LAPORAN AMALI KIMIA TAK ORGANIK

(KIM3302)

EKSPERIMEN 5
EXPERIMENT 5

PENYEDIAAN SEBATIAN ISOMER NITRO

[Co(NH3)5NO2]Cl2
SYNTHESIS OF NITRO ISOMER
[Co(NH3)5NO2]Cl2 COMPOUND
Nama (Name) :………………………………………

No.Matriks (Matric number) :………………………………

Tarikh (Date): ………………………………………………

Nama Ahli Kumpulan beserta no. matriks:

Group members with martic no.

1)

2)

3)

4)

5)

6)

Nama Demonstrator/Nama Pensyarah:

Demonstrator’s name / Lecturer’s name:

...................................................................................................................................... FRONT PAGE

/2
 LAPORAN AMALI KIMIA TAK ORGANIK
(KIM3302)
Markah laporan amali mengikut rubrik ICGPA:
Mark for laboratory report based on ICGPA rubic:
FRONT INTRO METHOD RESULTS DISCUSSION CONCLUSION REFERENCE WRITING
PAGE SKILL

PENGENALAN :
INTRODUCTION:

RUJUKAN :
REFERENCE:

OBJEKTIF :
OBJECTIVE:

i.

ii.
 LAPORAN AMALI KIMIA TAK ORGANIK
(KIM3302)

iii.

INTRO

/10
 LAPORAN AMALI KIMIA TAK ORGANIK
(KIM3302)
KAEDAH :
METHODOLOGY:

METHOD

/6
 LAPORAN AMALI KIMIA TAK ORGANIK
(KIM3302)
KEPUTUSAN DAN PENGIRAAN
RESULTS AND CALCULATION

PERHATIAN: Keputusan data inframerah perlu dilabel dan dilampirkan bersama LAPORAN
AMALI ini. Sila buat salinan spektrum IR ini kerana ia akan memerlukannya dalam Eksperimen 6
sebagai rujukan. Simpan juga sebatian ini untuk kegunaan dalam eksperimen 6.

ATTENTION: Compile the labeled IR spectrum along with this experimental datasheet. Please
make a copy of this IR spectrum as it will be used in Experiment 6 as a reference. Keep this
compound to be used in Experiment 6

Nyatakan Pemerhatian dan data-data yang diperolehi dengan lengkap:

State your observation and data(s) completely:

(I) Penyediaan [Co(NH3)5CI]CI2

Synthesis of [Co(NH3)5CI]CI2

(II) Penyediaan [Co(NH3)5NO2]CI2, (isomer nitro)

Synthesis of [Co(NH3)5NO2]CI2, (nitro isomer)
 LAPORAN AMALI KIMIA TAK ORGANIK
(KIM3302)
Pengolahan Data
Data Analysis

a. Kirakan peratus hasil untuk:

Calculate the percentage yield for:

i. [Co(NH3)5CI]CI2

ii. [Co(NH3)5NO2]CI2

b. Tuliskan persamaa kimia seimbang untuk pembentukan kompleks-kompleks:

Write the balance chemical equation for the formation of complexes:

i. [Co(NH3)5CI]CI2

ii. [Co(NH3)5NO2]CI2
 LAPORAN AMALI KIMIA TAK ORGANIK
(KIM3302)
SOALAN
QUESTION

1. Dengan menggunakan keputusan inframerah, berikan nombor gelombang (wave number) serta
kumpulan berfungsi yang utama dan penting bagi hasil (i) dan (ii).

By using IR data, list the wavenumbers and major functional groups for product (i) and (ii).

Hasil (i)
Product (i)
i)..................................................................................................
ii).................................................................................................
iii)................................................................................................
iv)................................................................................................

Hasil (ii)
Product (ii)
i)..................................................................................................
ii).................................................................................................
iii)................................................................................................
iv)................................................................................................

2. Lukiskan struktur molekul bagi hasil (ii) dan (iii).

Draw molecular structure for product (i) and (ii).

Hasil (i) Hasil (ii)

Product (i) Product (ii)
 LAPORAN AMALI KIMIA TAK ORGANIK
(KIM3302)
3. Nyatakan geometri bagi:

State the geometry for:

Hasil (i)
Product (i)

Hasil (ii)
Product (ii)

4. Nyatakan definasi bagi nombor koordinasi

Define coordination number

5. Nyatakan nombor koordinasi bagi:

State the coordination number for:

Hasil (i):
Product (i)

Hasil (ii):
Product (ii)

6. Takrifkan dan nyatakan fungsi ‘counter ion’

Define counter ion and state the function of counter ion

 LAPORAN AMALI KIMIA TAK ORGANIK
(KIM3302)
7. Berikan atom atau molekul yang bertindak sebagai ‘counter ion’ di dalam amali ini.

State the atom or molecule that acts as counter ion in this experiment

RESULTS

/20

PERBINCANGAN
DISCUSSION

(Perhatian: Gunakan helaian tambahan sekiranya tidak mencukupi.)

(Attention: Use extra sheets if the provided one is insufficient.)

DISCUSSION

/10
 LAPORAN AMALI KIMIA TAK ORGANIK
(KIM3302)
KESIMPULAN
CONCLUSION

CONCLUSION

/4

RUJUKAN
REFERENCE

REFERENCES

/4

WRITING
SKILLS

/4