VII.

Analisis data
• Kadar umpan (Feed) = 70,7% etanol dan 29,3% air

Kadar destilat = 99,6 % etanol dan 0,04% air

• Kadar residu (Bottom) = 53,7 % etanol dan 66,3% air

% 𝑚𝑎𝑠𝑠𝑎 𝑒𝑡𝑎𝑛𝑜𝑙 𝐹 0,707

o Mol etanol F = = = 0,0154
𝐵𝑚 𝑒𝑡𝑎𝑛𝑜𝑙 46
1−%𝑚𝑎𝑠𝑠𝑎 𝑒𝑡𝑎𝑛𝑜𝑙 𝐹 0,293
Mol air di F = = = 0,0163
𝐵𝑚 𝑎𝑖𝑟 18
𝑀𝑜𝑙 𝑒𝑡𝑎𝑛𝑜𝑙 𝐹 0,0154
XF etanol = 𝑀𝑜𝑙 (𝑒𝑡𝑎𝑛𝑜𝑙 𝐹+𝑎𝑖𝑟 𝐹) = 0,0154+0,0163 = 0,48580

% 𝑚𝑎𝑠𝑠𝑎 𝑒𝑡𝑎𝑛𝑜𝑙 𝐷 0,99,6

o Mol etanol D = = = 0,02165
𝐵𝑚 𝑒𝑡𝑎𝑛𝑜𝑙 46
1−%𝑚𝑎𝑠𝑠𝑎 𝑒𝑡𝑎𝑛𝑜𝑙 𝐷 0,0004
Mol air di D = = = 0,000022
𝐵𝑚 𝑎𝑖𝑟 18
𝑀𝑜𝑙 𝑒𝑡𝑎𝑛𝑜𝑙 𝐷 0,0180
XD etanol = 𝑀𝑜𝑙 (𝑒𝑡𝑎𝑛𝑜𝑙 𝐷+𝑎𝑖𝑟 𝐷) = 0,0180+0,0096 = 0,999

% 𝑚𝑎𝑠𝑠𝑎 𝑒𝑡𝑎𝑛𝑜𝑙 𝐵 0,537

o Mol etanol B = = = 0,01167
𝐵𝑚 𝑒𝑡𝑎𝑛𝑜𝑙 46
1−%𝑚𝑎𝑠𝑠𝑎 𝑒𝑡𝑎𝑛𝑜𝑙 𝐵 1−0,537
Mol air di B = = = 0,03683
𝐵𝑚 𝑎𝑖𝑟 18
𝑀𝑜𝑙 𝑒𝑡𝑎𝑛𝑜𝑙 𝐵
XB etanol = 𝑀𝑜𝑙 (𝑒𝑡𝑎𝑛𝑜𝑙 𝐵+𝑎𝑖𝑟 𝐵) = = 0,2405

o Cp Rata rata = ( Cp air x XF air ) + ( Cp etanol x XF etanol )

= ( 1 x (1-0,48580)) + ( 0,44 x 0,48580)

= …………. cal/mol.k

o λ campuran = ( λ air x XF air ) + ( λ etanol x XF etanol )

= ( 7,96 x 1-0,48580) + ( 7,36 x 0,48580)
= …………. cal/gmol

Garis umpan (q line)

o Dari grafik T vs X diperoleh nilai TB = 82oC = 355 K
TF = 25oC = 298 K
𝐶𝑝 𝑟𝑎𝑡𝑎−𝑟𝑎𝑡𝑎 (𝑇𝐵−𝑇𝐹)
o q =1+ λ campuran
 0,727952 ( 358,4−298 )
=1+ 7,670908

= 1 + 5,7318
= 6,7318
𝑞 6,7318
o Slope q line = 𝑞−1 = 6,7318−1 = 1,1745

Garis operasi Enriching (Enriching line)

6
o Dari praktikum R= 2 = 3

o Enriching line
𝑅 XD
yn+1 = 𝑅+1 Xn + 𝑅+1
3 0.999
= 3+1 Xn + 3+1

= 0,75 Xn + 0,24975
𝐿 𝑅 3
o Slope Enriching line = 𝑉 = 𝑅+1 = 3+1 = 0,75
𝐷 XD 0.999
o Intercept Enriching line = 𝑉 𝑋𝐷 = 𝑅+1 = = 0,24975
3+1

Garis operasi stripping (stripping line)

o Stripping line
𝑅 XB
ym+1 = 𝑅+1 Xm + 𝑅+1
3 0.2405
= 3+1 Xm + 3+1

= 0,75 Xn + 0,060125
𝐿 𝑅 3
o Slope stripping line =4 𝑉 = 𝑅+1 = 3+1 = 0,75
𝐵 XB 0.2405
o Intercept stripping line = 𝑋𝐵 = = = 0,060125
𝑉 𝑅+1 3+1