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Suggestion of activities. The specific dates of submission will be revised from time to time.
Activities Week 1 2 3 4 5 6 7 8 9 10 11 12 13 14
1 Literature Review
Properties , us es a nd economi cs of product
Phys i ca l a nd chemi ca l properties
Al terna tives proces s routes
Sa fety a nd envi ronment i s s ues
3 Process Flowsheeting
Ma teri a l a nd energy ba l a nces
Proces s Si mul a tion
Proces s Fl ow Di a gra m
Mid-Semester Evaluation ●
4 Heat Integration
Pi nch a na l ys i s
PFD wi th hea t i ntegra tion
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Appendix II: Sample Title Page
DESIGN OF
METHANOL-ACETIC ACID PRODUCTION PLANT
GROUP 1
21
Appendix III: Sample certification of approval
CERTIFICATION OF APPROVAL
DESIGN OF
METHANOL-ACETIC ACID PRODUCTION PLANT
GROUP 1
APPROVED BY:
_______________________
AP DR. CHE MAD CHE RUSLI (Group Supervisor)
DATE:
22
Appendix IV: Assessment Form
23
Doc. Ref. No. Issue Version Date
UTP-ACA-PROG-PDP I-2 3.0 May 2017
Student ID.: (1)__________________ (2) __________________ (3) __________________ (4) ___________________ (5) ___________________ (6) __________________
TOTAL
Comments: __________________________________________________________________________________________________________________________________
………………………………………………
Supervisor’s signature
Name: _____________________________________________________ Date : ___________________________
24
Doc. Ref. No. Issue Version Date
UTP-ACA-PROG-PDP I-2 3.0 May 2017
awarded
Marks
Excellent
Average
Average
Failure
Below
Good
Criteria for Judging Quality
Category
TOTAL
25
Doc. Ref. No. Issue Version Date
UTP-ACA-PROG-PDP I-2 3.0 May 2017
Comments: _______________________________________________________________________________________
_________________________________________________________________________________________________
_________________________________________________________________________________________________
________________________________________________________________________________________________
…………………………….
Supervisor’s/External Examiner's signature
Name: ___________________________________ Date: _____________
26
Doc. Ref. No. Issue Version Date
UTP-ACA-PROG-PDP I-3 3.0 May 2017
(To be completed by supervisor/external examiner) Programme : Chemical Engineering Group No. : ________________
Student ID.: (1)__________________ (2) __________________ (3) __________________ (4) ___________________ (5) ___________________ (6) __________________
Comments: __________________________________________________________________________________________________________________________________
………………………………………………
27
Doc. Ref. No. Issue Version Date
UTP-ACA-PROG-PDP I-4 3.0 May 2017
Awarded
Marks
Excellent
Average
Average
Failure
Below
Category Criteria for Judging Quality
Good
Highlight all the important features of the
Executive report from the technical reasons of the
design to the conclusion.
summary & A to A- B+ to B C+ to C D+ to D F
Chapter 1: Inclusion of problem statement (4.0 - 5.0) (3.3 - 3.9) (2.5 - 3.2) (2.0 - 2.4) (0.0 - 1.9)
Introduction and objective of design project. Highlight
(5) on the scope of work to be carried out and
the plant specification.
Chapter 2: The latest information on feed
Literature A to A- B+ to B C+ to C D+ to D F
and product properties and price, possible (8.0 - 10.0) (6.5 - 7.9) (5.0 - 6.4) (4.0 - 4.9) (0.0 - 3.9)
Review (10) site locations, right way of cited references
Piping and
Instrumentatio Basic Control strategy
A to A- B+ to B C+ to C D+ to D F
n Design Piping and instrumentation diagram (8.0 - 10.0) (6.5 - 7.9) (5.0 - 6.4) (4.0 - 4.9) (0.0 - 3.9)
(10)
Safety and Reasonable selection of study nodes for
Loss HAZOP A to A- B+ to B C+ to C D+ to D F
Prevention Scaled plant layout in A3 size (4.0 - 5.0) (3.3 - 3.9) (2.5 - 3.2) (2.0 - 2.4) (0.0 - 1.9)
(5) Reasonable justification on safety aspects
Appropriate standards and symbols.
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Doc. Ref. No. Issue Version Date
UTP-ACA-PROG-PDP I-4 3.0 May 2017
Conclusion
and Relevancy to the objectives
Recommend Suggested future works on feasibility of A to A- B+ to B C+ to C D+ to D F
ation design (4.0 - 5.0) (3.3 - 3.9) (2.5 - 3.2) (2.0 - 2.4) (0.0 - 1.9)
(5)
References are quoted ethically and listed
References appropriately A to A- B+ to B C+ to C D+ to D F
(5) (4.0 - 5.0) (3.3 - 3.9) (2.5 - 3.2) (2.0 - 2.4) (0.0 - 1.9)
Total (100)
TOTAL
Comments: __________________________________________________________________________________________________
____________________________________________________________________________________________________________
………………………………………………..
Supervisor’s/Internal Examiner’s signature
Name : ___________________________________ Date : _____________
29
Doc. Ref. No. Issue Version Date
UTP-ACA-PROG-PDP I-5 3.0 May 2017
(9 - 10) (7 - 8) (2 - 3)
(4 - 6) (0 - 1)
Comment: _________________________________________________________________________________________________________
__________________________________________________________________________________________________________________
30
Doc. Ref. No. Issue Version Date
UTP-ACA-PROG-PDP I-6 3.0 May 2017
2.
3.
4.
5.
6.
31
Doc. Ref. No. Issue Version Date
UTP-ACA-PROG-PDP I-7 3.0 May 2017
2.
3.
4.
5.
6.
…………………………………………
Supervisor’s Signature
Name: Date: __________________
32
Appendix V : Description of Assessment
33
DESCRIPTION OF ASSESSMENT CRITERIA FOR PDP I – MID-SEMESTER EVALUATION (INDIVIDUAL)
Able to answer all the Able to answer most of the Able to answer some of Able to answer the Could not answer
Q&A question given correctly and question given correctly. the question given question given though any question given.
(Total marks: 40) accurately. Good conduct in handling correctly. the answer is not Do not try to answer
Convincing answer, showing Provide relevant examples the Q&A session. accurate. at all.
creativity and innovativeness to clarify the answers.
Ability to anticipate and answer Good conduct in handling
questions the Q&A session.
Ability to maintain good
(Marks: 32.0 – 40.0) (Marks: 26.0 – 31.9) (Marks: 20.0 – 25.9) (Marks: 16.0 – 19.9) (Marks: 0.0 – 15.9)
relationship with questioners
34
DESCRIPTION OF ASSESSMENT CRITERIA FOR PDP I – EVALUATION OF INTERIM ORAL PRESENTATION (Group)
(Marks: 8.0-10.0) (Marks: 6.5-7.9) (Marks: 5.0-6.4) (Marks: 4.0-4.9) (Marks: 0.0-3.9)
Conceptual Design (35) Propose two or more Propose two or more Propose only two process Propose only one process Propose only one process
Development of process route process route alternatives process routes. Show clear routes. Show justification for route. Provide justification route. No evaluation
alternatives. Selection of the best with clearly marked justification on the route route selected. on the route selected but conducted for selecting the
route configuration. differences. Show clear selected. not significant/relevant. final route.
justification and evaluation
Perform preliminary mass and/or on the route selected.
energy balance
Produce clearly-marked Produce clearly- marked Produce block diagrams with Produce block diagrams No block diagram or produce
Establish initial economic block diagrams with block diagrams with mass balance data or without mass balance block diagrams with
feasibility of the process route sufficient and relevant mass relevant mass balance information. data. insufficient or no mass
selected. balance calculation/data. calculation/data. balance data.
Provide latest raw material Provide raw material costs Provide raw material costs No provision of clear No provision of clear pricing
costs and selling price of and selling price of and selling price of products. pricing on raw materials for raw materials and
products. products. and products. products.
Provide good evaluation Provide good evaluation Provide acceptable Minimum information on Insufficient information on
between all the costs (annual between all the costs evaluation between all the all the costs (annual or per all the costs (annual or per
or per weight unit of (annual or per weight unit costs (annual or per weight weight unit of products) weight unit of products)
products) and the expected of products) and the unit of products) and the involved. Minimum involved. Insufficient
revenue from sales of the expected revenue from sales expected revenue from sales information on the expected information on the expected
products. of the products. of the products. revenue from sales of the revenue from sales of the
products. products.
(Marks: 28.0-35.0) (Marks: 22.8-27.9) (Marks: 17.5-22.7) (Marks: 14.0-17.4) (Marks: 0.0-13.9)
35
DESCRIPTION OF ASSESSMENT CRITERIA FOR PDP I – EVALUATION OF INTERIM ORAL PRESENTATION (Group)
36
DESCRIPTION OF ASSESSMENT CRITERIA FOR PDP I – EVALUATION OF INTERIM ORAL PRESENTATION (Group)
(Marks: 12.0-15.0) (Marks: 9.8-11.9) (Marks: 7.5-9.7) (Marks: 6.0-7.4) (Marks: 0.0-6.0)
37
DESCRIPTION OF ASSESSMENT CRITERIA FOR PDP I – EVALUATION OF INTERIM ORAL PRESENTATION (Group)
Safety and Loss Prevention Provide a report on a Provide a report on a Provide a report on an Provide a report on an Lack or provide wrong
(10) complete HAZOP analysis complete HAZOP analysis incomplete HAZOP incomplete HAZOP HAZOP analysis.
Hazard and operability Studies on THREE (3) nodes on THREE (3) nodes analysis on THREE (3) analysis on THREE (3) No worksheet or evidence
(HAZOP) connected to ONE (1) major connected to ONE (1) major nodes connected to ONE (1) nodes connected to ONE (1) on the implementation of
Plant layout equipment equipment with minor major equipment with minor major equipment with major HAZOP study.
Provide through HAZOP errors. errors. errors. Lack or provide wrong plant
worksheet that clearly shows Provide a HAZOP Provide an incomplete Provide an incomplete layout.
the study results with worksheet that clearly shows HAZOP worksheet that HAZOP worksheet that NO drawing or evidence on
technical accuracy the study results with some clearly shows the study clearly shows the study the design of plant layout.
Provide a complete and technical accuracy. results with minor technical results with major technical
scaled plant layout with Provide a scaled plant errors. errors.
arrangement with access layout with arrangement Provide a scaled plant layout Provide a scaled plant layout
routes and safety appliances. with access routes and safety with arrangement with access with arrangement without
Following Codes of Practice appliances, following Codes routes and safety appliances access routes and safety
and Industry Guidance. of Practice and Industry loosely following Codes of appliances loosely following
Provide reason able and Guidance. Practice and Industry Codes of Practice and
practical Provide reason able and Guidance. Industry Guidance.
justification/statement on practical Provide relevant Provide limited
the safety aspects of plant justification/statement on the justification/statement on justification/statement on
layout. safety aspects of plant layout. the safety aspects of plant the safety aspects of plant
layout. layout.
(Marks: 8.0-10.0) (Marks: 6.5-7.9) (Marks: 5.0-6.4) (Marks: 4-4.9) (Marks: 0.0-3.9)
Team Work (10) Completed the presentation Completed the presentation Exceed the time given to Exceed the time given to Did not complete the
within the time given. Show within the time given. Show complete the presentation (1- complete the presentation (3- presentation within the time
Ability to work with others in order high coordination of tasks good coordination of tasks 2 minutes). Show moderate 4 minutes). Show no given (more than 5
to provide best and smooth transition and good/smooth transition coordination of tasks and coordination of tasks and minutes). No clear division
performance/presentation. between members. between members. smooth transition between or coordination of tasks
irregular/unsmooth
members. transition between among members.
members.
Highly awareness Good awareness Members are aware and Low focus /attentiveness Members are not focus and
/attentiveness between /attentiveness between focus with other member’s between members. attentive towards other
members. members. tasks. members.
(Marks: 8-10) (Marks: 6.5-7.9) (Marks: 5.0-6.4) (Marks: 4.0-4.9) (Marks: 0.0-3.9)
38
DESCRIPTION OF ASSESSMENT CRITERIA FOR PDP I---INTERIM ORAL PRESENTATION (Individual)
39
DESCRIPTION OF ASSESSMENT CRITERIA FOR PDP I - INTERIM REPORT
Perform preliminary Perform preliminary Perform preliminary hazard Perform preliminary No preliminary
Safety (5) hazard and operability hazard and operability and operability study for hazard and operability hazard and
Chapter 3: Preliminary Hazards Analysis study around the entire study for all major plant some of the major plant study on the plant items but operability study
plant and develop the items and develop the items and develop develop wrong control No provision of possible
correct overall plant control correct control scheme the control scheme (with scheme hazards and loss
Consideration of: scheme Highlight important minimum error) Identify possible hazards prevention strategies or
- Previous similar accidents Highlight important possible hazards and Highlight possible hazards and provide general loss irrelevant hazards and
- Identification of chemical hazards and provision of possible hazards and and provide general loss prevention
MSDS in the appendix indicate relevant indicate relevant loss prevention prevention strategies strategies
- Loss prevention strategies to provide loss prevention strategies prevention strategies on strategies
anticipatory safety measures for the accidents the hazards identified
prevention on the hazards specified
- Inclusion of relevant local safety regulations Provide correct MSDS Provide correct MSDS Provide MSDS only for Provide correct MSDS only No provision of
and design guidelines for all chemical for the main raw the raw material and for the main raw material MSDS in the
involved in the materials, products product in the and product in the appendix appendix
appendix and by-products involved appendix Indicate safety Indicate safety
in the Indicate safety regulations for design regulations but non-
Describe two specific appendix consideration related with design
regulations for design
local government safety Describe at least one consideration consideration
regulations for design specific safety
consideration regulations for design
consideration
40
DESCRIPTION OF ASSESSMENT CRITERIA FOR PDP I - INTERIM REPORT
State clearly the selected reactor State clearly the selected State the type of reactor selected State the type of reactor selected No statement on the mode
Conceptual Design (25) type and the mode of operation reactor type and the mode of and the mode of operation Provide minimum evaluation on of reactor operation and
Chapter 4: Conceptual Design Analysis and types of phases present operation present present the type of reactor selected type of
Provide complete evaluation on Provide good evaluation and Provide justification on the type reactor
The technical and economic evaluations of the design which the type of reactor selected and justification on the type of of reactor selected No evaluation on the type
consider the options and alternatives and then elimination of those justify its advantage over the reactor selected of reactor selected
which are not feasible or not required. non-selected type
To include:
- Preliminary reactor optimization Propose two or more process Propose two or more process Propose two process routes Propose two process routes Propose only one process route.
- Process route screening route alternatives with clearly routes Show evaluation and No clear justification on the No evaluation conducted
- Process flow sheeting marked differences. Show good evaluation on the justification on the route selected route selected for selecting the final route
- Economics evaluation Show good evaluation on the process route selected and
process route selected and justify its advantage over the
justify its advantage over the non-selected route
non-selected route
Provide latest raw material costs Provide good evaluation between Provide the costs (annual or per Minimum information on all the Insufficient information on
and selling price of products. all the costs (annual or per weight unit of products) and the costs (annual or per weight unit of all the costs (annual or per
Provide good evaluation between weight unit of products) and the expected revenue from sales of products) involved weight
all the costs (annual or per weight expected revenue from sales of the products. Minimum information on the unit of products) involved.
unit of products) and the expected the products. expected revenue from sales of Insufficient information on
revenue from sales of the the products. the expected revenue from
products. sales of the products.
Process Flow Diagram (PFD)(25) Produce a clearly-marked block Produce a clearly- marked block Produce a block diagram with Produce block diagram with No block diagram or produce
diagram with sufficient and diagram with important mass balance data minimum mass balance data block diagrams with no
Chapter 5: Heat Integration relevant/important mass relevant/important mass mass balance data
balance calculation balance calculation
Specification of performance for each plant unit in terms of flow Provide clearly-marked PFD Provide clearly-marked PFD Provide PFD generated by Provide PFD generated by No provision of PFD. If PFD
rates, operating temperature etc. for efficient plant operation. generated by ICON on A1 generated by ICON on A1 ICON on A1 paper. software other than ICON. is available, the streams are
Consideration of appropriate energy conservation and/or paper. All streams are paper. All streams are numbered Streams are numbered and the Streams are insufficiently not properly numbered and
integration schemes to minimize the energy requirement for the numbered and the units are and the units are labelled. units are acceptably labelled. numbered and the process units units
plant. labelled. Provide a table showing for each Provide a table showing for each are unclearly labelled are not properly labelled
Inclusion of: Provide a table showing for each numbered stream: numbered stream (at least): Provide a table showing No provision of a table that
- Manual calculation of mass balance numbered stream: - Total flow rate - Total flow rate minimum data for (only few) provide relevant data for
- Energy optimization through pinch analysis - Total flow rate - Flow rate of each chemical - Temperature & Pressure streams each
- PFD before and after heat integration - Flow rate of each chemical species numbered stream
species - Temperature & Pressure
- Temperature & Pressure
Show the concise and correct Show the correct heat integration Show the heat integration Provide minimum information No information on
heat integration analysis analysis analysis (with minor error) on the implementation of heat the implementation
Provide two PFDs which clearly Provide good information with Provide minimum information integration of heat
show the differences by the comparison on the with minimum comparison on integration
implementation of heat implementation of heat the implementation of heat
integration (before and after the integration (before and after the integration (before and after the
implementation) implementation) implementation)
Instrumentation and Control Strategy (10) Provide reasonable and Provide reasonable and limited Provide relevant but not Provide general and limited Lack or provide wrong
scientific justification on the scientific justification on the scientific justification on the justification on the justification on the
Basic Control strategy development of development of development of instrumentation development of development of
Piping and instrumentation diagram instrumentation and control instrumentation and control and control system for the instrumentation and control instrumentation and control
system for the process system for the process process system for the process system for the process.
Clearly show technical Show limited technical Show limited technical Show very limited or Lack or show wrong
application of fundamental application of fundamental application of fundamental minimum technical technical application of
knowledge on control strategy knowledge on control strategy knowledge on control strategy application of fundamental fundamental knowledge.
with latest literature support with textbook support Provide a summary of control knowledge Do not provide a summary of
Provide a summary of control Provide a summary of control requirement, possible controlled Provide a summary of control control requirement, possible
requirement, possible requirement, possible and manipulated variables in requirement, possible controlled and manipulated
controlled and manipulated controlled and manipulated table form. controlled and manipulated variables in table form.
variables in table form. variables in table form. Provide a PID (drawn based on variables in table form. No drawing or evidence on
Provide a PID (drawn based Provide a PID (drawn based on PETRONAS technical Provide a PID that shows the the implementation of
on PETRONAS technical PETRONAS technical standard) that do not show the incomplete control system, control strategy
standard) that clearly shows standard) that clearly shows control system thoroughly with some technical errors and
the control system thoroughly the control system with some (incomplete) not according to PETRONAS
with technical accuracy. technical accuracy. technical standard.
41
DESCRIPTION OF ASSESSMENT CRITERIA FOR PDP I - INTERIM REPORT
Safety and loss prevention (5) Provide a report on a complete Provide a report on a complete Provide a report on an Provide a report on an Lack or provide wrong
HAZOP analysis on THREE (3) HAZOP analysis on THREE (3) incomplete HAZOP analysis incomplete HAZOP analysis HAZOP analysis.
Reasonable selection of study nodes for HAZOP nodes connected to ONE (1) nodes connected to ONE (1) major on THREE (3) nodes connected on THREE (3) nodes connected No worksheet or evidence on
Scaled plant layout in A3 size major equipment. equipment with minor errors. to ONE (1) major equipment to ONE (1) major equipment the implementation of
Reasonable justification on safety aspects Provide through HAZOP Provide a HAZOP worksheet that with minor errors. with major errors. HAZOP study.
Appropriate standards and symbols worksheet that clearly shows the clearly shows the study results with Provide an incomplete Provide an incomplete Lack or provide wrong plant
study results with technical some technical accuracy. HAZOP worksheet that clearly HAZOP worksheet that clearly layout.
accuracy. Provide a scaled plant layout with shows the study results with shows the study results with NO drawing or evidence on
Provide a complete and scaled arrangement with access routes and minor technical errors. major technical errors. the design of plant layout.
plant layout with arrangement safety appliances, following Codes Provide a scaled plant layout Provide a scaled plant layout
with access routes and safety of Practice and Industry with arrangement with access with arrangement without
appliances. Following Codes of Guidance. routes and safety appliances access routes and safety
Practice and Industry Guidance. Provide reason able and practical loosely following Codes of appliances loosely following
Provide reason able and practical justification/statement on the Practice and Industry Codes of Practice and
justification/statement on the safety aspects of plant layout. Guidance. Industry Guidance.
safety aspects of plant layout. Provide relevant Provide limited
justification/statement on the justification/statement on the
safety aspects of plant layout. safety aspects of plant layout.
Follows directly the formatting Follows the formatting style Follows an acceptable formatting Provide an acceptable No formatting at all
Others (5) style stated by the guidelines stated by the guidelines provided style though not fully formatting style but did not Difficult to read and to
provided The report is well structured and as per the guidelines provided follow as what have been stated understand the contents of
Proper presentation and format of report which ensure the: The report is very well provides good flow of The report is well structured with in the guidelines provided the reports
- Compliance to standard guideline structured and provides good information (with very minimum minimum disorganization The report is not structured with
- Neatness and consistency in formatting style flow of information disorganization) Easy to read and understand the obvious disorganization
- References are quoted and listed appropriately Very easy to read and to Easy to read and understand the contents of the reports with error Can be read to understand the
- Usage of proper English understand the contents of the contents of the reports with very in terms of spelling and reports contents. Too many
- Implementation of correct writing style/skill reports with very minimum minimum spelling and grammar. spelling and grammatical errors
spelling or grammatical error grammar error
42