, etc., may affect 5.7 In-house poor crocking cloth. tester base. Move the crocking finger on
the degree of color transfer from a mate- 5.8 Crockmeter Verification Cloth. the crocking arm to the most forward po-
rial, the test may be made before, after, or This item may be used in lieu of an sition and observe whether it hits the in-
before and after any such treatment. in-house poor crocking cloth when such side edge of the holder. If this occurs,
poor in-house crocking cloth is not avail- move the holder slightly forward for all
able. tests. Without correction, this problem
2. Principle will cause a dark area on one side of the
2.1 A colored test specimen is rubbed crocking image.
6. Verification 6.2.7 Confirm the wet pick-up tech-
with white crock test cloth under con-
trolled conditions. 6.1 Verification checks on the opera- niques (see 9.2).
2.2 Color transferred to the white test tion of the test and the apparatus should 6.2.8 Replace the abrasive paper on the
cloth is assessed by a comparison with be made routinely and the results kept in tester base if it is smooth to the touch in
the Gray Scale for Staining or the Chro- a log. The following observations and the crocking area compared to the adja-
matic Transference Scale and a grade is corrective actions are extremely impor- cent area, or if slippage of the specimen
assigned. is noticed.
6.2.9 In routine testing, observe if mul-
3. Terminology tiple streaks are on the crocking image.
Position specimen normally with the long
3.1 colorfastness, n.—the resistance of dimension oblique to the warp and fill-
a material to change in any of its color ing. If the direction of rubbing falls along
characteristics, to transfer of its color- a twill line or surface pattern, etc., then
ant(s) to adjacent materials, or both, as a streaks may occur. If they do occur,
result of the exposure of the material to slightly adjust the angle for testing.
any environment that might be encoun-
tered during the processing, testing, stor- 7. Test Specimens
age or use of the material.
3.2 crocking, n.—a transfer of color- 7.1 Two specimens are used, one each
ant from the surface of a colored yarn or for the dry and the wet tests.
fabric to another surface or to an adjacent 7.1.1 Additional specimens may be
area of the same fabric principally by used to increase the precision of the aver-
rubbing. age (see 12.1).
7.2 Cut specimens at least 50 × 130 mm
4. Safety Precautions (2.0 × 5.1 in.) and position for testing pref-
erably with the long dimension oblique to
NOTE: These safety precautions are Fig. 1—Crockmeter. warp and filling or wales and courses.

AATCC Technical Manual/2012 TM 8-2007 21


Copyright © 2012 American Association of Textile Chemists and Colorists
7.2.1 Larger or full width lab samples matic pipetter, draw up water in mL to 11. Report
may be used without cutting individual 0.65 times weight of crocking square. If
specimens, when multiple tests are crocking square weight equals 0.24 gm, 11.1 State whether dry or wet crocking
needed and when using for production the mL used would be 0.24 × 0.65 = 0.16 test.
testing. mL. Lay crocking square on white plastic 11.2 Report the grade determined in 10.3.
7.3 Yarns. Knit a piece of fabric at least mesh over a dish. Apply water evenly 11.3 Report the grade determined in
50 × 130 mm, or wind yarn tightly on a over crocking square and weigh the wet 10.4 to the nearest 0.1 grade.
suitable form at least 50 × 130 mm with square. Calculate wet pickup according 11.4 State whether Gray Scale for
the yarn running in the long direction; or to instructions in this method and Method Staining (EP2), Chromatic Transference
otherwise stretched (see 13.8). 116, Colorfastness to Crocking: Rotary Scale (EP8) or Instrumental Assessment
Vertical Crockmeter Method. If needed, of Degree of Staining (EP12) was used
8. Conditioning adjust the amount of water used to wet for evaluating staining (see 13.6 and
the square and using a new crocking 13.9).
8.1 Prior to testing, precondition and square, repeat steps. When 65 ± 5% wet 11.5 If any pretreatment or aftertreat-
condition the test specimens and the ment was given to any specimens (see
pickup is achieved, record the amount of
crock squares for crock testing as di- 1.3) indicate method of treatment.
water used. Draw up the recorded amount
rected in ASTM D 1776, Conditioning
Textiles for Testing. Condition each spec- of water into the syringe tube, graduated
imen for at least 4 h in an atmosphere of pipette or automatic pipetter for each wet 12. Precision and Bias (see 13.15)
21 ± 1°C (70 ± 2°F) and 65 ± 2% RH by crocking performed during the current
day. Repeat this process each day. 12.1 Precision. An interlaboratory test
laying each test specimen or crock square was conducted in 1986 to establish the
separately on a screen or perforated shelf 9.2.3 Avoid evaporative reduction of precision of the test method. Testing was
of conditioning rack. the moisture content below the specified conducted under the normal atmospheric
level before the actual crock test is run. conditions of each laboratory and not
9. Procedures 9.2.4 Continue as directed in 9.1. necessarily under ASTM standard condi-
9.2.5 Air dry the white test square, then tions. Two operators at each of 12 labora-
9.1 Dry Crocking Test. tories evaluated 5 fabrics in 3 replications
9.1.1 Place a test specimen on the base condition (see 8.1) before evaluating. In
the case of napped, brushed or sanded by both dry and wet test method. Each of
of the crockmeter resting flat on the abra- 3 raters independently rated the stained
sive cloth with its long dimension in the material when loose fiber might interfere
with the rating, remove the extraneous crock squares using both the Gray Scale
direction of rubbing (see 13.7). for Staining and the Chromatic Transfer-
9.1.2 Place specimen holder over speci- fibrous material by pressing lightly on the
crock circle with the sticky side of cello- ence Scale. The original data is on file at
men as an added means to prevent the AATCC Technical Center.
slippage. phane tape before evaluating.
12.1.1 The components of variance as
9.1.3 Mount a white test cloth square,
standard deviations of the Gray Scale for
the weave parallel with the direction of
10. Evaluation Staining or Chromatic Transference Scale
rubbing, over the end of the finger which
rating units are given in Table I.
projects downward from the weighted
sliding arm. Use the special spiral wire 10.1 Rate the amount of color trans- 12.1.2 Critical differences are given in
clip to hold the test square in place. Posi- ferred from the specimen to the white test Table II.
tion the clip with loops upward. If the square under examination by means of the 12.1.3 Example for determining be-
loops point downward they can drag Chromatic Transference Scale or the Gray tween laboratory differences using one
against the test specimen. Scale for Staining (see 13.11 and 13.14). observer and the chromatic scale are
9.1.4 Lower the covered finger onto the 10.2 Back the test square with three given in Table III.
test specimen. Beginning with the finger layers of white test cloth while evaluating. Interpretation: For the dry crock test,
positioned at the front end, crank the since the difference between labs is less
10.3 Rate dry and wet crocking fast- than the critical differences in 12.1.2
meter handle 10 complete turns at the rate ness by means of the Gray Scale for
of one turn per second to slide the covered (0.82), the difference in results is not sig-
Staining (AATCC Evaluation Procedure nificant. For the wet crock test, since the
finger back and forth 20 times. Set and 2), or the AATCC 9-Step Chromatic
run the motorized tester for 10 complete difference between labs is greater than
Transference Scale (AATCC Evaluation the critical difference (1.53), the differ-
turns. Refer to individual specifications Procedure 8), or AATCC Evaluation Pro-
for any other required number of turns. ence in results is significant.
cedure 12, Instrumental Assessment of 12.2 Bias. The true value of colorfast-
9.1.5 Remove the white test cloth Degree of Staining, and record the nu-
square, condition (see 8.1) and evaluate ness to crocking can only be defined in
merical rating that corresponds to the ap- terms of a test method. Within this limita-
as directed in Section 10. In the case of propriate one on either of them.
napped, brushed or sanded material when tion, this test method has no known bias.
loose fiber might interfere with the rating, 10.4 Average individual results to the
remove the extraneous fibrous material nearest 0.1 grade when multiple speci- 13. Notes
by pressing lightly on the crock circle mens are tested or when a panel of evalu-
with the sticky side of cellophane tape ators rate color transfer. 13.1 For potential equipment information
before evaluating.
9.2 Wet Crocking Test.
9.2.1 Establish technique (see 13.10)
for preparing wet crock cloth squares by Table I—Components of Variance
weighing a conditioned square, then thor-
oughly wet out white testing square in Dry Wet
Test
distilled water. Prepare only one square at Scale Chromatic Gray Chromatic Gray
a time. Single Operator/Rater 0.20 0.20 0.24 0.25
9.2.2 Weigh dry crock square. Using a Within Laboratory 0.20 0.19 0.31 0.34
syringe tube, graduated pipette or auto- Between Laboratory 0.10 0.17 0.38 0.54

22 TM 8-2007 AATCC Technical Manual/2012


Copyright © 2012 American Association of Textile Chemists and Colorists
Table II—Critical Differences finger to dig into and push aside the yarns, or
slide off them and possibly give erroneous
For the components of variance in Table I, two averages of observed values should be considered results. This attachment is 25 mm in diameter
significantly different at the 95% probability level if the difference equals or exceeds the following critical by 51 mm long. Positioned on its side and held
differences. in place by the standard finger, it provides a
wider test area, and holds the white test square
Dry Wet by two spring loaded clips. For additional in-
Test No. of
Scale Observations Chromatic Gray Chromatic Gray formation on this development see the article
by C. R. Trommer, “Modification of the
Single Operator/Rater 1 0.55 0.54 0.68 0.70 AATCC Crockmeter for Yarn Testing,” Amer-
3 0.32 0.31 0.39 0.40 ican Dyestuff Reporter, Vol. 45, No. 12, p357,
5 0.24 0.24 0.30 0.31 June 4, 1956; also see articles by S. Korpanty
Within Laboratory 1 0.77 0.75 1.08 1.17 and C. R. Trommer, “An Improved Crock-
3 0.60 0.61 0.93 1.02 meter for Yarn Testing,” American Dyestuff
5 0.60 0.57 0.90 1.00 Reporter, Vol. 48, No. 6, p40, March 23, 1959.
Between Laboratory 1 0.82 0.89 1.53 1.90 13.9 It has been noted that different grades
3 0.69 0.77 1.43 1.81 may result depending upon whether the
5 0.66 0.74 1.41 1.79 Gray Scale for Staining or Chromatic Trans-
ference Scale is used for the evaluation. It is,
The critical differences were calculated using t = 1.96 which is based on infinite degrees of freedom. therefore, important to report which scale was
used.
13.10 Experienced operators do not have to
repeat this weighing procedure during a test
session once the technique is established.
Fiber 100% 10.3-16.8 mm combed
Table III—Crock Test Results cotton staple, desized, 13.11 For very critical evaluations and in
bleached, with no optical cases of arbitration, grades must be based on
Dry Wet brightener or finishing mate- the Gray Scale for Staining.
Lab A 4.5 3.5 rial present 13.12 For a discussion of crock testing, see
Lab B 4.0 1.5 Yarn 15 tex (40/1 cotton count), the article by J. Patton, “Crock Test Problems
Difference 0.5 2.0 5.9 turns/cm “z” can be Prevented,” Textile Chemist and Color-
Thread count 32 ± 5 warp ends/cm: 33 ± 5 ist, Vol. 21, No. 3, p13, March 1989; and “Test-
picks filling/cm ing for Crocking: Some Problems and Pitfalls”
Weave 1/1 plain by Allan E. Gore, Textile Chemists and Color-
pH 7 ± 0.5 ists, Vol. 21, No. 3, p17, March 1989.
pertaining to this test method, please visit
Mass/sq meter 100 ± 3 g finished 13.13 For prints where the singling out of
the online AATCC Buyer’s Guide at http://
Whiteness W = 78 ± 3 (Method 110) areas too small to test with the standard crock-
www.aatcc.org/bg. AATCC provides the pos-
meter is necessary (see AATCC Method 116,
sibility of listing equipment and materials sold 13.5.1 CAUTION: ISO crock cloth results Rotary Vertical Crockmeter Method). Speci-
by its Corporate members, but AATCC does may not be equivalent to AATCC crock cloth mens tested by both test methods may show
not qualify, or in any way approve, endorse or results/values based on crock cloth study. dissimilar results. There is no known correla-
certify that any of the listed equipment or 13.6 The Chromatic Transference Scale, tion between the two methods.
materials meets the requirements in its test Gray Scales for Staining and White AATCC
methods. 13.14 An automated electronic grading sys-
Textile Blotting Paper are available from tem may be used as long as the system has
13.2 For carpets, AATCC Method 165, Col- AATCC, P.O. Box 12215, Research Triangle
orfastness to Crocking: Carpets—Crockmeter been demonstrated to provide results that are
Park NC 27709; tel: 919/549-8141; fax: 919/ equal to and provide equal or better repeatabil-
Method, under the jurisdiction of Committee 549-8933; e-mail: orders@aatcc.org; web site:
RA57, Floor Covering Test Methods, should ity and reproducibility than an experienced
www.aatcc.org. grader performing visual evaluation.
be used. 13.7 Accidental damage to the rubbing fin-
13.3 The crockmeter provides a reciprocat- ger, spiral clip or abrasive paper should be 13.15 The precision of this test method is
ing rubbing motion simulating the action of a repaired as follows: neatly renew the abrasive dependent on the combined variability of the
human finger and forearm. paper; bend the clip further open or shut material being tested, the test method itself,
13.4 The crockmeter is so designed that the around a rod slightly smaller in diameter than and the evaluation procedure utilized.
16 ± 0.3 mm (0.625 ± 0.01 in.) diameter finger the crock peg; resurface the finger by move- 13.15.1 The precision statement in Section
moves back and forth, with each complete ment on an extra piece of fine emery cloth in a 12 was developed from results obtained by vi-
turn of the crank, in a straight line along a 104 manner simulating regular use. sual evaluation (EP 2 and EP 8).
± 3 mm track on the specimen, with a down- 13.8 For more convenient crock testing of 13.15.2 It is expected that the use of instru-
ward force of 9 N ± 10% (2 lb ± 10%). multiple strands of yarn or thread a dowel at- mental evaluation procedures (EP 12) will re-
13.5 Crockmeter Test Cloth should meet tachment is useful. This attachment was de- sult in greater precision than that obtained
the following specifications: veloped to avoid the tendency of the standard from visual evaluations.

AATCC Technical Manual/2012 TM 8-2007 23


Copyright © 2012 American Association of Textile Chemists and Colorists

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