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4-1.

Asphalt Mixture and Mix Design


- General Topics and Marshall Test -
Asphalt Concrete Mixture

Material Properties
 Binder (Asphalt Binder)
 Aggregate
 Modifier

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Petroleum Distilling Plant

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Classification of Bituminous Binder (1)

Asphalt Cement
 Semi-Solid, used for aggregates in pavement
construction
Cutback Asphalt
 Rapid curing: Gasoline or naphtha
 Tack coat or surface treatment
 Medium curing: Kerosene
 Prime coast, stockpile patching mixture
 Slow curing: Diesel or the other gas oil
 Prime Coat, stockpile patching mixture

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Classification of Bituminous Binder (2)

Emulsified Asphalt
 Asphalt cement + water + emulsifier
 Rapid setting: Surface treatment
 Medium Setting: Open graded cold asphalt mixtures
 Slow Setting :Tack coat, fog seal, dense graded cold mixture,
and slurry seal
Blown Asphalt
 Roofing, automobile undercoating
Road Tar
 Obtained from coal, rarely used in pavement
construction

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Property of Asphalt Materials (1)

Consistency (Temperature susceptibility)


 Variation of consistency with temperature and at
a specified temperature
Aging and temperature sustainability
 Changes in properties due to weathering
 Oxidation
 Volatilization

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Property of Asphalt Materials (2)

Rate of curing
 Increase in consistency due to evaporation
 Rate of curing of cutbacks
 Volatility of the solvent
 Quantity of solvent in the cutback
 Consistency of the base material
 Temperature
 Ratio of surface area to volume
 Wind velocity across exposed surface
Resistance to water action
Temperature effect on volume of asphalt

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Tests for Asphalt Binder (1)

Consistency Test
 Kinematic Viscosity Test
 Rotational Viscosity Test
Float Test
Penetration Test
Softening Point Test
Durability Test

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Tests for Asphalt Binder (2)

Rate of Curing
 Distillation Test for Cutbacks
Rheological Test
 Dynamic Shear Test
 Bending Creep Test
Other General Test
 Specific Gravity Test
 Ductility Test
 Solubility Test
 Flash-Point Test
 Loss-on-Heating Test
 Water Content Test

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Kinematics Viscosity Test

Capillary viscometer tube


 Zeitfuch’s cross-arm viscometer
 Asphalt Institute vacuum viscometer
 Cannon Manning vacuum viscometer

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Zeitfuchs Cross-Arm Viscometer

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The Asphalt Institute Vacuum Viscometer

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Cannon-Manning Vacuum Viscometer

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Penetration Test

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Penetration Test

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Softening Point Test

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Binder Grading System

Penetration: 40-50, 50-70, 85-100, 120-150,


200-300
Viscosity
 AC5, AC10, AC20, AC30, AC40
 RTFO (Rolling Thin Film Oven Test)
 AR-1000, AR-2000, …, AR-16000
PG Grade (SHRP)

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Penetration Grading System (1)

Five Penetration Grade


40-50, 60-70, 85-100, 120-150, 200-300
Advantages
 77F : average pavement temperature,
close relationship with lower temp.
properties

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Penetration Grading System (2)

 Low cost
 Available to find temperature susceptibility
Disadvantages
 Not a mechanical property

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Viscosity Grading System (1)

Poise : Standard unit of measurement for viscosity:


Obviously less poise means less viscous asphalt. AC
2.5 is softer than AC 40(4000 poise) @ 140 F
Advantages
 Viscosity: Fundamental Property
 Wide Range of Environment
 140F : Critical for pavement performance

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Viscosity Grading System (2)

 Reduce overlap
 Wide range of test instrument is available
 temperature susceptibility is measured
Disadvantages
 Deceptive performance
 Not adequate to safeguard against low temp cracking
 Time is longer
 Slightly more expensive

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Viscosity Grading System (3)

AR viscosity Grading System


 Western US
 Viscosity of the aged residual from TFOT
 AR-1000, AR-2000, AR-4000, AR-8000, AR-
16000
Advantages:
 Reasonable uniform behavior

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Asphalt Mixtures

Hot Mix, Cold Laid Asphalt Concrete


Cold Mix, Cold Laid Asphalt Concrete
Hot Mix, Hot Laid Asphalt Concrete

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Aggregate Gradation

Crushed rock, sand, & filler


>No 8 <No 8 <No 200
(2.36mm) (75 m)
Composition of AP mixture
Mechanical stabilization

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Examples of Composition of Asphalt Paving
Mixtures

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Determining proportions of different a aggregate to
obtain a required gradation

Specification
Available material
Trial mix
 CA: 55%
 FA: 39%
 Filler: 6%
 Result:

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Determining proportions of different a aggregate to
obtain a required gradation

Calculation
P  aA1  bA2  cA3  ......
Analysis: Yes or No
Graphical method or LP method

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Required limits for mineral aggregates gradation and mix composition for an
asphaltic concrete

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Sieve analysis of available materials

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Computation of percentages of different aggregate sizes

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Hot Mix Asphalt Concrete (HMA) Mix Designs

Objective:
 Develop an economical blend of aggregates and
asphalt that meet design requirements
Historical mix design methods
 Marshall
 Hveem
New
 Superpave gyratory

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Requirements in Common

Sufficient asphalt to ensure a durable


pavement
Sufficient stability under traffic loads
Sufficient air voids
 Upper limit to prevent excessive
environmental damage
 Lower limit to allow room for initial
densification due to traffic
Sufficient workability
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Volumetrics

All matter has mass and occupies


space.
Volumetrics are the relationships
between mass and volume
Marshall & Superpave mix design
based on aggregate and mixture
volumetrics

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토질 역학에서 이미 배웠음

Two tests are needed


 Coarse aggregate (retained on the
4.75 mm sieve)
 Fine aggregate (passing the 4.75
mm sieve)

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Coarse Aggregate Specific Gravity

ASTM C127
 Dry aggregate
 Soak in water for 24 hours
 Decant water
 Use pre-dampened towel to get SSD
condition
 Determine mass of SSD aggregate in bucket
 Determine mass under water
 Dry to constant mass
 Determine oven dry mass
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Coarse Aggregate Specific Gravity
Coarse Aggregate Specific Gravity
Coarse Aggregate Specific Gravity

Gsb = A / (B - C)
 A = mass oven dry
 B = mass SSD
 C = mass under water
Gs,SSD = B / (B - C)
Gsa = A / (A - C)
Water absorption capacity, %
 Absorption % = [(B - A) / A] * 100
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Phase Diagram in solid

V = (mass) / (Gs gw)

Volume Mass (Weight)


Asphalt
Vpp permeable Vap Wap
Water voids
permeable
voids Vpp-Vap
WT

Aggregate
Vs Solids
Ws

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Specific Gravity in Solid

Apparent specific gravity


 Gsa = Ws / Vs* gw
Bulk specific gravity
 Gsb = Ws / (Vs+Vpp)* gw
Effective specific gravity
 Gse = Ws / (Vs+Vpp-Vap)* gw

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Bulk, effective, and apparent specific gravities; air void; and effective asphalt content
in compacted asphalt paving mixture

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Weight-volume relationship & its parameter

VV Air 0

Vbe Effective AP wbe


Vb wb
wT
VT Vba Absorbed AP wba

Vs Aggregate ws

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Specific Gravity

Maximum Specific Gravity


 Assume no air voids in AC
 Gmm in Lab(ASTM D2041)
 Called rice specific gravity or theoretical max density

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Maximum specific gravity of paving mixture

Ws  Wb
Gmm  Gb = specific gravity of asphalt
Vs  Vv  Vb
Pb = percent by weight of asphalt in paving
WT mixture

Ws Wb Ps = percent by weight of aggregates in
 paving mixture
Gse Gb
WT

WT (1  Pb ) WT ( Pb )

Gse Gb
100

 Ps P
 b 
 G Gb 
 se
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Weight-volume relationship & its parameter

Effective Asphalt
 Percent void in compacted Mineral Aggregate
(Void in Mineral Aggregate)
VV  Vbe
VMA   100
VT
Voids filled with Asphalt(%)
Vbe
VFA   100
Vbe  VV
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Calculation of VTM, VMA, VFA

VV  Vbe
VMA  100
VT
Ws  WT  WT  Pb
VT  Vs
 100
VT  simplifying
 Vs  Gmb Ps
  1    100 VMA  100 
 VT  Gsb
 Ws 
 Gsb 
 1    100
WT
 
 Gmb 
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Percent air voids in compacted mixture
(VTM, % air)

VV
Pa  VTM   100, VV  VT  Vbe  Vs
VT
 1 
 VT  Vbe  Vs   Vbe  Vs   VT 
VTM     100   1    100   1    100
 VT   VT   1 
 V V 
 be s 
 WT 
 VT   G 
 1    100  1  mb G   100
 WT   mm 

 Vbe  Vs  

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Voids filled with asphalt(VFA)

VMA  VTM
VFA   100
VMA

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Asphalt absorption

  Ws Ws  
    Gb 
 Wap   Vap  Gb    Gsb Gse    100
Pba    100    100  
 Ws   Ws  Ws 
 
 
 Gse  Gsb 
Pba  100     Gb
 Gsb  Gse 

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Effective asphalt content

Pba
Pbe  Pb  Ps
100

Pba = amount of asphalt absorbed as a


percentage of the total weight of aggregates

Pb = percent by weight of asphalt in paving


mixture

Ps = percent by weight of aggregates in


paving mixture

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창의적인 숙제

기존의 방법론은 다양한 값의 G를 요구하고


있습니다
 실제 플랜트에서 이 값들을 통제하는 것은 불가함
 둘째 이 값들을 측정하는 것이 재료별로 날짜 별로
상이 함
다르게 이 속성을 체크하는 것이 가능?
 입도, 부피, 무게, 분포,

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MARSHALL
MIX
DESIGN

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Marshall Mix Design

Developed by Bruce Marshall for the


Mississippi Highway Department in the
late 30’s
WES began to study it in 1943 for WWII
 Evaluated compaction effort
 No. of blows, foot design, etc.
 Decided on 10 lb.. Hammer, 50
blows/side
 4% voids after traffic
Initial criteria were established and
upgraded for increased tire pressures
and loads
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Marshall Mix Design

Mashall method procedure


 4”D & 2½“ height
 Heating  Mixing  Compacting  Stability
flow test  Density void analysis

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Mashall Procedure

Range of prescribed limit


0.5% increment
Ex) 5~7% spec, 5, 5.5, 6, 6.5 ,7
Three specimens
Select and test aggregate, Amount of
aggregate: 1.2Kg
Dry agg @ 105도C ~ 110도C
 Until constant weight

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Mashall procedure

Develop trial blends


 Heat and mix asphalt cement and aggregates
 Compact specimen (100 mm diameter)
Select and test asphalt cement
 Establish mixing and compaction temperatures
 Asphalt kinematic viscosity 208 30 centistockes

Compactive effort: 35, 50, 75
(18” distance) : both sides
Bulk density of the sample
 Weighty the sample in air & in water (paraffin coating if necessary)

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Mashall Procedure

Bulk density of the sample

Where
Wa
Gmb  wa = weight in air
Wa  Ww
ww = weight in water

Maximum specific gravity of loose mix


Water bath with 60도C  for 30~40min
1C
Total time: < 30 sec

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Automatic Marshall Hammer
Mixing/Compaction Temps
Viscosity, Pa s
10
5

1
.5
.3 Compaction Range
.2 Mixing Range

.1
100 110 120 130 140 150 160 170 180 190 200
Temperature, C

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Marshall Mix Design Tests

Stability and flow


 60oC water bath (30 to 40 minutes)
 50 mm/min loading rate
 Max. load = uncorrected stability
 Corresponding vertical deformation =
flow

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Stability vs. flow

stability

flow

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Marshall Stability and Flow
Marshall Test Properties
% Air voids

VMA
Unit Wt.

AC weight(%) AC
weight(%) Asphalt Content, %
Stability

Flow

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AC weight(%) Highway Engineering & AAC weight(%)
irport Research Taskforce
Marshall Design Criteria

Light Traffic Medium Traffic Heavy Traffic


ESAL < 104 10 4 < ESAL< 10 ESAL > 106
Compaction 35 50 75

Stability N (lb.) 3336 (750) 5338 (1200) 8006 (1800)

Flow, 0.25 mm (0.1 in) 8 to 18 8 to 16 8 to 14

Air Voids, % 3 to 5 3 to 5 3 to 5

Voids in Mineral Agg.


(VMA) Varies with aggregate size

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아스팔트 표층-재료

아스팔트 혼합물의 품질기준


혼합물의 종류 WC – 1 ~ 4 WC - 5

안 정 도 (kg) 750 이상 600 이상


공 극 률 (%) 3~6 3~6
포 화 도 (%) 65 ~ 80 65 ~ 80
흐 름 값 (1/100cm) 20 ~ 40 15 ~ 40
수침 마샬 잔류안정도 (%) 75 이상 75 이상
다짐회수 75 회 75 회

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Marshall Design Use of Data
Asphalt Institute Procedure
Air Voids,
Stability Unit Wt.
%

4%

Asphalt Content, % Asphalt Content, % Asphalt Content, %

Target optimum asphalt content = average

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Marshall Design Use of Data
Asphalt Institute Procedure
Flow VMA, %

Upper limit OK
OK
Minimum
Lower Limit

Asphalt Content, % Asphalt Content, %

Use target optimum asphalt content


to check if these criteria are met
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Marshall Design Use of Data
NAPA Procedure

Air Voids,
%

4%

Asphalt Content, %

Target optimum asphalt content =

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the asphalt content
H
at 4%A air
E R
voids
T
ighway ngineering & irport esearch askforce
Marshall Design Use of Data
NAPA Procedure
Stability

OK

Asphalt Content, %

The target stability is checked

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Marshall Design Use of Data
NAPA Procedure
Flow VMA, %

Upper limit OK
OK
Minimum
Lower Limit

Asphalt Content, % Asphalt Content, %

Use target optimum asphalt content


to check if these criteria are met
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Trial mix can be adjusted

Low void & low stability


 VMA can be increased by more CA
 Reducing asphalt content, but care
should be taken
Low void & satisfactory stability
 Cause reorientation of particle
 {instability flowing}
 Adding more aggregates
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Trial mix can be adjusted

High void & satisfactory stability


 Air & water  premature handling
 Increasing the amount of mineral dust filler
Satisfactory void & low stability
 Low quality aggregate
High void & Low stability
 Adjust voids(1 step)
 Improve aggregate quality (2 step)
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Marshall Design Method

Advantages
 Attention on voids, strength, durability
 Inexpensive equipment
 Easy to use in process control/acceptance

Disadvantages
 Impact method of compaction
 Does not consider shear strength
 Load perpendicular to compaction axis

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마샬 배합 설계 예

다음 조건을 만족하는 경우의 AP함량은?


 Heavy traffic
 Aggregate characteristic: Table 18.8
 Marshall test Table 18.9
 Optimum AP content?

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Aggregate characteristic

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Marshall test

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i) average bulk specific gravity for 5%

1 1325.6 1325.4 1325.0 


Gmb     
3  1325.6  780.1 1325.4  780.3 1325.0  779.8 
1
  2.43  2.43  2.43
3
 2.43
Bulk density = 2.43 X 62.4 = 151.6lb/ft3
For 5.5%, 6%, 6.5%, 7%, we get 2.46, 2.48, 2.47, 2.45 (or
153.5, 154.8, 154.1, 152.9)

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단위 중량과 AP함량

2.49

2.48

2.47

2.46
Unit weight

2.45

2.44

2.43

2.42

2.41

2.4
5 5.5 6 6.5 7
%

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ii) stability & flow

% stability flow
5.0 1458 7.2
5.5 1602 95
6.0 1550 11.2
6.5 1412 13.2
7.0 1200 15.7

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1800 18

1600 16

1400 14

1200 12

1000 10
stability

flow
800 8

600 6

400 4

200 2

0 0
5 5.5 6 6.5 7 5 5.5 6 6.5 7
% %

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iii) VMA VMA  100 
Gmb Ps
Gsb

For 5% Asphalt content,


Gmb = 2.43
Ps = 95.0 (total aggregate percent)
Since Pca, Pfa, Pmf = percent by weight of coarse

Pca  Pfa  Pmf aggregate, find aggregate, mineral filler, and


Gsb  respectively
Pca Pfa Pmf
  Gbca, Gbfa, Gbmf = bulk specific gravity of
corase aggregate, find aggregate, and mineral
Gbca Gbfa Gbmf filler, respectively.
And since
Pca=0.523 X 95.0=49.7
Pfa=0.396 X 95.0=37.6
Pmf=0.081 X 95.0=7.7, therefore

49.7  37.6  7.7


Gsb   2.69
49.7 37.6 7.7
 
2.65 2.75 2.7
Ps  (100  5)  95
2.43  95
VMA  100   14.18
2.69
For 5.5% AP  VMA=13.58
For 6.0% AP  VMA=13.34
For 6.5% AP  VMA=14.15
For 7.0% AP  VMA=15.30

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15.5

15

14.5

14
VMA

VMA
13.5

13

12.5

12
5 5.5 6 6.5 7
%

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iV) Air voids

Gmm  Gmb
Pa  100
Gmm
For 5% AP
2.54  2.43
Pa  100   4.33
2.54

Similarly 5.5, 6, 6.5, 7% 에서 Pa=3.91,


3.88, 3.50, 3.54
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5

4.5

3.5

3
Air void %

2.5

1.5

0.5

0
5 5.5 6 6.5 7
%

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V) Optimum asphalt content
1. Max. unit weight = 6.0%
2. Max. stability = 5.5%
3. 공기량 제한값의 평균에 근거한 양 =
(3+5)/2=4% 5.4% AC
4. Optimum AP content = (6+5.5+5.4)/3 = 5.6%

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5. 5.6%에서의 기준값(이전 그림)과
기준(specification;표 19.8)비교
Unit weight = 153.8 lb/ft
Stability = 1600lb >1500
Flow = 9.5 unit of 0.01” (8< <16)
Percent void = 3.9 (3< <5)
VMA = 13 ( >13 이상 19mm골재)

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Marshall Design Method
Advantages
 Attention on voids, strength, durability
 Inexpensive equipment
 Easy to use in process control/acceptance

Disadvantages
 Impact method of compaction
 Does not consider shear strength
 Load perpendicular to compaction axis

Page  90 Highway Engineering & Airport Research Taskforce

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