CDB 2052 LAB I Course Outline 201901 TERM

CDB 2052 Chemical Engineering Lab I Jan 2019
CDB 2052
CHEMICAL ENGINEERING LABORATORY I
JAN 2019
LABORATORY COURSE OUTLINE
1. GENERAL INFORMATION & COURSE ADMINISTRATION
CREDIT UNIT : 2 CREDIT HOURS (Core Engineering subject)
COORDINATOR
Room 05-03-36, Block 5
1. AQSHA Ext 7602
aqsha@utp.edu.my
Room 05-03-08, Block 5

2. Zulfan Adi Putra, PDEng Ext 7562
zulfan.adiputra@utp.edu.my
LABORATORY TECHNOLOGISTS
Ext 7540 /
1. Muhammad Fairis Arifin fairis.arifin@utp.edu.my
0174288944
Ext 7569 /
2. Azriha Anuar azriha_anuar@utp.edu.my
0125294293
Ext 7542 /
3. Norhasneyza Bt Zakaria norhasneyza_zakaria@utp.edu.my
0199171601
M Shaharuddin Bin A Ext 7630 /
4. mshaharuddin_arahman@utp.edu.my
Rahman 0193339022
1
LAB INSTRUCTORS (GA STUDENTS)
No Name Phone Email Session

1 Zubair Shahid 01136283845 engrzubair86@gmail.com Tuesday
2 Farah Aina farahaina02@gmail.com Tuesday
3 M Zulfiqar 0143623707 zulfiqar_rehmani@hotmail.com Tuesday
4 Nor Faizatulfitri 01137728403 faizatulfitri23@gmail.com Tuesday
5 Ahmer Ali Siyal 0133214436 ahmersiyal@gmail.com Tuesday
6 Abdul Rahman abdul_17010239@utp.edu.my Tuesday
7 Prasenna Joy prasenna_18001892@utp.edu.my Tuesday
8 M. Mubashir +60-10-3912069 engr.mubashir37@gmail.com Tuesday
9 Hanan Mohsin hanan_16001757@utp.edu.my Tuesday
10 Shafiq Mohd. Hizam shafiq_17005830@utp.edu.my Tuesday
11 Rizwan Safdar 0102421497 engr_chem@hotmail.com Thursday
12 Premchand premchand_17006826@utp.edu.my Thursday
13 Hirra Anjum hirra.anjum_g03135@utp.edu.my Thursday
14 Farooqi Ahmad Salam ahmad_17007920@utp.edu.my Thursday
15 Lupete Bhullar 0193683219 lupetebhullar@gmail.com Thursday
16 Rendra Hafyan rendra_hafyan@ymail.com Thursday
17 Wegik Prasetyo wegik.dwi.prasetyo@gmail.com Thursday
18 Imtasal imtisalzahid@yahoo.com Thursday
19 Nur Syakinah 0175125872 nursyakinah94@gmail.com Thursday
20 Mansoor Shah engr.mansoor@nwfpuet.edu.pk Thursday
Duties and responsibilities of the lab instructors (GA students):

 All lab instructors and the coordinator are to assemble in Block 3, 10 minutes prior to each lab. Check if
the equipment is ready to use and report if there is any problem regarding previous week experiment to
the lab coordinator.
 Conduct viva/pretest to check the readiness of the students prior to the experiment. Starting from the 3rd
experiment only.
 Take note on the late comer(s) and deduct his/her marks by 50%.
 Supervise the students in doing the experiments.
 Evaluate the reports and give feedback on the content and what needs to be improved. E.g. report of
experiment in week 5 will be submitted by the students prior to the experiment in week 6. Evaluate the
report while the students doing their experiment. Once the students are finish with the experiment, give
them the feedback on the report.
2
2. COURSE LEARNING OUTCOME (CLO)
At the end of this course, you should be able to demonstrate the practical skills and the understanding of knowledge
on chemical engineering unit operations focusing on Fluid Mechanics and Process Heat Transfer.
3. LABORATORY MODULE CONTENT, GA LIST & LAB TECHNOLOGIST
FLUID MECHANICS
Tuesday Thursday
Experiment Number & Title Location Lab Technologist
(08.00 – 18.00) (08.00 – 18.00)
M. Fairis Arifin/M
Abdul
3. Impact of Jet 04.00.13 Zubair Shahid Shaharuddin Bin A
Rahman
Rahman
M. Fairis Arifin/M
4. Flow in Pipe and Fittings 04.00.13 Farah Aina Prasenna Joy Shaharuddin Bin A
Rahman
M. Fairis Arifin/M
5. Cavitation 04.00.13 M Zulfiqar M. Mubashir Shaharuddin Bin A
Rahman
M. Fairis Arifin/M
Nor Hanan
6. Fluid Mixing 04.00.13 Shaharuddin Bin A
Faizatulfitri Mohsin
Rahman
M. Fairis Arifin/M
Ahmer Ali Shafiq Mohd.
10. Pressure Drop in Packed Bed 04.00.13 Shaharuddin Bin A
Siyal Hizam
Rahman
PROCESS HEAT TRANSFER

Tuesday Thursday
Experiment Number & Title Location Lab Technologist
(08.00 – 18.00) (08.00 – 18.00)
M. Fairis Arifin/M
Rizwan Rendra
13. Plate Heat Exchanger 03.00.06 Shaharuddin Bin A
Safdar Hafyan
Rahman
M. Fairis Arifin/M
Wegik
14. Shell & Tube Heat Exchanger 03.00.06 Premchand Shaharuddin Bin A
Prasetyo
Rahman
M. Fairis Arifin/M
17. Heat Conduction 04.00.16 Hirra Anjum Imtasal Shaharuddin Bin A
Rahman
M. Fairis Arifin/M
Farooqi
19. Radiation Heat Transfer 04.00.16 Syakinah Shaharuddin Bin A
Ahmad Salam
Rahman
M. Fairis Arifin/M
Lupete Mansoor
20. Cross Flow Heat Exchanger 04.00.16 Shaharuddin Bin A
Bhullar Shah
Rahman
3
4. LABORATORY DELIVERY & SCHEDULING
a) Lab Session: Group A1-A10 : Tuesday 08.30 – 12.00

Group B1-B10 : Tuesday 14.30 – 18.00
Example: Group A1 will run Exp No. 3 (Impact of Jet) on the first week (Jan 22 2019, 8.30-12.00) and follow
by experiment No. 4, 5, 13, 14, 17 for the following week.
ACAD. Wk Wk Wk Wk Wk Wk Wk Wk Wk Wk Wk Wk
WK. 1 2 3 4 5 6 7 8 9 10 11 12
Tuesday
EXP. SEQ. (8.30 – 1ST 2ND 3RD 4TH 5TH 6TH
DATE OF
12.00) 15 22 29 5 12 19 26 5 12 19 26
EXP. Jan Jan Jan Feb Feb Feb Feb Mar Mar Mar Mar
A1 3 4 5 13 14 17
A2 4 5 6 14 17 19
LAB I PROJECT REPORT SUBMISSION

LAB I TEST, MARCH 15, 2019
A3 5 6 NO LAB ACTIVITIES 10 17 19 20
6 10 13 19 20 3
GROUP 1A
A4
LAB SEMINAR
A5 10 13 14 20 3 4
A6 13 14 17 3 4 5
A7 14 17 19 4 5 6
A8 17 19 20 5 6 10
A9 19 20 3 6 10 13
A10 20 3 4 10 13 14
WK. 1 2 3 4 5 6 7 8 9 10 11 12
Tuesday
DATE OF
18.00) 15 22 29 5 12 19 26 5 12 19 26
B1 3 4 5 13 14 17
B2 4 5 6 14 17 19
B3 5 6 10 17 19 20
NO LAB ACTIVITIES
6 10 13 19 20 3
GROUP 2A
B4
LAB SEMINAR
B5 10 13 14 20 3 4
B6 13 14 17 3 4 5
B7 14 17 19 4 5 6
B8 17 19 20 5 6 10
B9 19 20 3 6 10 13
B10 20 3 4 10 13 14
4
Lab Session: Group A11 – A20 : Thursday 08.30 – 12.00

Group B11 – B20 : Thursday 14.30 – 18.00
WK. 1 2 3 4 5 6 7 8 9 10 11 12
Thursday
DATE OF
12.00) 17 24 31 7 14 21 28 7 14 21 28
A11 3 4 5 13 14 17
A12 4 5 6 14 17 19

A13 5 6 10 17 19 20
6 10 NO LAB ACTIVITIES 13 19 20 3
GROUP 1B
A14
LAB SEMINAR
A15 10 13 14 20 3 4
A16 13 14 17 3 4 5
A17 14 17 19 4 5 6
A18 17 19 20 5 6 10
A19 19 20 3 6 10 13
A20 20 3 4 10 13 14
WK. 1 2 3 4 5 6 7 8 9 10 11 12
Thursday
DATE OF
18.00) 17 24 31 7 14 21 28 7 14 21 28
B11 3 4 5 13 14 17
B12 4 5 6 14 17 19
B13 5 6 10 17 19 20
NO LAB ACTIVITIES
6 10 13 19 20 3
GROUP 2B
B14
LAB SEMINAR
B15 10 13 14 20 3 4
B16 13 14 17 3 4 5
B17 14 17 19 4 5 6
B18 17 19 20 5 6 10
B19 19 20 3 6 10 13
B20 20 3 4 10 13 14
5
NOTE:
● On the day of the experiment, let the lab instructor knows that you’re there. Then, hand over the
report of the previous experiment to the corresponding lab instructor and discuss for the viva (post-
test), if applicable. Then, go back to your current experiment and do the pre-test (starting from the
3rd experiment onwards).
● DO NOT come late!!! 50% marks deduction on the pretest and 10% group marks deduction will be applied
to those (individual & group) who come late!
● DO NOT come unprepared! GA students will conduct a pretest, starting from the 1st experiment (week 3),
prior to the experiment to check if each student understands what to do. Pretest can be conducted in the
form of interview, short quiz or practice.
● Bold numbers in light yellow box = group numbers
● Numbers in white box = experiment numbers with short report
● Numbers in light orange box:

● LONG report
6
5. GROUPING
Please refer to group list distributed in Ulearn.
6. LABORATORY ASSESSMENT
Assessment Task Mark Assessment Type
Lab Reports 40% Group
Short Project 10% Group
Pretest and posttest 10% Individual
Final Presentation (with e.g. ppt, video, etc.) 10% Individual/Group
Test 30% Individual
TOTAL 100%
7. REPORT SUBMISSION
a) Table below illustrate the types of report and their submission criteria:
Experiment Type Report due Submit to Remarks
1st, 2nd, 3rd, 4th, Respective GA Please email

Short Report The following week softcopy of report
5th, (hardcopy)
to your respected
GA and CC the
coordinator
(Aqsha & Zulfan
Respective GA Adi Putra, PDEng)
6th Long report 15th March 2019
(hardcopy) according to the
deadline as well.
b) The length and contents of the report: please refer to Appendices.

c) The content of the videos: please refer to Appendices.
d) Submit report & presentation (video) on time. Late is not allowed.
e) Softcopy shall be emailed to the Coordinator.
● Please ensure the report file size does not exceed 5 MB.
● The filing name format for both reports and videos: YYYYMMDD-GXX-EXPXX.
Example: Group 1, Exp 1, Date 25/01/2019, the file name should be typed as:
20190125-G01-EXP01
7
8. REFERENCES
a) de Nevers, N., Fluid Mechanics for Chemical Engineers, 3rd Ed.,McGraw-Hill, 2005.
b) McCabe W.L., Smith J. C. and Harriot P., Unit Operations of Chemical Engineering,
7th Ed., McGraw-Hill. 2005.
c) Cengel, Y. A. and Cimbala, J. M., Fluid Mechanics: Fundamentals & Application, McGraw-Hill, 2006.
d) White, F. M., Fluid Mechanics, 5th Ed., McGraw-Hill, 2005.
e) Geankoplis, C.J., Transport Processes and Separation Process Principles, 4th Ed. Prentice Hall. 2003.
f) Mott, R.L., Applied Fluid Mechanics, 6th Ed. in SI Units, Pearson-Prentice Hall. 2006.
g) Holman, J. P., Heat Transfer, 8th SI Metric Ed., McGraw-Hill, 2001.
h) Hewitt, G. F., Shires, G. L. and Bott, T. R., Process Heat Transfer, CRC Press, 1993.
i) Green D. and Perry R.H., Chemical Engineers' Handbook, 8th Ed., McGraw Hill, 2007.
9. PROGRAM OUTCOMES
PO1 PO7
Apply knowledge of mathematics, science, engineering Understand the impact of professional engineering
fundamentals and an engineering specialization to the solutions in societal and environmental contexts and
solution of complex chemical engineering problems demonstrate knowledge of and need for sustainable
development
PO2 PO8
Identify, formulate, research literature and analyze Apply ethical principles and commit to professional ethics
complex chemical engineering problems reaching and responsibilities and norms of chemical engineering
substantiated conclusions using first principles of practice
mathematics, natural sciences and engineering sciences
PO3 PO9
Design solutions for complex chemical engineering Communicate effectively on complex chemical engineering
problems and design systems, components or processes activities with the engineering community and society
that meet specified needs with appropriate consideration
for public health and safety, cultural, societal, and
environmental considerations
PO4 PO10
Investigate complex chemical engineering problems using Function effectively as an individual, and as a member or
research based knowledge and research methods including leader in diverse teams and in multi-disciplinary settings
design of experiments, analysis and interpretation of data,
and synthesis of information to provide valid conclusions
PO5 PO11
Utilize modern engineering and IT tools to evaluate Recognize the need for, and have the preparation and
complex chemical engineering activities ability to engage in independent and life-long learning in
the broadest context of technological change
PO6 PO12
Apply reasoning informed by contextual knowledge to Demonstrate knowledge and understanding of engineering
assess societal, health, safety, legal and cultural issues and management, business acumen and entrepreneurship in
the consequent responsibilities relevant to professional multidisciplinary environments
engineering practice
8
DELIVERY
PROGRAM OUTCOMES (PO) ASSESSMENTS
METHODS
CDB2052
Laboratory Reports
Laboratory Session
CHEMICAL ENGINEERING LABORATORY I
Presentation
Presentation
Reflections
Viva Voce
Viva Voce
Lab Test
Lab Test
PO10
PO11
PO12
PO1
PO2
PO3
PO4
PO5
PO6
PO7
PO8
PO9
COURSE LEARNING OUTCOMES 1 2 3 4 5 6 7 8 9 10 11 12 1 2 3 4 1 2 3 4 5
Demonstrate the practical skills and the

understanding of knowledge on chemical
1 √ √ √ √ √ √ √ √ √ √ √ √
engineering unit operations focusing on
Fluid Mechanics and Process Heat Transfer.
9
10. DO’s and DON’Ts
a) You must attend all lab sessions. In case of absentees, these rules apply:
Absent because of: What should you submit to the Coordinator?
● Illness / hospitalization. A valid Medical Certificate issued by registered Medical Doctor.
● UTP commitments Release letter from the Chairman, lecturer or authorized personnel.
● Family matters Letter from parents or responsible next-of-kin.
You are required to inform the Lab Coordinator/Lab Technologist/ Lab

● Other emergencies/
Instructor. This needs to be supported by an authorized document that
unavoidable matters
has to be submitted later on.
b) Lab session is a GROUP EFFORT.

● If you are absent during the lab session, you cannot replace it. However, you have to be
involved in preparing the lab report with the group members to validate the mark on your
part.
● You must also attend the viva voce session accordingly (subjected to the arrangement with
the Lab Instructor).
● Without valid supporting document due to absenteeism, you will not be getting marks for any
of the lab assessments.
c) In case of lab falls on the public holiday, lab session will be replaced at other suitable time subjected
to availability.
d) In case of equipment breakdown, your experiment will be replaced with another available
equipment. However, cases below apply:
● If equipment breakdown happens after more than half of the experiment requirement, you
must proceed with the available results.
● If equipment breakdown happens less than half of the experiment requirement or before any
results obtained, the experiment must be replaced with other available
experiment/equipment.
11. LAB SAFETY
a) Properly attired.
● You MUST wear your lab coat whenever you are in the lab.
● Other personal protective equipment (PPE, such as goggles, safety helmet, ear plugs, ear muff,
etc) will be provided accordingly.
● These clothing are not allowed in the laboratory:
a. National costumes (baju kurung, cheongsam, saree, traditional outfit, etc),
b. Jubah, skirts (short or long), sarongs, shorts.
c. Sandals, slippers and any uncovered shoes.
● For those who are wearing tudung or hijab, and with long hair, you are required to keep them
neat.
b) The Lab Instructors and Lab Technologists have the authority to ask you to leave the lab if you do not
adhere to the safety regulations.
c) You ARE NOT ALLOWED TO PROCEED with your laboratory work if you fail to do that.
d) Abide to the safety signs in the lab.
10
APPENDICES
11
APPENDIX I: SHORT REPORT FORMAT
1. The report MUST be typed using MS WORD.

2. All graphical representation MUST be tabulated using MS EXCEL.
3. Length of report: NOT MORE THAN 10 pages excluding cover page and appendices.
4. FONT : Use Times New Roman, font size 12.
5. Spacing : 1.
6. Number each page accordingly.
7. Table and Figure Captions as below:
Measured/calculated
performance
Measured/calculated
variable
Figure 1 : Xxxxxx xxxx xxxxxx
Table 1 : Xxxxxx xxxx xxxxxx
12
ITEM DESCRIPTION OF THE CONTENT
 UTP logo – top, centered.

 The experiment number and title.
 The group number.
Cover Page
 The names and ID numbers of the group members.
 The name of the lab instructor in charge.
 The date of experiment.
 Write an abstract in not more than 300 words by highlighting the main
Chapter 1 : Summary &
objective of the experiment, summary of experimental results and brief
Objectives
conclusion.
Chapter 2 :
Methodology/  Write briefly the methodology / experimental procedures involved.
Experimental procedures
 Any observation/s that is/are relevant during the experiment must be

mentioned.
 The main body of the report should NOT exceed the requirement of the
10-pages.
 Each figure/graph must be followed by a relevant title. Put ONLY the
MAIN RESULTS.
E.g. effect of mixture compositions to densities. Density is the
measured/calculated performance (shown in y-axis), while mixture
compositions are the measured/calculated variables (shown in x-axis).
Chapter 3: Results&
 For each result obtained, it must be supported by the relevant
Discussion
description, which discusses the experimental findings with its associated
principles, highlighting weaknesses/discrepancy/errors encountered (if
any) that deviates from theory and propose method for results
improvement.
 Provide ONLY ONE (1) sample of calculation. Other calculations are in the
‘APPENDIX’. You, however, MUST mention anywhere in the main body of
the report that the remaining of the results are included in the
‘APPENDIX’.
 Limit all numbers with MAX 2 decimal points.
Emphasize the main findings of the experiment. The conclusion should answer
Chapter 4: Conclusion
every aspect of the experimental objectives.
Contains the list of references made in the report. (Minimum of 5 references.

References
DO NOT include Wikipedia)
 Set of tables with the raw and calculated data, sample calculations and
Appendix
any additional information.
13
APPENDIX II: LONG REPORT FORMAT
1. The report MUST be typed using MS WORD.

2. All graphical representation MUST be tabulated using MS EXCEL.
3. Length of report: Between 10 to 15 pages excluding cover page and appendices.
4. FONT : Use Times New Roman, font size 12.
5. Spacing : 1.
6. Number each page accordingly.
7. Table and Figure Captions as below:
Measured/calculated
performance
Measured/calculated
variable
Figure 1 : Xxxxxx xxxx xxxxxx
Table 1 : Xxxxxx xxxx xxxxxx
14
ITEM DESCRIPTION
Cover Page As per Short Report format above
Write a summary in not more than 300 words by highlighting the main
Summary & Objectives objective of the experiment, summary of experimental results and brief
conclusion.
 Highlight the fundamentals theory and background of the experiment.

This may include set of relevant equations relating the concept and the
Chapter 1:Literature experimental methodology.
Review & Theory  Include the history of the concept, the previous research that has been
done through the years and the applications in the industries,
emphasizing in oil, gas and petrochemical field.
Chapter 2: Methodology  Explain how the experiment was carried out.

/ Experimental  Use passive voice throughout.
Procedures  Include a flow chart indicating the process flow.
Chapter 3: Results &

As per Short Report format above.
Discussion
Chapter 4: Conclusion As per Short Report format above.
As per Short Report format above.. (Minimum of 10 references. DO NOT

References
include Wikipedia)
Appendices As per Short Report format above.
15
APPENDIX III: COVER PAGE FOR ALL REPORTS
16
APPENDIX IV: COURSE REFLECTIONS
Each student should write a reflection on this Chemical Engineering Laboratory I. The reflection should
include:
1) What you have learned and/or any interesting thing from each experiment that you’ve done.
2) What are the difficulties that you’ve faced
3) What is (are) their suggested action/corrective plan to make this lab better
The course reflection will be discussed during the final presentation in week 13.
Use the following Gibbs Reflective Cycle to guide you in writing the reflection.
17

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CDB 2052 Chemical Engineering Lab I Jan 2019

1. GENERAL INFORMATION & COURSE ADMINISTRATION

CREDIT UNIT : 2 CREDIT HOURS (Core Engineering subject)

Room 05-03-08, Block 5

LAB INSTRUCTORS (GA STUDENTS)

No Name Phone Email Session

Duties and responsibilities of the lab instructors (GA students):

2. COURSE LEARNING OUTCOME (CLO)

3. LABORATORY MODULE CONTENT, GA LIST & LAB TECHNOLOGIST

PROCESS HEAT TRANSFER

4. LABORATORY DELIVERY & SCHEDULING

a) Lab Session: Group A1-A10 : Tuesday 08.30 – 12.00

LAB I PROJECT REPORT SUBMISSION

Lab Session: Group A11 – A20 : Thursday 08.30 – 12.00

LAB I PROJECT REPORT SUBMISSION

● Bold numbers in light yellow box = group numbers

● Numbers in white box = experiment numbers with short report

● Numbers in light orange box:

Please refer to group list distributed in Ulearn.

Assessment Task Mark Assessment Type

Lab Reports 40% Group

Short Project 10% Group

Pretest and posttest 10% Individual

Final Presentation (with e.g. ppt, video, etc.) 10% Individual/Group

Test 30% Individual

Experiment Type Report due Submit to Remarks

1st, 2nd, 3rd, 4th, Respective GA Please email

b) The length and contents of the report: please refer to Appendices.

Demonstrate the practical skills and the

10. DO’s and DON’Ts

Absent because of: What should you submit to the Coordinator?

● Illness / hospitalization. A valid Medical Certificate issued by registered Medical Doctor.

● Family matters Letter from parents or responsible next-of-kin.

You are required to inform the Lab Coordinator/Lab Technologist/ Lab

b) Lab session is a GROUP EFFORT.

11. LAB SAFETY

1. The report MUST be typed using MS WORD.

Figure 1 : Xxxxxx xxxx xxxxxx

Table 1 : Xxxxxx xxxx xxxxxx

ITEM DESCRIPTION OF THE CONTENT

 UTP logo – top, centered.

 Any observation/s that is/are relevant during the experiment must be

Contains the list of references made in the report. (Minimum of 5 references.

APPENDIX II: LONG REPORT FORMAT

1. The report MUST be typed using MS WORD.

Figure 1 : Xxxxxx xxxx xxxxxx

Table 1 : Xxxxxx xxxx xxxxxx

Cover Page As per Short Report format above

 Highlight the fundamentals theory and background of the experiment.

Chapter 2: Methodology  Explain how the experiment was carried out.

Chapter 3: Results &

Chapter 4: Conclusion As per Short Report format above.

As per Short Report format above.. (Minimum of 10 references. DO NOT

Appendices As per Short Report format above.

APPENDIX III: COVER PAGE FOR ALL REPORTS

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