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Design Two-Phase

Separators Within
the Right Limits
iquid/vapor separators are one of stage, primary separation, uses an inlet

L the most common types of process


equipment. Many technical papers
have been written on separator
design and vast amounts of information
are also available in corporate process
diverter so that the momentum of the liq-
uid entrained in the vapor causes the
largest droplets to impinge on the diverter
and then drop by gravity. The next stage,
secondary separation, is gravity separa-
engineering design guidelines. The basic tion of smaller droplets as the vapor flows
equations used for sizing are widely through the disengagement area. The final
known; however, subjectivity exists dur- stage is mist elimination where the small-
Here is a proven, ing the selection of the parameters used in
these equations. This article attempts to
est droplets are coalesced so that larger
droplets are formed which will separate
address the basics of two-phase separator by gravity.
step-by-step design and provide step-by-step proce- For secondary separation, the allow-
dures and examples for two-phase able velocity must be calculated so that
method. vapor/liquid separator design. disengagement area can be subsequently
determined. Performing a force balance
Two-phase separator types on the liquid droplet settling out provides
and selection the necessary relationship. When the net
Two-phase separators may be oriented gravity force, given by Eq. 1,
either vertically or horizontally. In some
cases, it may be necessary to compare
both designs to determine which is more
economic. Separators may be designed
with or without mist eliminator pads and balances the drag force, given by Eq. 2,
may also have inlet diverters. Some sepa-
rators may have proprietary impingement (2)
W.Y. Svrcek. w.o. Monnery or settling internals. The vendor should be
University of Calgary contacted to design these types of vessels.
Vertical vapor/liquid separators are pre- the heavier liquid droplets will settle at a
ferred for separating liquid from mixtures constant terminal velocity, U; Equating
with a high vapor/liquid ratio while hori- Eqs. 1 and 2 results in,
zontal separators are preferred for sepa-
rating vapor from mixtures with a low 4g 4 (p
L - P v) (3)
vapor/liquid ratio.
3CD p v
Background Hence, as long as U v < U T' the liquid
Vapor/liquid separation is usually droplets will settle out. Typically, the
accomplished in three stages. The first allowable vertical velocity, U v' is set

CHEMICAL ENGINEERING PROGRESS • OCTOBER 1993 • 53


FLUIDS/SOLIDS HANDLING

between 0.75U, and U/. Eq. .1 can be ucs have been c urve fitted and arc
rearran ged as Eq. 4. a Sanders-Brown given in Table I.
type equat ion ( / ): When calculating UT II' there is no mist eliminator. it is
recommended to use one half or the
for a horizontal above values (2) or the "th eoretical"
value K can be calculated from Eq. 5 if
separator, a "no mist the liquid droplet size is known. The
where drag coe ffi cient. C" has been curve fit-
eliminator K value" led and is given in Tab le I or can be
where K= / 4gl1, (5)
should be used. obtained from Figure 7-.1 in the GPSA
V 3 c; " Enginee ring Data Book" (2 ).
Before proceedin g. it is worthwhile
Practically. very small droplets can- qu utcly predi ctable so the K va lues to clarify some definitions and criteria .
not be se pa rat ed by gravity alone. 1'01' mist eliminators arc typi cally Holdup is defined as the time it takes
These droplet s are coalesced to form empirical. This is where subje cti vity to reduce the liquid level from normal
larger dr opl et s which will settle by first e nte rs separator design . Th er e (NLL ) to empty (LLL ) while maintain-
gravity. Coalescing dev ices in separa - are severa l literature sources of K val- ing a normal outlet now without feed
tors force the gas to follow a tortuous ue s s uc h as the Gas Proc ess or' s makeup . Surge time is defined as the
path a nd th e mo m e n t u m o f th e S up p lie r A ssociation ( G PS A) time it takes 1'0 1' the liquid level to rise
droplets ca uses them to co llide with " Enginee ring Data Book" (2). numer- fr om normal (N L L ) to m a ximum
o t he r dro pl et s o r th e co a le sc i ng o us technical publications and ven- ( H L L ) whil e maint ainin g a normal
de vice. form ing larger droplet s. The dor ' s recommendation s. Th e G PSA reed with out an y o utlet n ow . Some
coa lesced droplet diam eter is not udc- (2) and York Mist Eliminat or (3) val- g uidelines base "s urge" on the volume
between low (LU .) and high (H LL )
liquid levels. Holdup time is based on
Table 1. Separator K values. the reserve required to maintain good
control and safe operati on of down-
Mist Eliminator
stream facilities. Surge time is usually
1:-:; P£ 15 K =0.1821 + 0.0029P+ 0.0460Ln IPI
15:-:; P:-:;4O K= 0.35 p. psia
based on requirements to accumulate
40:-:; P:-:; 5.500 K =0.430 - 0.023Ln( PI liquid as a result o r upstream or down-
stream variations or upsets. 1'01' exam-
GPSA K=0.35-0.0001*(P-100) ple. slugs. In the absenc e o r specific
os P:;; 1.500 K = 0.35 - 0.0l(P- 100/1 001 p. psig requirements. surge time may be takcn
• Most vapors undervacuum K = 0.20. as one hall' or holdu p time.
• Forglycol andamine solutions. multiplyKby 0.6-0.8. ve rtir a! se parat ors. Fo r ve rtica l
• Forverticalvessels without misteliminators, divide Kby2.
separators . the vapor disen gagem ent
• Forcompressor suctionscrubbers, mole sieve scrubbers and expander inlet
separators multiply Kby 0.7---{).8.
area is the entire cross-sectional area of
the vessel so that vapor disen gagement
Theoretical tno misteliminator) diameter call be calculated trom Eq. 6:

K -- J 4g~
3C D

Co =exp(}1 Technicall y. this is the mist eliminator


Y= 8.411 - 2.243X + 0.273X! -1 .865E - 2)(3 + 5.201 E- 4~
diameter and the inside diameter or the
X= u{ 0.95 + 8Pvg<PL- Pv») vessel must be ,.. li ghtl y larger so that
the mist eliminator can be installed
inside the vessel. Typically. the calcu-
lated value is taken up to the next six
Notes: in. This value is taken as the required
0". ft dia meter of the vessel. D. and the cor-
p,lb/ft l
respondin g cross-sectiona l area. A . is
II. cP
1 micron = 3.28084 x 10-' ft
calculated using this diameter.
T he next step in sizin g a vertical
se parator is to determine the height.

54 • OCTOBER 1993. CHEMICAL ENGINEERING PROGRESS


For a two-phase vertical separator, the shown simply by equat ing the "resi-
total height can he broken into sec- With Vapor Without dence" times of the liquid droplet to
tions, as shown in Figure I. The sepa- Mist Eliminator Outlet Mist Elimi nator he settled. That is. the time it takes to
rator height is then calculated by
add ing the hei ghts of these sections.
/~ ,.-
travel the horizont al len gth between
inlet and outlet must be greater than
as per Eq. 7. 1'-0' the time it takes to settle the vertical

~
~

6'
-
distance 10 the liquid surface.
I, > HI'
( 9)
ll", - VI
If a mist c l i m i nat or pad is used, Ho
additional hei ght is added, as Ho D, This can be rearranged in terms of the
shown in Figure I . The calculations allowable horizontal velocity.
of diameter and hei ght arc detailed ( 10)
d"r-
~
in the "Desi gn Procedu re s" section U ,\ /1 :s; ,; I ' U I
of thi s article .
Hori ro nta! scpa ra tOI'S . For hori-
Hr Feed
Inlet -I ~N - '-----
The length , L divided by the height of
zo nta l two-pha se se pa ra to rs . the the va por di sen gagem ent a rea , H I"
cross-section is oc cup ied by both HUN would alw ays be g reate r than unit y.
vapor and liquid , as shown in Figure HLL The allo wable hor i zontal velocity is a
2. When si/.ing horizontal two-phase - -- very subje cti ve topic with several
Hs 1
separators . usually a diameter is empirical approaches to modify the
NLL
assumed, LLL is select ed or calculat- - -- vertical "K" value available in the lit-
ed. NLL is set by liquid holdup, and HH erature (2, 5, 7. 8). For horizontal sep-
HLL is set by liquid sur ge. Th e cross-
HUl
- -LLL- arator desi gn . the subsequent desi gn
sectional area bet ween HLL and the procedure s usc a "droplet set rl in g
top o f the ves se l is used for va por approach " similar to the API proce -
disengagement. Th e length of the dure ( ()) whi ch d o e s not require
vess el is then c a lculated to accom- Liquid empirical modificati on of the "K' val-
Outl et Nozz le
modate holdup and sur ge or to facili- ue for vert ical se ttlers. It should he
tate vapor liquid se paration. Hence, • Figure I. Vertical two-phase separator. noted that when calculating VI for a
this approach to sizing horizontal horizontal separator. a "no mist elimi-
separators, or var ia tio ns of it, arc required for vapor-liquid sepa ration is nator K value" should be used.
iterative calculati ons . much greater than the length required
The foll owin g wi ll de velop the for holdup and surge , for a g iven Design Procedures
basic equation used for calculating the diameter. Equation 8 is then a func- The foll owin g de sign procedures
size of a horizontal se parato r. For a tion o f the inside diameter. D. and and heuristics arc a result of a review
horizontal sepa rator c ross section. a length. L. o f I iicruturc so urc e s and accepted
" volume balan ce" is written. For horizontal separators. the I iq- industrial design guidelines. Th e hori-
uid droplet to be separated from the zonial desi gn pro cedure incorporates
gas has a horizontal drag force which optimizing the diameter and length by
is not directly opposite to gravity as in minimizing the weight of the shell and
Holdup and surge volumes are calcu- the verti cal case. Without detail ed heads. To add a degree of conser-
lated from holdup and surge times treatm ent of two-dimensional particle vatism to the de si gn , the volum e
which arc selected accordi ng to guide- mot ion , most literature sour ces rccog - available in the hea ds is ignored.
line s. The low liquid level are a is a nizc th at the all owable hori zontal Vertical d es ign p ro c edure (Sec
function of the low liquid level height . veloci ty ca n he higher than the lenni- Figure I):
obtained from guidelines, and the ves - nul ve loci ty ( 2, 5. 7). Thi s can be 1. Calculate th e ve rt ic a l termin al
sel inside di am et er . Th e minimum vapor velocity:
vapor disengagem ent area , AI/) ' is 11.1
typically specified as one to two ft or U I =K P I - P \' .ft Is (11)
20 Ck of the vessel inside diameter, If a mist eliminator pad (
P II )
whichever is g re a ter . The sizing
method in the " Desig n Procedures" is used, additional Set U , = O.75 V r for a conservati ve
sec tion of this article ass umes this for de sign. Calcula te the K va lue from
A 1'/) and o nly increases it if the length height is added. Table 1_

CHEMICAL ENGINEERING PROGRESS • OCTOBER 1993 • 55


FLUIDS/SOLIDS HANDLING

Nomenclature

A = vertical vesselcross-sect ional 2. Ca lcul a te t he v a por vo lu metri c 3. C alc u la te th e V e sse l ( i ns id e)


Area. fl2 fl ow rate: d ia me ter :
AUL = cross section For LLL (horizontal
vessel),fl1
j1(,
Qv = (3,600) /"'/ (1 2 ) ( 13)
AT = total cross sectional area (PI')' . I .I' D VI!
(horizontal vessel), fl '
A\'0 =vapor disengagement area
required, fl1
ell = drag coefficient
D = vesseldiameter, ft or in. Table 2. Liquid holdup and surge times,
Dp = droplet diameter, fl.
Ds = nozzle diameter, in. (inlet or out Services Holdup Times Surge Time
let vaporlliquid as specified)
D YIl = vapor disengagement diameter, ft
LLL-NLL (NLL-HLLI NLL-HLL INLL-LLLI
min. min.
E = weldedjoint efficiency
F Il =drag force.lb,
Fa = gravity force, Ib, A. Unit Feed Drum 10 5
g :: gravitational constant. 32.17 fl/s'
8.. = 32. 17 (lbmlft)/O b.-s') B. Separators
H Il =disgengagement height, fI . 1. Feedto column 5 3
H II = holdup height. fl 2. Feedto other drumor tankage
HUN = H,.L to inlet nozzle centerline al with pump or through exchanqer 5 2
height. ft bl withoutpump 2 1
HLL = high liquid level
3. Feedto fired heater . 10 3
H LU . =low Liquid Level height, ft
H,,,; =mist eliminator to top tankheight, It
C. Reflux or product accumulator
Hs '" surge height, ft
H; = total vertical separator height, ft 1. Reflux only 3 2
Hy '" vapor disengagementarea height, fl 2. Reflux and product 3+ 2+
K '" terminal velocity constant, ftls • based on reflux (3 rnin.] + appropriate
L '" vessel length, ft holdup time of overhead product
LLL =low liquid level (per B-1, 2,3) .
L. II" :: vapor/liquid separation minimum
length, ft D. Column bottoms
Me :: droplet mass, lb,
1. Feedto another column 5 2
NLL :: normal liquid level
2. Feedto other drumor tankage
P = pressure, psig or psia
Q( :: liquid volumetric flow, fl·'1 min
a)with pumpor throughexchanger 5 2
Q.<I :: mixture volumetric flow, ft'/s, b)withoutpump 2 1
IPflmin 3. Feedto firedboiler 5·8 2-4
Qv '" vaporvolumetric flow. fl9/ s, fl'/min • based on reboilervapor expressed as
S :: vessel material stress value, psi liquid (3 min.) + appropriate
TH =holdup lime, min. holduptimeforthe bottom product
I. :: head thickness. in (per 0·1, 21
I, = shell thickness. in
V Ail '" allowable horizontal velocity, ftls
E. Compressor suction!interstagescrubber
U; '" terminal velocity. ftls
• 3 min between HLL (HIA) and HLSD
V.. '" mixture velocity, ftls
U; :: vapor velocity, ftls • 10 min from bottom tangent lineto HIA
VH =holdup volume. f!'
VU L :: LLL volume, fl' F.Fuel gas knockout drum
V5 '" surge volume. ft' • 20 ft slug inthe incoming fuel gas line
VT '" total volume (horizontal vessel), ft' between NLL and HLSD
W '" vessel weight, lb"
Greek Letters G. Aare knockout drum
• 20 to 3D min. to HLL
I.. = mixture liquid fraction
!Jv '" vapor viscosity, cP
Personnel Factor Instrumentation Factor
PL '" liquid density, (b/fl"
Experienced 1.0 Well instrumented 1.0
P... = mixturedensity, Ib/ft'
P" = vapordensity, Ib/ft' Trained 1.2 Standard instrumented 1.2
¢ :: liquiddropout time, s Inexperienced 1.5 Poorly instrumented 1.5

56 • OCTOBER 1993. CHEMICAL ENGINEERING PROGRESS


If there is a mist eliminator, add 3 to 6 6. If the surge volume is not specified, a. the vessel top tangent line if there is
in. to DVf) to accommodate a support select a surge time from Table 2 and no mist eliminator or
ring and round up to the next 6 in. calculate the surge volume: b. the bottom of the demister pad.
increment to obtain D. If there is no
mist eliminator D = DVI)' v, = (T) (OJ ft· ([6) Hn = 0.5 D; or a minimum of
4. Ca lc ulate the liquid volum etric 7, O bta in lo w liquid le vel height ,
fl ow rate: H LLL , from Table 3. HI) = 36 + 1f2 dN' in. (without mist
8. Calculate the height from low liq- eliminator) (2 0)
_ W I. .3 .
Q L - (60) (p I.) .ft /m in ([ 4) uid level to normal liquid level:
HI) = 24 + 1f2 d". inches (with mist
H = VH tt ( 17) eliminator)
5. Selec t holdu p time from Table 2 H (n / 4) D~! '.J'
and calculate the holdup volume: 12. If there is a mist eliminator. take 6
i ft minimum in. for the mist eliminator pad and take
v, = (T,,) (Q,) It' (15) 9. Calculate the height from norm al I fl. from the top of the mist eliminator
liquid level to high liqu id level (or to the top tangent line of the vessel.
high level alarm): 13. Calcul ate the total height. HI' of
the vessel:
Table 3. Low liquid V .~
level height. Hs = 2 ,j .t ( 10)
. 0

(n /4) D \I H r = HILL + H" + H I' + HUN+


Vessel Vertical Horizontal
H[J + HII/o' ft (2 1)
diameter LLL LLL
6 in minimum
10. Calculate the height from high liq- where H ,II/; is the height from step 12;
< 300 psia > 300 psia uid level to the centerline of the inlet if there is no mist eliminator H .\W = O.
nozzle: Horizont al design proced ure (See
S4ft 15 in. 6 in. 9 in. Figure 2).
6ft 15 in. 6 in. 10 in. HUN= 12 + d.\" in. (with inlet diverter) 1. Calculate the vapo r volumetric
8ft 15in. 6 in. 11 in. flow rate, Q\, using Eq. 12.
10 ft 6 in. 6 in. 12 in.
12ft 6 in. 6 in. 13 in.
HUN = 12 + 1f2 d.\" in. (without inlet 2. Calcu late the liqu id volumetric
16 ft 6 in. 6 in. 15 in.
div crter ) ([ 9) flow rate, QI.' using Eq. 14.
3. Calcu late the vertical termin al
Note: d" is calculated as per Table 4. vapor velocity. U'; using Eq. 13. ( K
11. Calcula te th e disengage men t va lue as per T abl e I for no mi st
a e 4. n et nozz e srzmq. height, from the centerline of the inlet eliminator). Set VI' = 0.75 V I for a
nozzle to: con servative desi gn.

T!~
v D S HLL
NLL
I ~ A H
~ All LLL

/ ~
Feed Inlet

fi-
· ~H!:.l _ - J~v - - =-~~. ~"-~
VaporDutlet

Table 5. LID ratio guidelines.


Vessel Operating
Pressure (psig)

0<PS250
250 < Ps 500
IJD

1.5-3.0
3.0-4.0
• Fig ure 2.
E
Hor izontal two-phase
o
-,
_N.!-L

----1---------
LLl
Hl l
M~. ~2·~ _ _ ±surge
Holdup

separator.
500<P P>500 4.0-6.0

CHEMICAL ENGINEERING PROGRESS • OCTOBER 1993 • 57


F L U I D S / S OLIDS HA N D LI N G

Table 7. Wall thickness, surface area and


approximate vessel height.
Wall Thickness Surface Area
(in.] (ft')
hX4
HID to AlAr Shell PD !tDL
y= AlAr 2SE-I.2P + t•.
X= HID
a =4.755930E-5 2:1 Elliptical Heads PD 1.09lJ2
b = 3.924091 2SE.....O.2P + I,
c =0.174875
d = -6.358805 Hemispherical Heads PD 1.571lJ2
e = 5.668973 4SE-o.4P + t,
f = 4.018448
g= 4.916411
Dished Heads 0.842lJ2
h =-1.801705 O.885PD +1
i = -0.145348 SE-o.IP c

AlA,to HID Appropriate Vessel Height


y= HID
X=AlA r Notes:
a = 0.00153756
b =26.787101 P,design pressure, psig(typically, operating pressure + (15-30) psi or 10-15%, whichevergreater
c =3.299201 Temperature
d = - 22.923932 T,design pressure, OF (typically, operating pressure +25-50°F if TO
ft > 200°F. if T.,. < 200°F, 250°F
e = 24.35351 8 • under650°Fdoesnot reduce wall thickness
f = -14.844824
g = - 36.999376
• if overpressure caused by boiling, should be Tap
Temperature
h =10.529572
i = 9.892851 D, diameter, in.
S, allowablestress, psi (Reference 91
E, joint eHiciency, (0.6-1.0), 0.85 for spot examined joints, 1.0for 100% x-ray joints
4. Select a holdup time from Tabl e t" corrosion allowance, in,typically 0 to q in.
2 and calculate the holdu p volum e, t. in.,larger of t. and tH (to nearestq in.]
VII' using Eq. IS.
5. If the surge volume is not speci-
fi ed, select the surge time from Table 8. Us ing H u./D, obt ain AII./A) 12. Ca lc u la te th e ac t ua l va po r
2 and calculate the surge volume, V,. using Tab le 6 and calculate the low velocity, V I •..\ :
using Eq. 16. liquid area. A u l '
6. Obtain an estimate of UD from 9. If there is no mist eliminator pad, o, " /'/Is
u =A
V.\
(27)
T abl e 5 a nd initi all y calc ulate th e the minimum height of the vapor disen- v
diameter acco rding to: gagement area (A I) is the larger of O.2D 13. Calculate the minimum length
or I fl. If there is a mist eliminator pad, required for vapor-liqu id dis engage-
_ / + \.\/ ) )11.1 .
4 (\/1 (22) the minimum height of the vapor disen- ment, L HI S :
D- ( (lr) (O .6)(U D) ,.II gagement area is the larger of O.2D or 2
fl. Hence. set HI ' to the larger of O.2D or (2 X)
(Round to nearest 0.5 ft.) 2 ft ( 1 n if there is no mist eliminator).
Calculate the total cross-sectional area Using H //). obtain A/A } using Table 6 14. If L < L II IN , then set L = L Ilis '
_ Tr 2 and calculate AI ' (Vapor/l iquid sepa ration is co ntrol -
A I - 4D (23) 10. Calculate the minimum length to ling ). T his s imply resu lts in so me
accommodate the liquid holdup/surge: e x tra holdup . If L IllY » L . then
Calc ulate the low liquid level height, increase /-II' and repeat from the step
Hul' using Ta ble 3 or 9. If L > L HIS ' the desig n is accep table
for va por/liquid separat ion. If l . »
H, li = O.S/) + 7, ill . (24 ) L I II., ,, (Liquid holdu p is controlling), L
I I. Calculate the liquid dropout time, ca n on ly be d ec reas ed a nd L All i\'
increased if H I' is decreased. H I' may
wh e re [) in I'l and ro und up to the A,
'Il = HI'
I I ' S
LJ v
( 26) only be dec reased if it is greater than
neares t in.. if D ~ 4'0" , H U I = 9 in. the minimum spec ified in the step 9.

58 • OCTOBER 1993· CHEMICAL ENGINEERING PROGRESS


Qv = 145,6001blh = 10.09 fi'l s
( 3,600l. )(4.0 1-'&)
h, .Ii'
.
Table 8. Conditions for
the horizontal separator • Equation A.
(See Example calculation).
MassRow(lb/h) p (IbM)

Vapor Wy= 145,600 py= 4.01


Uquid WL =46,100 p[ = 38.83
• Equation IJ.

Table 9. Selection of
head types.
• Equation C.
1. 2:1 ellipticalheads aretypicallyused

(
when D < 15 hand P> 100 psig. l /i
2. Hemispherical heads aretypicallyused
when D> 15 ft regardless of P.
3. Dished heads with knuckle radius =0.6D
Bre typicallyused when D< 15 ft and
P< 100 psig.
D =
4(1 97.90+98.95)

• Equation D.
7[(0.6)(5.0)
l .
= 5.01 [tls,
.
usc 5.0./t

Notes:
P= design pressure _ VH+~' _ 197.90+98.95 ? . . ( .
0= drum diemeter
L - AI _ A - A ' L - 19.63 _ 7.34 _ 2.16' _9.3, say 29.5.1t
v U L

• Equation E.
(Calcul ati ons would h a vc to b e
repeated from the step 9 with reduced
H v)' Calculate VD . If VD > 6.0 then 2.0 Ii 690
¢ = 0.29 [tls =. s
increa se D and repe al ca lc ulatio ns
from the step 6 . If V D < 1.5, then
• Equation F.
decrea se J) and rep eat calc ulations
from the step 6.
15. Calc ulate the thickness of the 4. Calculat e the holdup volume:
shell and head s acco rding to Table 7. \/ " = (10 min .) (19.79 ft /min.) =
16. Calculate the surface area of the Size a horizontal 197.90 ft '
'
shell and heads accordin g to Ta ble 7. 5. Calculate the surge volume:
17. Calculate the approximate ves- separator with a mist \/\=(5 min.) ( 19.79 Inmin.) =98.95 ft-'
sel weight according to Table 7. 6. Assume VD = 5.0. Initially set
18. In cre a se a nd d ec re ase the eliminator pad. the diameter (Eq. D)
d iam et er by 6 in. inc re me nts and A , = rr/4 (S.O lW = 19.63 It'.
repeat the calc ulations until VD has separate the following mixture . The 7. Calculate low liquid height:
ranged from 1.5 to 6.0. operating pressure is 975 psig and the H,u = (0.5)(5.0) +7 = 9.5 in., usc lOin .
19. With the optimum vessel size holdup and surge are to he 10 min and 8. Calcul ate the low liqu id level
(minimum weight), calculate normal S min respecti vely. Usc a design tem- area:
and high liquid levels: perature of 650°F. Sec Table X. H,jD = D.1 67
I. Calcul ate the vapor volumetric Using Tabl e 6, A,,/AT = 0. 110
A\,[,[ = A u l . + \//L (29 ) flow rate (Eq. A). A IL! = (0. 110) ( 19.63 ft ~ ) = 2.16 IF

2. Calcul ate the liquid volumetric 9. Set H I' = 2 It, H /D = 2/5 =0.4
With A v ,,1A, obtain H \U from Tabl e 6 fl ow rate (Eq. B). From Tabl e 6, A/A, = 0.374
3. Cal cul ate the vert ical terminal A I' = (0.373)( 19.(3 ) = 7.34 IF
(30) velocity (Eq. C): K = 0.13 (GPSA val- 10. Calculat e the length to accom-
ue di vid ed by two since " no mist modate holdup /surge (Eq. E).
Example: Size a horizontal sepa- eliminator" value is used ) II. Calcu late the liqu id dropout
rater wi th a mist el iminator pad to V I' = O.75U, = 0.29 ft/s time (Eq. F).

CHEMICAL ENGINEERING PROGRESS • OCTOBER 1993 • 59


FLUIDS/SOLIDS HANDLING

12. Calculate the a ctual va po r


ve loc ity (Eq. G ).
10.09.fi'ls
13. Calculat e L \ II ,V (1.37 u..,.\ = 1.37 [tls
ft/s)(6.90 s) = 9.45 ft 7.34.fi2
14. L » L'd/V but /-I v is minimum
and cannot be reduced so L cannot be • Equation G.
red uced .
UD= 29 .5/5 .0 = 5.9
15. Calculate the thi ckness of the
she ll and heads acc ordin g to Table 7:
t - (l,072)(60 ) L - '1 1')') .
• Tabl e 9, use 2: I e lliptica l heads , - 2( 17,500)(0.85)- ( 1.2)( 1.072) + 16 -.:.. .. __ 111
• Assume E = O.~5
• Assume SA 516 70 Carbon Steel,
Design Temp. = 65(rF
• Equation H.
• From ( 9), S = 17,500 psi
• Ass ume c orrosion allowance =
YII, in.
• P = 9 75 x 1.1 = I.on ps ig (See
Eq. H ). t- (I()~2)(60) 1-'1')40 '
use I, = 2-·% in. (See Eq . I) u>: 2 (17500)(().~5) - (0.2)( 1(72) + 16 - .:.. .- 111.
use III = 2-Y, in., and usc I = 2-'% in.
16. Calc ula te the surface area of the
shell and heads accordin g to Tabl e 7: • Equation J.
A~ = ]"(5.0 ft) (29.5 ft) = 463 .38 ft"
and
All = ( l. 09) (5.0 ft)" = 27 .25 IF
17. Calculate the upprox imatc vessel
weight (Eq. J): = 50,224 lb .
w II )(2.375 in)(463.38
490 ~ Ii" + (2)(27.25)
18. Try [) = 5.5 ft and repeat ca lc ula-
tio ns until minimum we ight o f she ll
( [t (12
inlft )
and heads is obtai ned. mil
• Equation ./.
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Facilities Engineering, Facilities/ University of Calgary. Calgary. Alberta. Canada


Literature Cited Chemical Engineering Conference (I (88). {403/220·5751; Fax: 403/282-3945; E-mail: svrcek
@ acs.ucalgary. cal. Or. Svrcek previously
I. Sauders M.• and G.G. Brown, Ind. Eng. 6. American Petroleum Institute, worked as a senior systems engineer in the
Chcm.. 2ti( l ), p. 98 (1934). Recommended Practice 521 (1982). controlsystems groupof Monsanto Company,
SI. Louis. MO. Upon leaving Monsanto. he
7. Watkins, R.N., "Sizing Separators and joinedthe University ofWestern Ontario. He
2. Gas Processors Suppliers Association,
.. ngineering Data Book," 10th edition, Accumulators," Hvdrocarbon received his SSc and PhD degrees in chemical
Vol. I. Chapter 7 ( 1(87). Processing, 46( 11), p. 253-256 (1967). engineering from the University of Alberta,
Edmonton.
3.0110 H. York Company Inc., "Mist 8. Gerunda, Arthur, "How To Size Liquid
Vapor Separators:' Chem . Eng., p. 81-84 W. MONNERY is a PhD candidate atthe
Elimination in Gas Treatme-nt Plants and
Refineries," Engineering, Parsippany. NJ. (1981). University of Calgary, Calgary, Alberta.
Canada (403/220-5751; Fax: 403/282·3945; E-
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4. Perry, Robert H. and Cecil H. Chilton.
cds., "Chemical Engineers' Handbook," VIlI . Division I, Table UCS-2J , p. 270· researching the predictionof physical proper-
Sth edition, Chapter 2. p. 2-6 (1973). 21771 (1986). ties. He previously workedas a process engi-
neer for Colt Engineering Corp. and lava lin
5. Carpentier, P,L.. "Important Parameters Inc. Mr. Monnery received his SSc and MSc
For Cost Effectil'e Separator Design," W. Y. SVRCEK is a professor in the department degrees in chemical engineeringfrom the
Shell Oil Company-Head Office of chemicaland petroleum engineering at the University of Calgary.

60 • OCTOBER 1993. CHEMICAL ENGINEERING PROGRESS

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