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1. Introduction has been successfully employed for such purposes (with operat-
ing temperatures of around 550 ◦ C) for many years [1,2]. Recent
At both room temperature and elevated temperature, the ma- research [3–8] has examined the suitability of employing stainless
terial characteristics of stainless steel differ from those of carbon steel for fire resistant structural applications, where the demands
steel due to the high alloy content. At room temperature, stainless are very different from those in long service industrial applica-
steel displays a more rounded stress–strain response than carbon tions. For instance, for structures in fire, the duration of exposure to
steel and no sharply defined yield point, together with a higher high temperatures will be relatively short, while the temperatures
ratio of ultimate-to-yield stress and greater ductility. At elevated reached may exceed 1000 ◦ C. Additionally, owing to the low prob-
temperatures stainless steel generally exhibits better retention of ability of occurrence of fire, large plastic deformations are tolera-
strength and stiffness in comparison to carbon steel. For a struc- ble in the structural members, provided overall structural collapse
can be avoided. General background information related to the be-
ture under fire conditions, these material properties are beneficial.
haviour of steel structures at elevated temperatures and guidance
Austenitic stainless steel, in particular, shows the best combination
on design for fire safety may be found in [9,10].
of strength, oxidation resistance and elevated temperature proper-
Appropriate assessment of the fire resistance of stainless
ties for long service, high temperature industrial applications and
steel structures depends largely on the ability to accurately pre-
dict the material response at elevated temperature. This pa-
per presents an overview and reappraisal of existing pertinent
∗ Corresponding author. research, proposes strength and stiffness reduction factors at ele-
E-mail address: Leroy.gardner@imperial.ac.uk (L. Gardner). vated temperatures for a range of grades of stainless steel, some of
0143-974X/$ – see front matter © 2010 Elsevier Ltd. All rights reserved.
doi:10.1016/j.jcsr.2009.12.016
L. Gardner et al. / Journal of Constructional Steel Research 66 (2010) 634–647 635
Notation
k0.2,θ σ0.2,θ /σ0.2
k2%,θ Factor for determining σt2.0,θ
kE ,θ Eθ /E
ku,θ σu,θ /σu
ky,θ σt2.0,θ /σ0.2
E Young’s modulus at room temperature
E0.2 Tangent modulus at the 0.2% proof stress at room
temperature
E0.2,θ Tangent modulus at the 0.2% proof stress at elevated
temperature θ
Eθ Young’s modulus at elevated temperature θ
n Ramberg–Osgood (R–O) exponent at room temper-
ature
n00.2,1.0 Exponent stage 2 of compound R–O formulation at Fig. 1. Strength reduction factors for carbon steel and stainless steel at elevated
temperatures.
room temperature
nθ Ramberg–Osgood exponent at elevated tempera-
tures
n0θ Exponent stage 2 of compound R–O formulation at
elevated temperatures
θ Temperature
ε Strain
εt0.2 Total strain corresponding to σ0.2
εt1.0 Total strain corresponding to σ1.0
εu,θ Ultimate strain at elevated temperature θ
σ Stress
σ0.2 0.2% proof strength at room temperature
σ1.0 1.0% proof strength at room temperature
σ0.2,θ 0.2% proof strength at elevated temperature θ
σt2.0,θ Strength at 2% total strain at elevated temperature
θ
σu Ultimate tensile strength at room temperature
σu,θ Ultimate tensile strength at elevated temperature θ Fig. 2. Stiffness reduction factors for carbon steel and stainless steel at elevated
temperatures.
Fig. 4. 0.2% strength reduction factors k0.2,θ for different stainless steel grades from Fig. 5. Ultimate strength reduction factors ku,θ for different stainless steel grades
EN 1993-1-2 and Euro Inox/SCI design manual for structural stainless steel. from EN 1993-1-2 and Euro Inox/SCI design manual for structural stainless steel.
An alternative approach to the material modelling of stainless properties can vary markedly between different grades, but this
steel at elevated temperatures was proposed by Chen and has to be justified with sufficient test data and balanced against
Young [22], whereby the compound Ramberg–Osgood material ease of design.
model [34,35], which is now widely adopted at room temperature,
was recalibrated for elevated temperatures. Good agreement 3.2. Basis for derivation of strength reduction factors
was reported between the observed stress–strain behaviour and
the compound Ramberg–Osgood formulation when experimental 3.2.1. Testing techniques
values for the key material parameters were employed. A modified Elevated temperature material testing may be conducted using
compound Ramberg–Osgood expression, which provides greater isothermal or anisothermal techniques. At high temperatures,
accuracy than existing models and utilises the material parameters above about 400 ◦ C, creep strains become increasingly influential,
generally resulting in lower reduction factors being obtained
currently employed for fire design in Eurocode 3, is proposed
from transient tests than steady state tests. The isothermal and
herein.
anisothermal tests reported by Ala-Outinen [18] and Ala-Outinen
and Oksanen [3], together with those presented by Sakumoto [20],
3. Strength and stiffness reduction factors at elevated temper-
allow a direct comparison between the results obtained for
atures stainless steel from these two testing techniques. With reference
to the 0.2% proof strength, the authors of both of the above studies
3.1. Introduction indeed observed lower reduction factors from anisothermal tests,
but at higher strains the differences were small. Under fire
Material properties at elevated temperatures form an essential conditions, high strains are tolerable, reflected by frequent use of
part of structural fire modelling and design. Guidance on stainless the strength at 2% strain for elevated temperature design, and on
steel material properties at elevated temperature, including this basis, Kirby and Preston [36] argued that data derived from
strength and stiffness reduction factors and description of the either testing technique may be used to predict the behaviour of
stress–strain response, is provided in EN 1993-1-2 (2005) [15] steel elements in fire.
and in the Euro Inox/SCI Design Manual for Structural Stainless The rate of testing is also important, and for derived strength
Steel [16]. The key parameters i.e. 0.2% proof stress σ0.2,θ , stress reduction factors to be representative, the rate of temperature
at 2% total strain σt2.0,θ , ultimate stress σu,θ and Young’s modulus increase employed during testing should broadly match that expe-
Eθ at an elevated temperature θ are typically expressed as a rienced by structural members in fires. The rates of temperature in-
proportion of the corresponding room temperature properties, crease utilised in the transient tests reviewed herein were between
with the exception of the stress at 2% total strain, which is generally 5 ◦ C/min and 10 ◦ C/min, which approximates the rate of temper-
normalised by the room temperature 0.2% proof strength, since this ature increase in protected steelwork in fire. This is appropriate for
is the accepted design strength for general structural calculations structural carbon steel, which is rarely used unprotected, but this is
and is widely available. not the case for stainless steel, where use in exposed unprotected
structural applications is commonplace, and thus the rate of tem-
In this section, all available elevated temperature material test
perature development is considerably higher and the influence of
results on stainless steel alloys are analysed in order to obtain
creep less significant. Strength reduction factors obtained for stain-
accurate strength reduction factors (k0.2,θ = σ0.2,θ /σ0.2 , ku,θ =
less steel by anisothermal testing at the relatively low temperature
σu,θ /σu ), a factor k2%,θ (denoted g2,θ the in the Euro Inox/SCI development rates reported in the literature may therefore be ex-
Design Manual [16]) used to determine the elevated temperature pected to be conservative for practical fire situations.
strength at 2% total strain (see Eq. (5)) and stiffness reduction factor Regarding the testing techniques used for establishing existing
(kE ,θ = Eθ /E). An additional objective was to extend the range of design guidance, the strength reduction factors provided for
grades covered by current structural design guidance, while also carbon steel in EN 1993-1-2 [15] were developed on the basis of
rationalising the number of strength reduction factors provided to anisothermal testing, while those provided for stainless steel [15,
designers by grouping grades that exhibit similar characteristics. 16] were derived on the basis of both isothermal and anisothermal
A total of eight sets of reduction factors (see Figs. 4 and 5) are testing.
currently provided for stainless steel compared to a single set for Given the above described observations and to maintain con-
carbon steel; five sets of reduction factors are given in EN 1993- sistency with the manner in which current strength reduction fac-
1-2 [15] and seven sets (four of which are the same as the EN tors [15,16] were obtained, while also maximising the usage of
1993-1-2 sets) are given in the Euro Inox/SCI Design Manual for the limited available data for stainless steel, both isothermal and
Structural Stainless Steel [16]. A number of sets of reduction factors anisothermal test results will be considered for the derivation of
are appropriate for stainless steel since the elevated temperature strength reduction factors in this study.
638 L. Gardner et al. / Journal of Constructional Steel Research 66 (2010) 634–647
Fig. 7. Proposed 0.2% strength reduction factors k0.2,θ , for different stainless steel grades.
Table 1
0.2% strength reduction factors at elevated temperatures k0.2,θ = σ0.2,θ /σ0.2 for all stainless steel grades.
Temp θ (◦ C) 1.4301 1.4318 1.4818 1.4401/4 1.4541 1.4571 1.4362 1.4462 1.4162 1.4003 1.4318 C850 1.4571 C850
20 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00
100 0.80 0.76 0.76 0.86 0.87 0.89 0.83 0.86 0.79 1.00 0.86 0.96
200 0.67 0.64 0.63 0.72 0.72 0.82 0.75 0.72 0.67 1.00 0.77 0.95
300 0.62 0.58 0.58 0.67 0.68 0.77 0.69 0.67 0.63 0.98 0.69 0.92
400 0.58 0.52 0.56 0.62 0.63 0.72 0.58 0.62 0.59 0.91 0.68 0.89
500 0.53 0.48 0.54 0.59 0.60 0.69 0.43 0.56 0.51 0.80 0.65 0.83
600 0.48 0.44 0.52 0.58 0.55 0.65 0.27 0.45 0.40 0.45 0.54 0.81
700 0.39 0.37 0.46 0.50 0.50 0.59 0.14 0.28 0.26 0.19 0.40 0.60
800 0.27 0.24 0.35 0.40 0.42 0.51 0.07 0.17 0.14 0.13 0.23 0.35
900 0.15 0.16 0.18 0.19 0.26 0.29 0.04 0.09 0.05 0.10 0.11 0.10
1000 0.06 0.09 – 0.10 0.18 0.15 – 0.02 0.01 0.07 – –
1100 – 0.05 – – 0.07 – – – – – – –
640 L. Gardner et al. / Journal of Constructional Steel Research 66 (2010) 634–647
Fig. 7. (continued)
Table 2
Ultimate strength reduction factors at elevated temperatures ku,θ = σu,θ /σu for all stainless steel grades.
Temp θ (◦ C) 1.4301 1.4318 1.4818 1.4401/4 1.4541 1.4571 1.4362 1.4462 1.4162 1.4003 1.4318 C850 1.4571 C850
20 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00
100 0.86 0.76 0.96 0.92 0.82 0.88 0.94 0.93 0.99 0.94 0.71 0.94
200 0.77 0.68 0.88 0.87 0.73 0.81 0.87 0.87 0.96 0.88 0.61 0.88
300 0.74 0.62 0.83 0.85 0.71 0.79 0.79 0.85 0.91 0.86 0.60 0.84
400 0.74 0.59 0.82 0.84 0.70 0.79 0.70 0.82 0.83 0.83 0.57 0.82
500 0.68 0.55 0.79 0.80 0.68 0.77 0.59 0.72 0.70 0.81 0.53 0.79
600 0.59 0.49 0.69 0.73 0.61 0.71 0.47 0.58 0.54 0.42 0.45 0.72
700 0.43 0.38 0.53 0.55 0.48 0.57 0.33 0.40 0.36 0.21 0.34 0.53
800 0.26 0.25 0.35 0.34 0.33 0.38 0.20 0.23 0.22 0.12 0.24 0.38
900 0.14 0.12 0.21 0.18 0.19 0.23 0.09 0.13 0.12 0.11 0.10 0.20
1000 0.07 0.09 0.10 0.09 0.11 0.10 0.04 0.04 0.07 0.09 – –
1100 – 0.05 – – 0.07 – – – – – – –
L. Gardner et al. / Journal of Constructional Steel Research 66 (2010) 634–647 641
Fig. 8. Proposed ultimate strength reduction factors ku,θ for different stainless steel grades.
Table 3
k2%,θ factors to predict σ2.0,θ at elevated temperatures for all stainless steel grades.
Temp θ (◦ C) 1.4301 1.4318 1.4818 1.4401/4 1.4541 1.4571 1.4362 1.4462 1.4162 1.4003 1.4318 C850 1.4571 C850
20 0.29 0.18 0.21 0.24 0.16 0.25 0.46 0.37 0.28 0.37 0.21 0.36
100 0.22 0.21 0.23 0.24 0.25 0.25 0.26 0.33 0.23 0.37 0.24 0.36
200 0.23 0.22 0.22 0.24 0.25 0.25 0.18 0.37 0.21 0.37 0.25 0.36
300 0.23 0.22 0.19 0.24 0.24 0.24 0.23 0.40 0.22 0.37 0.24 0.36
400 0.25 0.21 0.17 0.21 0.21 0.22 0.35 0.37 0.24 0.42 0.24 0.36
500 0.26 0.24 0.15 0.20 0.21 0.21 0.47 0.36 0.26 0.40 0.25 0.36
600 0.30 0.25 0.16 0.19 0.21 0.21 0.52 0.45 0.29 0.45 0.25 0.36
700 0.30 0.25 0.19 0.24 0.29 0.25 0.49 0.53 0.31 0.46 0.26 0.37
800 0.39 0.21 0.28 0.35 0.27 0.35 0.35 0.48 0.34 0.47 0.25 0.39
900 0.28 0.05 0.29 0.38 0.21 0.38 0.12 0.39 0.34 0.47 0.25 0.40
1000 – 0.05 – 0.40 – 0.40 – 0.44 0.22 0.47 – –
1100 – 0.13 – 0.40 – 0.40 – – – 0.47 – –
642 L. Gardner et al. / Journal of Constructional Steel Research 66 (2010) 634–647
Fig. 8. (continued)
Table 4
0.2% strength reduction factors at elevated temperatures k0.2,θ = σ0.2,θ /σ0.2 for the proposed groups.
Table 5
Ultimate strength reduction factors at elevated temperatures ku,θ = σu,θ /σu for the proposed groups.
Table 6
k2%,θ reduction factors at elevated temperatures to predict σ2.0,θ for the proposed groups.
4. Material modelling
Fig. 10. Comparison between the measured stress–strain curve and the basic
4.1. Material modelling at room temperature Ramberg–Osgood material model for an austenitic grade 1.4301 tensile coupon
with σ0.2 = 296 N/mm2 and n = 5.8.
At room temperature, stainless steel exhibits a rounded
stress–strain response with no sharply defined yield point, which applications, requires one less material parameter and may be ap-
is in contrast to the well defined yield point and characteris- plied to the description of compressive as well as tensile material
tic yield plateau of carbon steel. At elevated temperatures, the behaviour.
yield point of carbon steel tends to be less pronounced and the
σ σ n
stress–strain curve becomes more rounded, whilst the basic form ε= + 0.002 for σ ≤ σ0.2 (7)
of the stress–strain of stainless steel remains similar to that at room E σ0.2
temperature. The origins of many of the recently proposed ma- σ − σ0.2 σ1.0 − σ0.2
terial models for stainless steel lie in the early work of Ramberg ε = + εt1.0 − εt0.2 −
E0.2 E0.2
and Osgood [38]. In 1943, the widely used three-parameter Ram- n00.2,1.0
σ − σ0.2
berg–Osgood model was proposed to describe the nonlinear be-
× + εt0.2 for σu > σ > σ0.2 (8)
haviour of aluminium. This was later modified by Hill [39] resulting σ1.0 − σ0.2
in the familiar expression of Eq. (6).
where σ0.2 and σ1.0 are the 0.2% and 1% proof stresses respectively,
σ σ
n σu is the ultimate tensile strength, εt0.2 and εt1.0 are the total strains
ε = + 0.002 (6) corresponding to σ0.2 and σ1.0 , E0.2 is the tangent modulus at σ0.2
E σ0.2 and n and n00.2,1.0 are the exponential constants to define the de-
where n is the exponential coefficient to take account of the non- gree of the material nonlinearity. A more detailed review of previ-
linearity. The basic Ramberg–Osgood model (Eq. (6)) may also be ous material models, together with an assessment of their relative
applied to the modelling of stainless steel stress–strain behaviour, advantages and limitations, has been performed elsewhere [43].
but becomes inaccurate beyond the 0.2% proof stress, as illustrated Table 7 lists the proposed compound Ramberg–Osgood coef-
in Fig. 10. This observation led to the proposal [34] and the modi- ficients n and n00.2,1.0 for different stainless steel grades at room
fication and development of [35,40–42], the two-stage compound temperature, which were obtained by analysing all available ma-
Ramberg–Osgood material model. The initial concept of the two- terial test results [44].
stage model was that the basic Ramberg–Osgood expression was
adopted up to the 0.2% proof stress, and beyond the 0.2% proof 4.2. Material modelling at elevated temperatures
stress and up to ultimate stress, a second Ramberg–Osgood curve
was used. The origin of the second curve was defined at the 0.2% For design, accurate representation of the elevated temperature
proof stress, and continuity of magnitude and gradient was en- material stress–strain response may generally not be necessary.
sured at the transition point. A modified version of this model, However, for detailed insight into the response of stainless steel
whereby the second Ramberg–Osgood curve passed through the structures in fire, accurate material modelling is essential, and
1.0% proof stress instead of the ultimate stress was proposed is sought herein. The proposed material model for stainless
[40,41]. This model, represented by Eqs. (7) and (8), provides steel at elevated temperatures is based on the compound
greater accuracy at strains associated with common structural Ramberg–Osgood concept, and is thus of a similar form to Eqs. (7)
L. Gardner et al. / Journal of Constructional Steel Research 66 (2010) 634–647 645
Fig. 12. Proposed material models for austenitic grade 1.4301 at elevated
Fig. 11. Schematic representation of the proposed material model at elevated temperatures.
temperatures.
Table 7
Compound Ramberg–Osgood parameters obtained from coupon test results at room
temperature.
Type Grade Forming Tension/ n n00.2,1.0 σ1.0 /σ0.2
process Compression
σ σ
nθ
ε= + 0.002 for σ ≤ σ0.2,θ (9)
Eθ σ0.2,θ
σ − σ0.2,θ σt2.0,θ − σ0.2,θ
ε = + 0.02 − εt0.2,θ −
E0.2,θ E0.2,θ
n0θ
σ − σ0.2,θ
× + εt0.2,θ for σu,θ > σ > σ0.2,θ (10) Fig. 14. Stress–strain curves predicted using EN 1993-1-2 [15] guidelines for
σt2.0,θ − σ0.2,θ austenitic grade 1.4301 at elevated temperatures.
Table 8
Ramberg–Osgood parameters for stainless steel alloys at elevated temperatures.
Grade Exponent Compound Ramberg–Osgood parameters nθ and n0θ at elevated temperatures (◦ C)
20 100 200 300 400 500 600 700 800 900 1000
nθ 7.5 9.0 6.5 6.5 6.5 7.5 7.0 6.5 4.0 3.0 1.2
1.4301
n0θ 2.0 2.3 1.9 2.0 2.0 1.8 2.0 2.2 1.9 2.6 3.0
nθ 8.0 – 10.0 8.0 9.0 7.0 9.0 9.0 8.0 – –
1.4401/4
n0θ 1.8 – 2.3 2.6 1.7 1.8 1.9 1.9 4.2 – –
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Acknowledgements stainless steel hollow section columns. Engineering Structures 2009;31(12):
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[26] Ala-Outinen T, Viherma R, Nilimaa H. Work package 6: Elevated temperature
The authors would like to thank Outokumpu for the provision properties—Isothermal material tests. ECSC project ‘Structural design of cold
of test data and technical input, as well as Nancy Baddoo of the worked austenitic stainless steel’. Contract no. 7210-PR-318. VTT building
and transport. Finland; 2003.
Steel Construction Institute and Alan Harrison of the British Stain- [27] Conrad F. Work package 6: Elevated temperature properties—Anisothermal
less Steel Association for technical advice. The authors also would material tests. ECSC project ‘Structural design of cold worked austenitic
like to acknowledge the Basque Government (Department of Ed- stainless steel’. Contract no. 7210-PR-318. Ugine & Alz–Arcelor group; 2003.
[28] Zhao B, Blanguernon A. Work package 6: Elevated temperature properties—
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under the overseas post-doctoral development scheme in 2009. structural members under standard fire. ECSC project ‘Structural design of
cold worked austenitic stainless steel’. Contract no. 7210-PR-318. CTICM.
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