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Interdigitated Sensors: A Design Principle for Accurately Measuring the


Permittivity of Industrial Oils

Article  in  IEEE Sensors Journal · July 2017


DOI: 10.1109/JSEN.2017.2732942

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6232 IEEE SENSORS JOURNAL, VOL. 17, NO. 19, OCTOBER 1, 2017

Interdigitated Sensors: A Design Principle for


Accurately Measuring the Permittivity
of Industrial Oils
Alex Risos, Nick Long, Arvid Hunze, and Gideon Gouws

Abstract— An accurate measurement of the relative permit- TABLE I


tivity, ε r , of industrial oils using interdigitated dielectrometry T YPICAL VALUES OF THE R ELATIVE S TATIC P ERMITTIVITIES
sensors (IDS) is challenging due to the parasitic capacitance FOR S ELECTED O ILS AT R OOM T EMPERATURE
caused by the IDS spatial structure. In this paper, the investigated
IDS structure consists of a substrate, a ground plane, an insulat-
ing layer below the electrodes and a solder mask above the elec-
trodes having a periodicity of λ. This structure was simulated to
determine the influence on the expected values of capacitance C,
sensitivity S, and deviation D (accuracy) for typical values of ε r
for industrial oils. It is shown that for particular structure ratios
and values of ε r , the parasitic capacitance can be compensated
in order to provide an accurate measurement of ε r . A standard
rapid and cost efficient printed circuit board (PCB) technology
is used to manufacture an IDS based on the simulations to verify
the expected high accuracy in practice. Experiments conducted
with this IDS structure on both new and degraded oils showed a
high accuracy ≈99.5%, verifying the simulations. These results
have the potential to reduce the number of IDS design iterations
in order to carry out highly accurate and precise measurements.
This may go beyond the in-situ monitoring of oil degradation,
such as a number of related sensing applications employing
interdigitated sensor platforms.
Index Terms— Interdigitated dielectrometry sensor (IDS),
permittivity, tan delta, dissipation factor, acidity, oxidation,
aging/degradation, transformer/lubricant/hydraulic oil, in-situ/
online measurement.

I. I NTRODUCTION

O ILS play many roles in industry. They are used as


lubricants, hydraulic fluids, or as insulators and cooling
fluids in transformers. Particularly in the case of trans- Fig. 1. (a) A cross section view showing the general structure of the IDS.
former oils, the oil inevitably degrades with service time, (b) FEM simulation geometry of the IDS and boundary conditions. Depicted
are the relative permittivities and distances for each layer with the
losing the desired characteristics. This deterioration is linked IDS surrounded at a distance by a grounded boundary. Electric field
to the increase in oxidation, acidity, moisture and sludge lines (dotted) which contribute to the sensing are shown schematically.

Manuscript received June 30, 2017; accepted July 20, 2017. Date of publi-
cation July 27, 2017; date of current version September 8, 2017. This work content, affecting its lubricating or electrical breakdown
was supported in part by Ministry of Business, Innovation and Employment properties [1]–[3]. Thus oil quality monitoring can be a key
New Zealand acquired by the Robinson Research Institute as part of the element for predicting transformer failures and is therefore
Victoria University of Wellington under Grant RTVU 1304 and in part by the
ETEL Limited, Auckland. The associate editor coordinating the review of this highly desirable in the electrical distribution industry. A mea-
paper and approving it for publication was Prof. Tarikul Islam. (Corresponding sure of the relative permittivity, εr , has been shown to be
author: Alex Risos.) a good indicator of the oil condition [4]. The standard for
A. Risos is with the School of Chemical and Physical Sciences, Victoria
University of Wellington, Wellington 6012, New Zealand, and also insulating liquid measurements [5] specifies the procedure to
with the Robinson Research Institute, Victoria University of Wellington, measure εr for monitoring the oil condition. It is known that
Lower Hutt 5010, New Zealand (e-mail: alex.risos@protonmail.com). the εr value of oils increase with service time [1], [3], [5]–[10],
N. Long and A. Hunze are with the Robinson Research Institute,
Victoria University of Wellington, Lower Hutt 5010, New Zealand (e-mail: so that a measure of εr in theory enables the real time health
nick.long@vuw.ac.nz; arvid.hunze@vuw.ac.nz). monitoring of oil. Table 1 provides an overview of industrial
G. Gouws is with the School of Engineering and Computer Sciences, oils, their application and nominal εr values.
Victoria University of Wellington, Wellington 6012, New Zealand (e-mail:
gideon.gouws@vuw.ac.nz). The standard process in industry determining the condi-
Digital Object Identifier 10.1109/JSEN.2017.2732942 tion of an oil via εr is a time consuming and thus costly

1558-1748 © 2017 Crown Copyright


RISOS et al.: IDS: A DESIGN PRINCIPLE FOR ACCURATELY MEASURING THE PERMITTIVITY OF INDUSTRIAL OILS 6233

procedure [5]. Co-axial probes are commonly used for mea- simulated geometry depicted in Fig. 1b having sharp electrode
suring the permittivity. However, they are used at microwave boundaries. The electric field lines (dotted lines) represent
frequencies to determine the reflection coefficient for lossy schematically the sensing mechanism; these electric field lines
mediums such as water [16]. This method requires a prior penetrate the oil as well as dielectric layers, causing parasitic
calibration due to the two wire measurement principle causing capacitances [20]. The IDS structure employs a common
parasitic effects and has been reported to exhibit a maximum ground plane as this is believed to reduce major parasitic
accuracy of 94% at 1 GHz and 80% at 2.45 MHz [17]. capacitances (GND = 0 V ) [20], [31].
However, it has been shown that εr can potentially be measured The electrodes “VAC ” and “V0 ” with a periodicity of λ are
with interdigitated dielectrometry sensors (IDS) [18]–[22] in separated from this ground layer by an insulator layer with
order to facilitate an on-line measurement system. The use distance dins. A soldermask (an epoxy resin) is a standard
of IDS benefits from a capacitance scalability (i.e. using protection coating for PCBs, as for IDS in a liquid, certain
more electrodes to suit the measurement system) and four dielectrics can dissociate due to electrolysis or react with
wire impedance measurement principle. This is especially the electrode’s surface in other ways. In order to investi-
true when measuring impedances of insulating liquids at line gate its effects of the IDS figures of merits the soldermask
frequencies (∼50 Hz) as per the defined standard [5]; larger was considered with thickness dSM in the simulations. This
capacitances due to the material under test help to improve structure was simulated with the aid of the finite element
the signal to noise ratio in the measurement. Furthermore, method (FEM) to determine the impact of the spatial structure
a four wire measurement system is designed to be free of on the capacitance C by varying the ratios dins/λ, and dSM /λ
lead impedances through e.g. BNC measurement connectors. while changing εr .
Here, we particularly show how the IDS technology can be Simulations were performed for a structure of
improved by reducing parasitic capacitances using a special 20 electrodes (10 λ). The first figure of merit considered
design. in the simulation is the capacitance C, which is important
The insight provided by this work may be useful beyond for maximizing the signal to noise ratio (S/N). From this
the application of IDS structures for the measurement capacitance, the figure of merit sensitivity S is defined as:
of oil degradation, as these sensor platforms has been
shown by many workers to be suitable for measurements S = CIDS /εr, IDS . (2)
in a range of physical, chemical and biological sensing The deviation D from a reference value (accuracy) is
applications [23]–[27]. determined by the ratio of the IDS permittivity, εr,IDS , over
The value of εr can be readily determined by the ratio of the reference value εr,ref :
the IDS capacitance with oil vs. the IDS capacitance with air
where εr = Coil /Cair as εr,air ∼
= 1. D = (εr,ref − εr,IDS )/εr,ref , (3)
However, the measured value of Coil can be a result of
contributions from the dielectric liquid, the sensor structure with the measured permittivity by the IDS given by:
as well as the sensor environment. The value of permittivity εr,IDS = Coil,IDS /Cair,IDS (4)
calculated for the oil will thus be influenced by parasitic
capacitances of each measurement for oil Cparasitic, and for and the reference value, measured as:

air Cparasitic so that
εr,ref = Coil,ref /Cair,ref . (5)

εr = (Coil + Cparasitic )/(Cair + Cparasitic ), (1)
The value εr,ref is used in section III and was obtained via
where Coil/air = (1/V )ε0 ∫s1 Ed A with s1 is the upper a plane parallel test cell exhibiting a standard deviation and
surface of the V0 electrode and Cparasitic = (1/V )ε0 ∫s2 Ed A accuracy of λ ≤ 0.01%, as shown in Fig. 9. It represents
where s2 is the lower surface of the V0 electrode [28]. The a typical value of new, unused paraffinic oils as commonly
electrostatic potential between the electrodes was V = 1 in used as coolants in an electrical environment [2], see Table 1.
the simulations in section II, E is the electric field and ε0 is Thus it was used by the authors for testing and verifying the
the permittivity of free space. IDS simulations.
Indications for such parasitic capacitances of IDS were
observed in previous work [20] and [29]. The expected
increase of εr during the oil’s lifetime is generally about +5% II. FEM S IMULATIONS WITH C OMSOL M ULTIPHYSICS
to +10% [7]–[10], [30], which can easily be swamped by the The simulations in Comsol Multiphysics version 4.2 used
parasitic capacitance in the system. A more accurate IDS is electrostatics for a simplification as the conductivity for oil
thus needed to allow the measurement of a true value of εr at 50 Hz can be neglected [18]. The electrostatics module
and provide information on the state of degradation in an oil computes the potential field based on the Laplace equation by
over time. applying Dirichlet boundary conditions. The resulting surface
This paper identifies the parasitic capacitances of an charges on the electrodes VAC and V0 are used to compute
IDS in order to design an optimised IDS using printed circuit the capacitance. The geometry in Fig. 1 depicts the Dirichlet
board (PCB) technology measuring εr accurately. A cross FEM boundary held at zero potential (GND). This surrounds
sectional view of the IDS structure is shown in Fig. 1a. the IDS structure with spacing to the grounded structure
This model is transferred to the FEM simulation using the of 12.5λ. This is mimicking a grounded plane to left and
6234 IEEE SENSORS JOURNAL, VOL. 17, NO. 19, OCTOBER 1, 2017

to the right at infinity. Here, the deviation D in the sim- This does not appear to significantly affect the accuracy D as
ulations was obtained similar to Equation 3 through D = shown in Fig. 2f; it exhibits a similar behaviour as observed
(εr − εr,IDS )/εr , where εr,IDS is the permittivity calculated in Fig. 2c, exhibiting a steady decrease with increasing dSM /λ.
from Coil,IDS /Cair,IDS as a result of the FEM simulation with More specifically, D decreases throughout dSM /λ from approx-
the IDS structure. Therefore a comparison of the defined imately +10% down to -30%. This in turn also exhibits a zero
permittivity as entered in the simulation as material under test crossing for the deviation at around dSM /λ = 0.025.
above the IDS electrode structure (see Fig. 1) εr was possible. The third set of figures, Fig. 2g to Fig. 2i, shows the
The width of the electrode and the gap between each impact of varying dSM /λ and dins /λ on C, S and D when
pair of electrodes were equal as adopted from previous εr = 3.5 is held constant. Fig. 2g plots an increase in
designs [13], [18]–[21], [28], [31], [32]. The electrodes were capacitance C with increasing dins/λ while dSM /λ has a less
set to a potential of VAC = 1 V and V0 = 0 V . The significant effect on C. However, Fig. 2h demonstrates an
oil was located above the IDS geometry. The thickness of opposite behaviour as can be seen via the contour lines. The
the soldermask was modeled for values of dSM /λ = 0 sensitivity S generally increases with dins/λ but at high dSM /λ
to 0.1 and the insulator distance was varied from dins/λ = 0 this is a weak effect. The accuracy D was affected by both,
to 0.2. The oil layer, doil = h − (dSM + dins) ∼ = 25, was dSM /λ and dins/λ, Fig. 2i. In general, high values of dSM /λ
effectively infinite relative to the soldermask and insulator and dins /λ produce a large D of more than −25% in the
distances. These values are likely to be encountered in a typical negative space. However, small values of dSM /λ increase D
IDS design. In a standard PCB structure, the dielectrics of the with increasing dins /λ similar to Fig. 2c. It is possible to find
soldermask and insulator are a resin based type coating and a zero deviation for a certain combination of dSM and dins,
FR4 laminate which is a standard material and thus widely as well as whendSM and dins is equal to zero which would
available. The permittivity of FR4 is known to be ≈ 4.5 in kHz represent an IDS having no substrate dielectrics – as this is
regime [33], [34]. commonly assumed in approximations [32].
No information regarding the permittivity of the used solder- The simulations show that the spatial structure strongly
mask was available from the supplier (Pcbway.com, Shenzhen affects the figures of merit of an IDS. The soldermask
JDB Technology Co., Ltd, Shenzhen, China), therefore the per- decreases the sensitivity throughout as it provides a direct
mittivity value for the soldermask was approximated to 4.5 as parasitic capacitance in between the sensed oil and electrodes.
εr = 4 to 5 is a common value for epoxies in literature [35]. Increasing the insulator distance in turn increases C and S, as
Using this value has shown to give accurate results with a larger separation of the electrodes to the ground plane results
experimental observations in preceding research [29]. While in fewer field lines being pulled downwards to the ground. The
the relative permittivity of the soldermask εr,SM and insulator insulator thickness can control the accuracy while maintaining
εr,ins was held constant at 4.5, the permittivity of the oil, a high sensitivity.
εr , was varied from 2 to 5, covering a wide range of oil In order to facilitate a measurement of εr with high accuracy,
permittivities. Fig. 2 shows the results of our simulations one aim of the work was to find the design for an IDS with
presented as contour plots. the best possible accuracy, ideally D = 0.
The first set of simulations, Fig. 2a to Fig. 2c, show the For an experimental verification of these simulations,
impact that changes in εr and dins/λ have on C, S and D. the practical design for a possible IDS was informed with
The value of dSM /λ was held constant at 0.007 and the values the aid of the data shown in Fig. 2i. It can be seen clearly
of C, S and D were calculated as shown in Fig. 2a. The that a particular ratio of dins /λ is needed in order to achieve
results show an increase in the capacitance C as both εr and a high accuracy. With aid of this knowledge, a suitable
dins/λ increase. The sensitivity S is predominantly affected IDS measuring accurately a specific value of εr in practice can
by an increase in dins/λ, and is less sensitive to εr , as is seen be created. A new insulating oil having εr,ref = 2.1065 was
in Fig. 2b. The accuracy D, shown in Fig. 2c, is also primarily used to simulate this specific case, Fig. 5. This Fig. 5 shows
affected by dins/λ. At low values of dins/λ, D is rising for a similar pattern as Fig. 2i. With aid of the FEM simulations,
dins/λ ∼= 0.03 up to ≈ 15%, then follows a linear decrease it could be identified that the presence of a soldermask,
to −30 % at dins /λ ∼ = 0.2. This results in a zero cross- dSM , is detrimental to the sensitivity. Therefore, dSM was
ing at dins /λ ∼ = 0.075 resulting in high accuracy at this removed in the manufactured IDS. The thickness dins is fixed
ratio. by the manufacturer at ∼ = 120 μm. From Fig. 5, a D = 0%
The second set of simulations, shown in Fig. 2d to Fig. 2f, can be created for dins /λ ∼ = 0.096 resulting in an electrode
illustrates the change of C, S and D when εr and dSM /λ are periodicity of λ = 1.247 mm.
varied. Here the value of dins/λ was held constant at 0.03. This simulated D = 0% is achieved by a sensing mech-
In Fig. 2d it can be seen that the capacitance C is pre- anism which is dependent on the dimensions and dielectric
dominantly affected by a change in εr and less by dSM /λ, properties of the IDS and the εr of the oil under test. The
contrary to the previous observation varying dins/λ. The electric field distribution changes for different values of εr ,
sensitivity S in Fig. 2e varies with εr and dSM /λ. This occurs as shown in Fig. 6. This affects the sensed capacitance and
in a way that low values for dSM /λ increase the sensitivity thus εr in a convoluted manner. With reference to Eq. 1,
with increasing εr , whereas this pattern is the opposite at an accurate εr can be measured when no parasitic capacitance
high values of dSM /λ. The sensitivity decreases as the para- 
is present or when a particular set of Cparasitic, Cparasitic ,
sitic capacitance through this soldermask gradually increases. Coil and Cair compensates the remaining parasitic capacitance.
RISOS et al.: IDS: A DESIGN PRINCIPLE FOR ACCURATELY MEASURING THE PERMITTIVITY OF INDUSTRIAL OILS 6235

Fig. 2. FEM Simulations for the capacitance C, sensitivity S and accuracy D of εr,IDS . The first row (a, b, c) shows the figures of merit while varying εr
and dins of the IDS structure. The second row (d, e, f) shows the figures of merit when altering εr and dSM . The third row (g, h, i) shows the figures of merit
dependent on dSM and dins having εr,oil = 3.5.

The latter is case of the IDS; choosing λ = 1.247 for negative for εr > εr,FR4 as more field lines progressively
εr = 2.1065 has such an effect on εr,IDS . connect to V0 than to GND, Fig. 6c, causing a capacitance
The physics in this case is predominantly based on two over-proportional to εr . This special interaction is dependent
effects, illustrated with Fig. 6. For the capacitance with εr = 1 on the insulator thickness dins allowing an optimal value of λ
(Fig. 6a), the field lines emanated from VAC are strongly in the sensor design.
pulled downwards to the ground plane (GND) due to the
vicinity of the FR4 dielectric (εr,FR4 = 4.5 > εr,air ). This is III. D EVELOPING AND TESTING ACCURATE IDS
causing a lowered air capacitance, Cair , and a strong parasitic A PCB-IDS based on λ = 1.247 for a target deviation

capacitance, Cparasitic , through field lines connecting to the D = 0% was designed and fabricated without soldermask
underside of V0 (see circle in Fig. 6a). When measuring as the soldermask is detrimental to the sensing proper-
the oil (εr > 1) the field distribution changes as illustrated ties. A gold finish onto the electrodes provided sufficient
in Fig. 6b. This is yielding an increased E-field density through electrochemical inertness in the oil environment. Measure-
the oil than air. This produces an increased capacitance, Coil , ments on this IDS were done at 50 Hz using a standard
through εr and weak parasitic capacitance, Cparasitic. This impedance analyser (Hioki IM3590, Hioki, Nagano, Japan)
parasitic capacitance vanishes for εr = εr,FR4 and becomes with guarded four wire BNC connectors. Fig. 3 shows the
6236 IEEE SENSORS JOURNAL, VOL. 17, NO. 19, OCTOBER 1, 2017

Fig. 3. Designed IDS in standard PCB technology with four point measure-
ment principle through shielded BNC connectors. Sensor surface is Ni as a
diffusion barrier for copper and subsequently Au plated as corrosion reduction.
Active IDS sensing area highlighted and electrically grounded areas are
marked.

Fig. 4. A SEM cross sectional image of the manufactured IDS as a cross


sectional view showing the electrode width, thickness and separation from the
common ground layer as dins .

Fig. 6. Electric field lines (1 to 8) depicted for one pair of the simulated
electrodes in Log(E/E0 ) where E0 is 1 V/m. The field lines curl above
the electrodes and reconnect to the opposite electrode dependent on the
permittivity under test (red circle). A grey arrow supports the visual field
line tracking representatively between 1 and 5. (a) Two field lines connected
to the upper side of V0 while one reconnects to the underside. (b) Three field
lies connect to the upper side when measuring oil. (c) For higher εr values
Fig. 5. Simulation results for the deviation D dependent on dSM and dIns of oil, the increasing relative field intensity above the sense electrodes is
as a specific case for the MUT having εr = 2.1065. responsible for a non-constant parasitic capacitance.

manufactured PCB IDS. The four BNC connectors provided standard industrial oil base. This oil was heated to 140 °C
shielded measurement leads. These four leads merge onto the with 500 g of transformer insulating paper ‘Diamond-Paper’
PCB board surface in a shielded manner at the electrodes. (Weidmann Diamond Dotted 380 μm). The high temperature
The SEM image in Fig. 4 shows a cross sectional view of the treatment and presence of a thin copper sheet with a sur-
electrodes and indicates the actual dimensions. The ground face area of 40 cm2 accelerated the aging. The aging time
layer is indicated with “GND”. This confirms the designed was 600 h, which results in aged oil equivalent to its end of
parameter of width = gap = 312μm for dins ∼ = 120 μm. life condition [36]. The measured moisture value of the opaque
The SEM image is accurate within ±1 μm. These dimensions brown coloured oil was 103 ±5 ppm, measured via Karl Fisher
were consistent within ±1 μm for three examined IDS cross titration by eNZoil Ltd (Lower Hutt, New Zealand).
sections. Two vials, one containing the new oil and the other the
In order to verify the functionality of the IDS, showing the degraded oil, were prepared. In Fig. 7, we measured air, new
capability to measure εr of the new and degraded oil accu- oil and degraded oil manually with our optimized IDS. The
rately, six litres of a new insulating transformer oil (Savita Oil procedure was as follows: after measuring the air capacitance
Technologies Ltd. Grade BS 148 Class-I) were degraded with the IDS, the IDS was placed in a vial containing new oil
in an accelerated manner. This oil is a purified paraffinic for about 20 seconds. The IDS was removed and exposed to
oil without additives which has properties equivalent to a air for 10 seconds. Subsequently, the IDS was inserted into
RISOS et al.: IDS: A DESIGN PRINCIPLE FOR ACCURATELY MEASURING THE PERMITTIVITY OF INDUSTRIAL OILS 6237

Fig. 7. Repeatability and response of the sensor showing air and oil Fig. 9. Permittivity via IDS measured εr,IDS compared with reference
capacitance without hysteresis effect. The IDS was exposed to air and values εr,ref showing a good agreement. The exact value for the new oil was
manually inserted into vials containing new and old oil (each two times). εr,ref = 2.1065 and for the aged oil εr,ref = 2.2453 from which the
εr,IDS differs of about 0.5 %.

using three sensors from which we observed a consistent


deviation of 0.4 - 0.5% emphasising a manufacturing issue.
Examining Fig. 5, a lower value of dins/λ causes a trend
towards a positive deviation. The reduced thickness of the
insulator dins = 119 μm vs. designed 120 μm, explains this
shift. Still, this result is within the measurement error of the
experiment which was ± 0.5%. We did not observe any capac-
itance fluctuations dependent on the environment or sensor’s
temperature. An explanation for this lays in the thermal expan-
sion of dins. The thermal expansion of the FR4 insulator layer
may result in a dimensional change of not more than 100 nm
per 10 °C which is well below the 1 μm manufacturing
tolerance causing the 0.5% deviation.
This is a valuable outcome and verifies that standard
PCB production with FR4 laminate is capable of manufac-
turing the proposed design.

IV. SUMMARY AND C ONCLUSION


A procedure has been demonstrated for the development of
an accurate interdigitated sensor for measuring the degradation
Fig. 8. (a) Capacitance C measured vs. simulated. (b) Sensitivity S measured
vs. simulated. FEM simulation showing similar values to the experimental of industrial oils. This design procedure simulated figures of
data. merit of the sensor for particular combinations of dimensions
and sensor structure. The examined figures of merit (capac-
the vial containing degraded oil for about 20 seconds. This itance, sensitivity and accuracy) are strongly affected by the
process was repeated again and no cleaning of the IDS was spatial structure of the IDS making it important to know the
done. This sensor exhibited an instantaneous response without dimensions and permittivities of the physical layout. It was
lag or hysteresis effect to the air and different oils. This found that the soldermask throughout has a negative impact
shows that this IDS is capable of reflecting changes in the on the sensitivity but if this layer thickness is well con-
oil instantaneously. This is possible when the capacitance is trolled, it can improve accuracy. A similar result regarding
directly and linearly proportional to εr . In this experiment, accuracy was obtained from a variation of the insulator dis-
the capacitance of the IDS followed εr accurately within the tance dins between the IDS electrodes and a common ground
measurement uncertainty of 0.5%. plane (GND) without a soldermask. This also exhibited a
For a comparison of the measured vs. simulated figures of positive impact on the sensitivity.
merit C, S and D, the capacitance was measured over 51 data The high accuracy emerges from parasitic capacitances
points at 50 Hz in accordance with the standard [5]. Both which are auto-compensated choosing a right combination of
results of C and S are shown in Fig. 8. The capacitance C the IDS insulator dins and wavelength λ for a given εr of the
(Fig. 8a) and the sensitivity S (Fig. 8b) are slightly higher oil. The accuracy is achieved at the ratio of dins /λ ∼
= 0.95 with-
than simulated. In Fig 9, the measured permittivity of oil out the soldermask. Standard PCB technology was then used
via the manufactured IDS (Fig. 3) is compared to reference to manufacture an IDS with this given ratio.
values (εr,IDS vs. εr,ref ) for the new (εr,ref = 2.1065) and The efficacy of this design in discriminating changes in
aged oil (εr,ref = 2.2453). The mean value yields a slight the properties of industrial oil during degradation was shown
consistent positive deviation D of about +0.45% due to the by a measurement of the permittivity on unused and aged
manufacturing tolerances. We have conducted the experiment insulating oil and by comparing measured values to the values
6238 IEEE SENSORS JOURNAL, VOL. 17, NO. 19, OCTOBER 1, 2017

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four open-ended coaxial probe models for permittivity measurements engineering and photonics in Gottingen, Germany,
of lossy dielectric/biological materials at microwave frequencies,” IEEE in 2013. He is currently pursuing the Ph.D. degree
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RISOS et al.: IDS: A DESIGN PRINCIPLE FOR ACCURATELY MEASURING THE PERMITTIVITY OF INDUSTRIAL OILS 6239

Nick Long received the master’s degree in physics Gideon Gouws received the Ph.D. degree in physics
from Victoria University and the Ph.D. degree in from the University of Port Elizabeth, South Africa.
physics from the University of Southern California. He then joined the CSIR and was involved in the
He is currently Director of the Robinson Research development of thin film II–VI semiconductors by
Institute, Victoria University of Wellington, New organometallic vapor phase epitaxy. He also spent
Zealand. From 1994 to 2013, he was with Industrial several years with Rakon Ltd, New Zealand, where
Research Ltd. His primary research has been in high he developed commercial quartz crystal resonators.
temperature superconductivity. He was a Founder He is currently on the academic staff in engineering
of the program with IRL to develop HTS Roebel and computer science with the Victoria University
cables including development of manufacturing and of Wellington, New Zealand. His research interest is
characterisation processes. His other HTS work has in materials and sensor instrumentation, with focus
focused on enhancing wire performance and understanding the phenom- on impedance-based sensing for environmental and industrial applications and
enology of critical currents. He is also involved in many projects with the fabrication of microstructured materials for sensing and energy transfer
NZ companies in the application of electromagnetic sensing. His previous applications.
research experience includes quantum transport phenomenon in low temper-
ature physics and materials research in oxygen ion conductors.

Arvid Hunze received the M.Sc. degree in physics


from the University of Saarbruecken in 1999 and
the Ph.D. degree in materials science from the Uni-
versity Erlangen-Nuernberg in 2003. From 2003 to
2011, he was a Senior Scientist and Scientific Con-
sultant in the area of organic LEDs and photovoltaic
in the research and renewable energy business,
Department of Siemens, Germany. From 2011, he
was a Senior Scientist with IRL, Callaghan Inno-
vation, and Victoria University of Wellington, New
Zealand, developing optical and magnetic sensors
and systems for non-destructive testing and monitoring assets for energy
transmission.

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