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BASICS:
This test is performed to determine the percentage of different grain sizes contained within a
soil. The mechanical or sieve analysis is performed to determine the distribution of the
coarser, larger-sized particles, and the hydrometer method is used to determine the distribution
of the finer particles .
Standard reference :
Commonly based on grain size and soil consistency. Several classification systems exist:
1. Unified Soil Classification System (USCS) (ASTM D2487-11).
4.75 to
Sand S 2 to 0.075 2 to 0.05 2 to 0.06
0.075
0.075
Clay C < 0.002 < 0.002 < 0.002
1.SPECIFIC GRAVITY OF SOIL SOLIDS
15 131.72
36 131.31
Bath
Hot
30 131.44
Mass o f w ater & p ycn o u m eter (g m )
Mass of Water & Pycnoumeter
131.73
131.65
131.57
131.49
131.41
131.33
131.25
13.0 18.0 23.0 28.0 33.0 38.0
Temperature (C)
Figure1.2calibration curve mass of volumetric filled with water over a range of temperatures.
From (Fig 1.2)at 26o C MPw,C = 131.54 g
𝑀𝑠
𝐺𝑆 =
𝑀𝑃𝑤 ,𝐶 − (𝑀𝑃𝑤𝑠,𝐶 − 𝑀𝑠 )
𝐺𝑆@20° = 𝐺𝑆 × 𝐾
Opening Opening
Sieve No. Notes
(mm) (in)
3/4 in 19 0.75 Gravel
#4 4.75 0.187
2.3. Significance:
The distribution of different grain sizes affects on engineering properties of soil. Grain size
analysis provides the grain size distribution, and it is required in classifying the soil.
2.4. Equipment:
Balance, Set of sieves, Cleaning brush, Sieve shaker.
2.5.Test Procedure:
1. Obtain the mass of soil retained on each sieve and record this mass as the weight
retained on the data sheet. The sum of these retained masses should be
approximately equals the initial mass of the soil sample. A loss of more than two
percent is unsatisfactory.
2. Calculate the percent retained on each sieve by dividing the weight retained on
each sieve by the original sample mass.
3. Calculate the percent passing by starting with 100 percent and subtracting the
percent retained on each sieve as a cumulative procedure.
For example: Total mass = 60.5 g
Mass retained on No. 16 sieve = 1 g
Mass retained on No. 30 sieve = 10.2 g
For the No.16 sieve
The percent retained is calculated as;
% retained = Mass retained/Total mass
= (1/60.5) X 100 = 1.65 %
From this, the % passing = 100 - 1.9 = 9 8.35 %
For the No. 30 sieve:
% Retained = (10.2/60.5) X 100 = 16.86 %
% Passing = 96.75 - 16.86 = 79.89%
4. Make a semi logarithmic plot of grain size vs. percent finer.
5. Compute Cc and Cu for the soil.
Key Particle Sizes (D = Diameter)
D60 = Diameter corresponding to 60% finer in the grain size distribution.
6. D30 = Diameter corresponding to 30% finer in the grain size distribution.
D10 = Diameter corresponding to 10% finer in the grain size distribution. Also
known as Effective Size.
Key Coefficients (C):
Cu = Coefficient of Uniformity (ASTM D2487)
= D60/D10 =3.15
Cc = Coefficient of Gradation
= Coefficient of Curvature (ASTM D2487)
= (D30)2/(D60xD10) =1.01
Opening
Sieve No (mm) Retained (gm) Retained (%) Passing (%)
No.4 4.75 0 0 100
No.8 2.36 0 0 100
No.10 2 0 0 100
No.16 1.18 1 1.6 98.35
No.18 1 1 1.6 96.75
No.30 0.6 10.2 16.86 79.89
No.50 0.355 6.1 10.08 69.81
No.100 0.15 24.1 39.83 29.9
No.200 0.075 18.1 29.9 0
Pan
Total wt 60.5 gm
Sand Gravel
Silt & Clay
Fine Medium Coarse
#200 #40 #10 #4
110
100
90
80
70
Passing (%)
60 D60 = 0.3
50
D30 = 0.17
40
D10 = 0.095
30
20
10
0
0.001 0.01 0.1 1 10
Seive NO.
2.7.Some errors and problems:
1. After weighing the remaining on each sieve, after weight was collected there was
a total weight loss from the original weight This is due to the survival of parts
stuck in the sieves that caused this loss.
2. We must weigh all the sieves before work and it is empty and then weighed after
working with the soil remaining on it and from the difference in weight we find
the weight of the soil remaining to reduce the percentage of error
3. LIQUID AND PLASTIC LIMIT TESTING
ASTM D4318: Standard Test Methods for Liquid Limit, Plastic Limit, and Plasticity
Index of Soils.
3.3. EQUIPMENT
The following equipment and materials required for plastic limit testing:
Fine-grained soil.
#40 sieve (0.425-mm opening).
Distilled water.
Balance to the nearest 0.01 g.
Glass to soil mixing.
Soil drying oven set at 110o ± 5 o C.
Soil moisture container.
3.4. PROCEDURE
The liquid limit is defined as the water content at which the soil starts to act as a
liquid. To derive liquid limit, the following procedure, described as the Multipoint
Method (Method A) in ASTM D4318, is described:
1) Pass the soil through a #40 sieve and use the fraction that passes the sieve.
2) Add distilled water to approximately 50 g of soil until it has the consistency of
peanut butter or frosting.
3) Check that the drop height of the cup in the liquid limit device is 1.0 cm (Fig.
3.1), and adjust the apparatus as necessary. Most grooving tools have a tab with a
dimension of exactly 1.0 cm that you can use.
Fig. 3.1
4) Spread a flat layer of soil in the cup with the frosting knife (Fig. 3.2).
Fig. 3.2
5) Use the grooving tool to cut a groove in the soil (Fig. 3.3).
Fig. 3.3
6) Turn the crank on the liquid limit device at a rate of 2 cranks per second and
closely observe the groove. For each crank, the cup will drop from a height of 1.0
cm. Count and record the number of cranks that are required to close the groove
over a length of 0.5 in (13 mm) (Fig. 3.4). Most grooving tools have a dimension
of 0.5 in. that you can use.
Fig. 3.4
7) Clean out the cup and repeat steps 4-6 until successive trials yield consistent
results that are within a few cranks of each other, and record the average number of
cranks for the soil.
8) Remove the soil from the cup, place it in a moisture container, and obtain its
water content using the ASTM D2216 method.
9) the procedure is repeated at three different water contents, and the data are
plotted on a semi-log graph of w versus number of cranks. The water content
corresponding to 25 cranks (i.e. LL) .
3.4.2. ONE-POINT LIQUID LIMIT—METHOD B
LL n
=KW
5) the liquid limit is the average of the two trial liquid limit values.
Table 2.1
3.4.3. Plastic Limit Test
The plastic limit is defined as the water content at which a 0.125-in. diameter rod
of soil begins to crumble. It is measured using the following procedure:
1) Pass some soil through the #40 sieve and use the soil that passes the sieve.
2) Take a pea-sized mud ball and roll it out onto the frosted plate to form a rod
with a diameter of 1/8 in (3.2 mm ). Use the 1/8-in. diameter metal rod as a
reference (Fig.2.5). If the soil crumbles the first time, add more water and repeat.
3) If the rod doesn’t crumble, pick it up and make another mud ball in your hands .
As you do this, you will dry the soil.
4) Repeat the process of making a rod, rolling up in your hands with a ball, making
a rod, etc., until the soil crumbles while you are making the rod (Fig. 3.5). At this
point, the water content of the soil is the PL. Quickly obtain its moist weight and
place it in the oven for a moisture content reading in accordance with ASTM D
2216.
Repeat this entire procedure three times, and report an average value for the plastic
limit.
Fig.3.5
3-5 MEASUREMENTS AND CALCULATIONS
LL Expon. (LL)
40
Water content [%]
30
20
10
0
5 50
Nr. of Blows
𝑀1 − 𝑀2
𝑃𝐿 = × 100
𝑀2 − 𝑀𝑐
𝑀1 − 𝑀2
𝐿𝐿 = × 100
𝑀2 − 𝑀𝑐
𝑃𝐼 = 𝐿𝐿 − 𝑃𝐿
𝑁 tan 𝛽 𝑛
28 0.121
𝑛
𝐿𝐿 = 𝑤 ( ) = 36.7( ) = 37.2%,
25 25
27 0.092
𝑜𝑟 = 40.22 ( ) = 37.08%
25
𝐿𝐿𝑛 = 𝑘. 𝑤 𝑛 = 1.009 × 40.22 = 37.21%
4. Cone penetrometer method
4.2PURPOSE OF MEASUREMENT
This method covers the determination of the liquid limit of a sample of soil in its
natural state, or of a sample of soil from which material retained on a 425 μm test
sieve has been removed.
4.4Procedure
1)Take a sample of about 300 g from the soil paste prepared and place it on the
glass plate.
2)Mix the paste for at least 10 min using the two palette knives. If necessary add
more distilled water so that the first cone penetration reading is about 15 mm.
3)Push a portion of the mixed soil into the cup with a palette knife taking care not
to trap air. Strike off excess soil with the straightedge to give a smooth level
surface.
4)With the penetration cone locked in the raised position lower the supporting
assembly so that the tip of the cone just touches the surface of the soil. When the
cone is in the correct position a slight movement of the cup will just mark the soil
surface. Lower the stem of the dial gauge to contact the cone shaft and record the
reading of the dial gauge to the nearest 0.1 mm.
5)Release the cone for a period of 5 ± 1 s. If the apparatus is not fitted with an
automatic release and locking device take care not to jerk the apparatus during this
operation. After locking the cone in position lower the stem of the dial gauge to
contact the cone shaft and record the reading of the dial gauge to the nearest 0.1
mm. Record the difference between the beginning and end of the drop as the cone
penetration.
6)Lift out the cone and clean it carefully to avoid scratching.
7)Add a little more wet soil to the cup, taking care not to trap air, make the surface
smooth as in 3 and repeat 4 to 6.
8)If the difference between the first and second penetration readings is not more
than 0.5 mm record the average of the two penetrations and proceed to 9. If the
second penetration is more than 0.5 mm and less than 1 mm different from the
first, carry out a third test. If the overall range is then not more than 1 mm record
the average of the three penetrations and proceed to 9. If the overall range is more
than 1 mm remove the soil from the cup, remix and repeat 3 to 8 until consistent
results are obtained and then proceed to 9.
9)Take a moisture content sample of about 10 g from the area penetrated by the
cone and determine the moisture content.
10)Repeat 3 to 9 at least three more times using the same sample of soil to which
further increments of distilled water have been added. Proceed from the drier to the
wetter condition of the soil. The amount of water added shall be such that a range
of penetration values of approximately 15 mm to 25 mm is covered by the four or
more test runs and is evenly distributed. Each time soil is removed from the cup for
the addition of water, wash and dry the cup.
11)If at any time during the above procedure the soil has to be left for a while on
the glass plate cover the soil with the evaporating dish or a damp cloth to prevent
the soil drying out.
Fig.4.1 — Details of cone for liquid limit test
60
50
40
W % 30
Series1
20
10
0
0 5 10 15 20 25
cone penetration in mm
L.L in cone penetration in 20 mm = 37.9 %
5. Hydrometer Analysis (ASTM D422)
5.2. Equipment :
5.3.Procedure:
1) Combine approximately 50.0 g (Md) of the soil that passed the #200 sieve
after dried in oven with 125 ml of the sodium hexametaphospahte solution in a
250-ml glass beaker. Allow the mixture to soak for at least 16 hours in accordance
with ASTM D422 procedures
2) Transfer all of the mixture to an ASTM D422-specified dispersion cup
(Fig. 5.1). Use a squeeze bottle of distilled water to wash all of the soil solids from
the inside of the beaker into the dispersion cup. After transfer, the dispersion cup
should be more than half full of mixture.
Fig. 5.1
Fig. 5.2
4) Pour the slurry into a 1000-ml etched cylinder and fill with distilled water to just
below the etch mark. Use a squeeze bottle of distilled water to wash all of the
slurry from the cup into the cylinder.
5)Mix the cylinder by turning it upside down and back at a rate of 1 turn per
second for 1 minute.
6) Set the cylinder down and start the timer immediately. Using the squeeze bottle,
wash the remaining soil off the stopper and lip of the cylinder down into the
cylinder, and fill the cylinder to the etch mark with distilled water.
7) Take your first hydrometer reading at 1,2 minutes, with subsequent readings at
4,8, 16, 30, 60, and 1440 minutes. The hydrometer reading, R, is read off the neck
of the hydrometer at the top of the meniscus (Fig. 5.3). Record the time, t, in
minutes.
Fig. 5.3
8) Remove the hydrometer after each reading, and place it in a 1000-ml cylinder
filled with distilled water between readings. Spin the hydrometer while it is in this
cylinder to remove adhered soil particles .
9) Record the water temperature in the cylinder containing the soil slurry and
estimate Gs. If distilled water at room temperature is used for the test, and the
room is kept at a constant temperature, a single water temperature reading should
suffice.
10) At a given time t, particles larger than D have settled past the center of mass of
the hydrometer and no longer affect its buoyancy. Use Stoke’s Law to calculate the
particle diameter, D, in mm, corresponding to t in minutes:
𝐷 = 𝐾√𝐿/𝑡
In Eqn. above, K is a function of temperature and Gs, which both affect the density
of the slurry (Table 4-1). The parameter L represents the distance between the
center of mass of the hydrometer and the point where the hydrometer is read (Fig.
5.4), and is expressed in cm as a function of R (Table 4.2).
Fig. 5.4
Table 4-1
Table 4.2
As shown in (Fig. 5.5), the hydrometer floats high in the slurry at the start of the
test, but sinks with the passage of time as soil solids settle and the density of the
slurry decreases. The total change in R during the test is a function of Gs, water
temperature, and the soil concentration.
11) For each measurement, use the following equation to calculate the percent
passing, corresponding to D:
(𝑅 − 𝑏)𝑎
%𝑓𝑖𝑛𝑒𝑟 = × 100%
𝑀𝑠
In this equation, Msis the oven dried mass of the soil in the slurry (approximately
50.0 g). Since the hydrometer is calibrated for Gs= 2.65, the correction factor
is used to account for deviations in Gs from 2.65. The “composite” correction
factor b is used to account for the effects of) sodium hexametaphosphate on slurry
density) deviations from the hydrometer calibration temperature of 20oC, and)
reading from the top of the meniscus instead of the bottom. Values for a and bare
given Table 4.3.
Table 4.3
Temperature
o CT
C
16 -0.90
17 -0.70
18 -0.50
19 -0.30
20 0.00
21 +0.20
22 +0.40
23 +0.70
24 +1.00
25 +1.30
26 +1.65
27 +2.00
28 +2.50
29 +3.05
Fig. 5.5
12) Since the values for P’ from the hydrometer test were derived using the
fraction of the soil passing the #40 sieve, they must be multiplied by P-#40 for
plotting with the points derived by mechanical sieving.
5.4 MEASUREMENTS AND CALCULATIONS
152H
Corr. Corr.
Hydro.
Time Temp. Hydro. % Hydro. D
Reading L L/t K
(min) C Reading Finer only for (mm)
R
R meniscus R
1 24 48 44.2 87.25 49 8.3 8.3000 0.0128 0.0368
2 24 46 42.2 83.3 47 8.6 4.300 0.0128 0.0265
4 24 43 39.2 77.38 44 9.1 2.2750 0.0128 0.0193
8 24 41 37.2 73.43 42 9.4 1.1750 0.0128 0.0138
16 23 38 33.9 66.9 39 9.9 0.6187 0.0129 0.01014
30 23 36 31.9 62.97 37 10.2 0.3400 0.0129 0.00752
60 23 33 28.9 57.04 34 10.7 0.1783 0.0129 0.00544
120 23 31 26.9 53.1 32 11.1 0.0925 0.0129 0.00392
1440 23 15 10.9 21.51 16 13.7 0.0095 0.0129 0.00125
𝑅𝑐 = 𝑅𝑎 − 𝐶𝑧 + 𝐶𝑡
Where Ct from Table 4.3a
Cz assume = +4.8
𝑅𝑐 × 𝑎152𝐻
% Finer = × 100%
𝑀𝑠
𝐷 = 𝐾√𝐿/𝑡
100
90
80
Percent Passing (%)
70
60
50
40
30
20
10
0
0.001 0.01 0.1 1 10
𝐺𝑆 2.71
𝑎151𝐻 = = = 1.59
(𝐺𝑠 − 1) (2.71 − 1)
100000∗𝑎151𝐻
% Finer = 𝑀𝑠
× (𝑅𝑐 − 1 )……….. eq1 in ASTM D 422 – 63
L = L1 + 1 / 2 [L2 - VB/A] ……………eq5 in ASTM D 422 – 63
L = effective depth, cm,
L1 = distance along the stem of the hydrometer from the top of the bulb to
the mark for a hydrometer reading, cm,
L 2 = overall length of the hydrometer bulb, cm,
VB = volume of hydrometer bulb, cm 3, and
A = cross-sectional area of sedimentation cylinder, cm 2
Values used in calculating the values in Table 2 are as follows:
For both hydrometers, 151H and 152H:
L2 = 14.0 cm
VB = 67.0 cm 3
A = 27.8 cm 2
For hydrometer 151H:
L1 = 10.5 cm for a reading of 1.000
= 2.3 cm for a reading of 1.031
L1 =10.5 - n * 0.264516129032258 # n =( Rm – 1) *1000
𝐷 = 𝐾√𝐿/𝑡
140 GRAIN - SIZE DISTRIBUTION
120
Percent Passing (%)
100
80
60
40
20
0
0.001 0.01 0.1 1 10
60
A Line
Plasticity Index (PI)
50
CH
40
30
CL
20 MH
10 ML
CL-ML
0
0 10 20 30 40 50 60 70 80 90 100
Liquid Limit (LL or wL)
Fig 6.1
Fig 6.2
1. In Specific Gravity test seen it is equal to 2.71, it indicate this soil is clay
according to Table 7-1, however; the specific gravity of soil it range from
2.60 to 2.85 but when it exceed 2.85 that mean soil is mineral because the
mass of minerals is great than mass of natural soil and since specific gravity
is directly proportional to mass of soil as shown in eq.
𝑀𝑠
𝐺𝑠 =
𝑉𝑠 × 𝜌𝑤
When specific gravity is below 2.60 it mean organic soil because organic
material is dissolves in water that leading to decrease soil mass as well as
specific gravity.
The one – point methods are useful as a rapid procedures when only a
small amount of soil available, or when a lesser accuracy is acceptable.
Because it depend on slope of flow curve that it is different from soil to
anther like in ASTM tan β = 0.121 but in BS 1377 tan β = 0.092 for
Casagrande method. So the difference of values between this method and the
method Casagrande of attributing to the fact that this method is approximate
and not strictly the method of Casagrande.
4. ASTM D422 specifies a type 151H hydrometer, which measures the specific
gravity of the suspension, or a type 152H, which measures the density of
solids in the suspension.
From Grain Size Distribution curve H152 and Plastic Index got Activity
of clay which reference to clay mineral, if the activity between (0.75 – 1.25)
classified as normal when it below 0.75 became inactive and if above 1.25
became active.
𝑃𝐼 𝟐𝟏. 𝟎𝟓
𝐴= × 100 = = 𝟎. 𝟔𝟏𝟒𝟐%
(% of clay size fraction, by weight) 𝟑𝟓
That mean the soil in this report is active.
5. In classification of soil there are mean difference between AASHTO and
USCS from MIT and USDA because the first two methods it take in
consideration Atterberg limit (LL, PI) with percent of passing, on other hand
MIT & USDA it depend on percent of passing only.
The difference between AASHTO and USCS methods seen in treatment of
course – grained soils as shown in (Table 7-2&7-3), and for fine – grained
soils the major difference is shown in Fig. 7.3 were line A & U on chart LL-
PI for AASHTO, Also use PI = 10 as a dividing line between silty and
clayey soils seems rather arbitrary and probably does not relate to
engineering properties for fine – grain soils.
Table 7-2 USCS Definition for Gravel, Sand and Clay-Silt