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Separators Within
the Right Limits
iquid/vapor separators are one of stage, primary separation, uses an inlet
between 0.75U, and U/. Eq. .1 can be ucs have been c urve fitted and arc
rearran ged as Eq. 4. a Sanders-Brown given in Table I.
type equat ion ( / ): When calculating UT II' there is no mist eliminator. it is
recommended to use one half or the
for a horizontal above values (2) or the "th eoretical"
value K can be calculated from Eq. 5 if
separator, a "no mist the liquid droplet size is known. The
where drag coe ffi cient. C" has been curve fit-
eliminator K value" led and is given in Tab le I or can be
where K= / 4gl1, (5)
should be used. obtained from Figure 7-.1 in the GPSA
V 3 c; " Enginee ring Data Book" (2 ).
Before proceedin g. it is worthwhile
Practically. very small droplets can- qu utcly predi ctable so the K va lues to clarify some definitions and criteria .
not be se pa rat ed by gravity alone. 1'01' mist eliminators arc typi cally Holdup is defined as the time it takes
These droplet s are coalesced to form empirical. This is where subje cti vity to reduce the liquid level from normal
larger dr opl et s which will settle by first e nte rs separator design . Th er e (NLL ) to empty (LLL ) while maintain-
gravity. Coalescing dev ices in separa - are severa l literature sources of K val- ing a normal outlet now without feed
tors force the gas to follow a tortuous ue s s uc h as the Gas Proc ess or' s makeup . Surge time is defined as the
path a nd th e mo m e n t u m o f th e S up p lie r A ssociation ( G PS A) time it takes 1'0 1' the liquid level to rise
droplets ca uses them to co llide with " Enginee ring Data Book" (2). numer- fr om normal (N L L ) to m a ximum
o t he r dro pl et s o r th e co a le sc i ng o us technical publications and ven- ( H L L ) whil e maint ainin g a normal
de vice. form ing larger droplet s. The dor ' s recommendation s. Th e G PSA reed with out an y o utlet n ow . Some
coa lesced droplet diam eter is not udc- (2) and York Mist Eliminat or (3) val- g uidelines base "s urge" on the volume
between low (LU .) and high (H LL )
liquid levels. Holdup time is based on
Table 1. Separator K values. the reserve required to maintain good
control and safe operati on of down-
Mist Eliminator
stream facilities. Surge time is usually
1:-:; P£ 15 K =0.1821 + 0.0029P+ 0.0460Ln IPI
15:-:; P:-:;4O K= 0.35 p. psia
based on requirements to accumulate
40:-:; P:-:; 5.500 K =0.430 - 0.023Ln( PI liquid as a result o r upstream or down-
stream variations or upsets. 1'01' exam-
GPSA K=0.35-0.0001*(P-100) ple. slugs. In the absenc e o r specific
os P:;; 1.500 K = 0.35 - 0.0l(P- 100/1 001 p. psig requirements. surge time may be takcn
• Most vapors undervacuum K = 0.20. as one hall' or holdu p time.
• Forglycol andamine solutions. multiplyKby 0.6-0.8. ve rtir a! se parat ors. Fo r ve rtica l
• Forverticalvessels without misteliminators, divide Kby2.
separators . the vapor disen gagem ent
• Forcompressor suctionscrubbers, mole sieve scrubbers and expander inlet
separators multiply Kby 0.7---{).8.
area is the entire cross-sectional area of
the vessel so that vapor disen gagement
Theoretical tno misteliminator) diameter call be calculated trom Eq. 6:
K -- J 4g~
3C D
~
~
6'
-
distance 10 the liquid surface.
I, > HI'
( 9)
ll", - VI
If a mist c l i m i nat or pad is used, Ho
additional hei ght is added, as Ho D, This can be rearranged in terms of the
shown in Figure I . The calculations allowable horizontal velocity.
of diameter and hei ght arc detailed ( 10)
d"r-
~
in the "Desi gn Procedu re s" section U ,\ /1 :s; ,; I ' U I
of thi s article .
Hori ro nta! scpa ra tOI'S . For hori-
Hr Feed
Inlet -I ~N - '-----
The length , L divided by the height of
zo nta l two-pha se se pa ra to rs . the the va por di sen gagem ent a rea , H I"
cross-section is oc cup ied by both HUN would alw ays be g reate r than unit y.
vapor and liquid , as shown in Figure HLL The allo wable hor i zontal velocity is a
2. When si/.ing horizontal two-phase - -- very subje cti ve topic with several
Hs 1
separators . usually a diameter is empirical approaches to modify the
NLL
assumed, LLL is select ed or calculat- - -- vertical "K" value available in the lit-
ed. NLL is set by liquid holdup, and HH erature (2, 5, 7. 8). For horizontal sep-
HLL is set by liquid sur ge. Th e cross-
HUl
- -LLL- arator desi gn . the subsequent desi gn
sectional area bet ween HLL and the procedure s usc a "droplet set rl in g
top o f the ves se l is used for va por approach " similar to the API proce -
disengagement. Th e length of the dure ( ()) whi ch d o e s not require
vess el is then c a lculated to accom- Liquid empirical modificati on of the "K' val-
Outl et Nozz le
modate holdup and sur ge or to facili- ue for vert ical se ttlers. It should he
tate vapor liquid se paration. Hence, • Figure I. Vertical two-phase separator. noted that when calculating VI for a
this approach to sizing horizontal horizontal separator. a "no mist elimi-
separators, or var ia tio ns of it, arc required for vapor-liquid sepa ration is nator K value" should be used.
iterative calculati ons . much greater than the length required
The foll owin g wi ll de velop the for holdup and surge , for a g iven Design Procedures
basic equation used for calculating the diameter. Equation 8 is then a func- The foll owin g de sign procedures
size of a horizontal se parato r. For a tion o f the inside diameter. D. and and heuristics arc a result of a review
horizontal sepa rator c ross section. a length. L. o f I iicruturc so urc e s and accepted
" volume balan ce" is written. For horizontal separators. the I iq- industrial design guidelines. Th e hori-
uid droplet to be separated from the zonial desi gn pro cedure incorporates
gas has a horizontal drag force which optimizing the diameter and length by
is not directly opposite to gravity as in minimizing the weight of the shell and
Holdup and surge volumes are calcu- the verti cal case. Without detail ed heads. To add a degree of conser-
lated from holdup and surge times treatm ent of two-dimensional particle vatism to the de si gn , the volum e
which arc selected accordi ng to guide- mot ion , most literature sour ces rccog - available in the hea ds is ignored.
line s. The low liquid level are a is a nizc th at the all owable hori zontal Vertical d es ign p ro c edure (Sec
function of the low liquid level height . veloci ty ca n he higher than the lenni- Figure I):
obtained from guidelines, and the ves - nul ve loci ty ( 2, 5. 7). Thi s can be 1. Calculate th e ve rt ic a l termin al
sel inside di am et er . Th e minimum vapor velocity:
vapor disengagem ent area , AI/) ' is 11.1
typically specified as one to two ft or U I =K P I - P \' .ft Is (11)
20 Ck of the vessel inside diameter, If a mist eliminator pad (
P II )
whichever is g re a ter . The sizing
method in the " Desig n Procedures" is used, additional Set U , = O.75 V r for a conservati ve
sec tion of this article ass umes this for de sign. Calcula te the K va lue from
A 1'/) and o nly increases it if the length height is added. Table 1_
Nomenclature
T!~
v D S HLL
NLL
I ~ A H
~ All LLL
/ ~
Feed Inlet
fi-
· ~H!:.l _ - J~v - - =-~~. ~"-~
VaporDutlet
0<PS250
250 < Ps 500
IJD
1.5-3.0
3.0-4.0
• Fig ure 2.
E
Hor izontal two-phase
o
-,
_N.!-L
----1---------
LLl
Hl l
M~. ~2·~ _ _ ±surge
Holdup
separator.
500<P P>500 4.0-6.0
Table 9. Selection of
head types.
• Equation C.
1. 2:1 ellipticalheads aretypicallyused
(
when D < 15 hand P> 100 psig. l /i
2. Hemispherical heads aretypicallyused
when D> 15 ft regardless of P.
3. Dished heads with knuckle radius =0.6D
Bre typicallyused when D< 15 ft and
P< 100 psig.
D =
4(1 97.90+98.95)
• Equation D.
7[(0.6)(5.0)
l .
= 5.01 [tls,
.
usc 5.0./t
Notes:
P= design pressure _ VH+~' _ 197.90+98.95 ? . . ( .
0= drum diemeter
L - AI _ A - A ' L - 19.63 _ 7.34 _ 2.16' _9.3, say 29.5.1t
v U L
• Equation E.
(Calcul ati ons would h a vc to b e
repeated from the step 9 with reduced
H v)' Calculate VD . If VD > 6.0 then 2.0 Ii 690
¢ = 0.29 [tls =. s
increa se D and repe al ca lc ulatio ns
from the step 6 . If V D < 1.5, then
• Equation F.
decrea se J) and rep eat calc ulations
from the step 6.
15. Calc ulate the thickness of the 4. Calculat e the holdup volume:
shell and head s acco rding to Table 7. \/ " = (10 min .) (19.79 ft /min.) =
16. Calculate the surface area of the Size a horizontal 197.90 ft '
'
shell and heads accordin g to Ta ble 7. 5. Calculate the surge volume:
17. Calculate the approximate ves- separator with a mist \/\=(5 min.) ( 19.79 Inmin.) =98.95 ft-'
sel weight according to Table 7. 6. Assume VD = 5.0. Initially set
18. In cre a se a nd d ec re ase the eliminator pad. the diameter (Eq. D)
d iam et er by 6 in. inc re me nts and A , = rr/4 (S.O lW = 19.63 It'.
repeat the calc ulations until VD has separate the following mixture . The 7. Calculate low liquid height:
ranged from 1.5 to 6.0. operating pressure is 975 psig and the H,u = (0.5)(5.0) +7 = 9.5 in., usc lOin .
19. With the optimum vessel size holdup and surge are to he 10 min and 8. Calcul ate the low liqu id level
(minimum weight), calculate normal S min respecti vely. Usc a design tem- area:
and high liquid levels: perature of 650°F. Sec Table X. H,jD = D.1 67
I. Calcul ate the vapor volumetric Using Tabl e 6, A,,/AT = 0. 110
A\,[,[ = A u l . + \//L (29 ) flow rate (Eq. A). A IL! = (0. 110) ( 19.63 ft ~ ) = 2.16 IF
2. Calcul ate the liquid volumetric 9. Set H I' = 2 It, H /D = 2/5 =0.4
With A v ,,1A, obtain H \U from Tabl e 6 fl ow rate (Eq. B). From Tabl e 6, A/A, = 0.374
3. Cal cul ate the vert ical terminal A I' = (0.373)( 19.(3 ) = 7.34 IF
(30) velocity (Eq. C): K = 0.13 (GPSA val- 10. Calculat e the length to accom-
ue di vid ed by two since " no mist modate holdup /surge (Eq. E).
Example: Size a horizontal sepa- eliminator" value is used ) II. Calcu late the liqu id dropout
rater wi th a mist el iminator pad to V I' = O.75U, = 0.29 ft/s time (Eq. F).