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Keywords: The failure mechanism in ductile cast iron under static loading is nucleation, growth, and coalescence of voids. It
Nodular cast iron is known from the literature that elastic–plastic porous materials under strain controlled cyclic loading show an
Low cycle fatigue increase of void volume fraction called void ratchetting effect. From this observation, we suggest that void
Strain-life approach ratchetting is the relevant mechanism for low cycle fatigue in nodular cast iron as well. The low cycle fatigue
Void ratcheting
process in the microstructure of ductile cast iron has been simulated cycle by cycle using unit cell models. The
Strong effect of shape of particle
strain-life approach for fatigue is followed in this work. The matrix material behavior is modeled as an elas-
tic–plastic one. From the simulations, void ratchetting is identified as a potential mechanism of low cycle fatigue
in nodular cast iron which finally leads to failure. The lifetime of different load ratio and different matrix
material behavior is extracted from the simulations. The simulated strain-life curves are compared with ex-
perimental data from literature.
1. Introduction more popular and efficient to understand the interaction between mi-
crostructure and material behavior [1].
Nodular cast iron (NCI) or ductile cast iron is an iron-carbon alloy. As NCI is mostly used in high cycle fatigue (HCF) applications, there
In NCI, the shape of graphite particles is nearly spherical that makes is scarcity of literature reporting on extremely low cycle fatigue (ELCF)
NCI’s properties unique as compared to the other types of cast iron. NCI of NCI. Komotori et al. [3] have experimentally observed void growth
has mechanical properties like steels. However, in comparison to steels, and coalescence in the ferritic NCI material. The schematic diagram of
NCI reduces manufacturing costs. For these reasons, NCI is widely used this process is shown in Fig. 1. In another article, Komotori et al. [4]
in transportation, nuclear and energy industries. A few examples of the have mentioned that the fracture mode is depended on the applied
application of NCI are gearboxes and crankshafts in automobile in- strain amplitude. The fracture mode can be surface mode or internal
dustry, wind turbine rotor hubs in energy industry and nuclear storage mode. Although, this behavior is observed for ferritic-pearlitic steel, it
and transportation casks [1]. is supposed to be equally applicable to nodular cast iron also. Mot-
The properties of NCI are dependent on the material’s micro- titschka et al. [5] conducted LCF experiments on ferritic cast iron GJS
structure, the form, size, and distribution of graphite particles and the 400 using round tensile bars at load ratio Rε = −1. The SEM picture of
defects present in the matrix due to the casting process. A ferritic matrix the fracture surface is shown in Fig. 2. It is clearly visible that fatigue
leads to ductile behavior of NCI, whereas a pearlitic matrix not only starts at graphite particles in the interior of the cross section. The li-
increases the strength but also brittleness. The combination of two gaments between the particles experience severe plastic deformations
phases shows the intermediate material behavior. with dimple structure.
The material fatigue under cyclic loading is the relevant damage Numerically, Gilles et al. [6] have first time observed void ratch-
cause in most practical applications since most structural components etting under cyclic loading in ductile materials. In their study, they
are exposed to alternating service loads. Thus, a better understanding of have created a cylindrical unit cell and carried out finite element cal-
fatigue failure is very important. Murakami [2] has mentioned previous culations under cyclic loading at constant triaxiality. The results of
studies related to the effect of shape and size of graphite nodules and these simulations show an initial spherical void experiencing de-
microstructure on the fatigue strength of NCI. No information is men- formation that leads to increasing of the mean void volume fraction
tioned regarding extremely low cycle fatigue in NCI. after every cycle which is defined as void ratchetting. The void ratch-
To gain information about low cycle fatigue (LCF), experimental etting due to hardening and residual stresses after each loading cycle
and computational approaches can be used. With significant advance- was observed by Leblond [7] as well. Devaux et al. [8] have studied
ments in the computational power, the simulation approach becomes void growth in ductile metals due to applied cyclic loading. They have
⁎
Corresponding author.
E-mail address: mehul.lukhi@imfd.tu-freiberg.de (M. Lukhi).
https://doi.org/10.1016/j.ijfatigue.2018.04.019
Received 4 January 2018; Received in revised form 10 April 2018; Accepted 17 April 2018
Available online 19 April 2018
0142-1123/ © 2018 Elsevier Ltd. All rights reserved.
M. Lukhi et al. International Journal of Fatigue 113 (2018) 290–298
Fig. 1. Void coalescence in NCI under cyclic loading (schematic after [3]).
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M. Lukhi et al. International Journal of Fatigue 113 (2018) 290–298
σ0 ⎝ σ0 σ0 ⎠ (6)
Here, σy is yield stress, σ0 is initial yield stress and n is hardening ex-
ponent.
The material parameters have been taken from Rabold et al. [10].
Fig. 4. Type of cast iron according to graphite particle shape [18]. The material parameters are shown in Table 1.
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M. Lukhi et al. International Journal of Fatigue 113 (2018) 290–298
Table 1 the softening would lead to localization of the deformation and com-
Parameters for ferritic matrix. plete failure within the next few cycles. The point C can be treated as a
Parameter Value transition to the cyclic void coalescence. That is why this point is de-
fined as the failure point in this study. In the experiments, degradation
Young’s modulus (E) 210,000 MPa of macroscopic stress or stiffness of 1% or 2% is considered as a cri-
Poisson’s ratio (ν) 0.3 terion of fracture initiation.
Hardening exponent (n) 0, 0.05, 0.1, 0.2
Initial yield stress (σ0 ) 230 MPa
The void distortion process is shown in Fig. 7. Fig. 7(A) shows
perfect spherical void at the beginning of the simulation. Fig. 7(B)
shows the distorted void and Fig. 7(C) represents the void shape at the
model failure.
Firstly, graphite is modeled as a spherical void. The model has been Interesting is the concentration of accumulated plastic strain at the
simulated cycle by cycle as per the above-mentioned material para- deformed void, see Fig. 7(C). The maximum local equivalent plastic
pl
meters and boundary conditions. The load ratio of applied cyclic de- strain εmax is plotted in Fig. 8 vs number of cycles for different strain
formation is Rε = −1. The macroscopic stress vs cycles response of the amplitudes. The x-axis scale is logarithmic and y-axis scale is linear. The
model is shown in Fig. 6(a). The applied strain amplitude for this curve failure points for different strain amplitudes are marked with crosses in
is Δε = 5% and hardening exponent n = 0.2. All the points in the dia- Fig. 8. For lower strain amplitudes Δε, the maximum accumulated
pl
gram represent the maximum values of the macroscopic stress during plastic strain εmax reaches higher values. This tendency is in contra-
the cycle, i.e. at points of reversal. diction to classical fatigue laws like Coffin–Manson, which would pre-
pl
In Fig. 6(a), the curve starts with zero stress at the beginning of the dict failure at equal values of εmax . It is again an indication that another
simulation. As the simulation progresses, the macroscopic stress in- mechanism, namely void ratchetting is responsible for failure of NCI
creases due to isotropic hardening of the matrix. The macroscopic stress under cyclic loading at large strain amplitudes Δε. In case of small
reaches a peak level. After the peak point, the macroscopic stress starts strain amplitudes, the formation of fatigue cracks in the matrix becomes
decreasing. The overall behavior of the curve can be described as initial more likely, however.
cyclic hardening followed by geometric softening behavior. The plastic The effect of different hardening exponents n on the macroscopic
strain accumulation with each cycle leads to an increase in the overall stress response has been studied using the simulations. The compiled
volumetric strain EV of the unit cell which is attributed to void growth, results are shown in Fig. 9. The hardening exponent n = 0 represents
since the plastic matrix is incompressible. This void ratcheting is shown the elastic–ideal plastic material behavior. As expected the macroscopic
in Fig. 6(b). The initial perfect spherical void is now distorted. The void stress increases with the increase in hardening exponent. The full line
ratchetting leads to a cyclic necking of the cross-section of the unit cell. shows strain amplitude Δε = 2% and the dotted line shows strain am-
This leads to initiation of cyclic softening. When this plastic strain ac- plitude Δε = 1%. The macroscopic stress also increases with the in-
cumulation reaches a critical limit, there is a drop in the macroscopic crease in applied strain amplitude.
stress response. After the peak point, geometric softening begins, which Different strain amplitudes Δε have been imposed on the cell model.
is defined as the failure point of the unit cell. This point is marked as The obtained cycles to failure Nf are extracted from the simulation
point “C” in Fig. 6. As mentioned in the introduction, the cyclic necking results. This data is plotted on logarithmic scale for the different
is associated with coalescence of voids and it leads to the formation of hardening exponents n in Fig. 10. The strain-life curve is approaching
the macroscopic crack. In a real material with many graphite particles, monotonic failure on the left-handed side of the diagram. When the
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applied strain amplitude is very high, the cell model fails immediately.
It is evident from Fig. 10 that the number of cycles to failure is de-
creasing with the increase in hardening exponent. With increase in
hardening exponent n, the slope of strain-life curve is decreasing.
Furthermore, Fig. 10 shows corresponding experimental data from
literature [3,21–27] for ferritic NCI GJS-400. All the experimental data
lie within a narrow band. The metallographic characteristics of NCI are
mentioned in Appendix A. From the comparison of the experimental
and simulation strain-life curves, it can be concluded that the simula-
tion results are in qualitative agreement with the experimental results
but there is a quantitative mismatch between them. The simulations
overestimate the lifetime by an order of magnitude. The potential
reasons of overestimation will be discussed below. The effect of load
ratio Rε on the strain-life diagram is shown in Fig. 11. It can be observed
that an increase in the load ratio increases the number of cycles to
failure. In the low strain amplitudes region, the predicted influence of
load ratio Rε is negligible.
This simple model uses just four material parameters to predict the
above-mentioned results. The quantitative mismatch between the si- pl
Fig. 8. The maximum local equivalent plastic strain εmax evolution with number
mulation and experimental results provided additional motivation to
of cycles.
carry on this study to find out the potential reasons that might be
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Fig. 9. Macroscopic stress vs cycles for different hardening exponents. Fig. 11. Effect of load ratio R ε on strain-life diagram.
3 dev
1. Type of hardening Φ= (σ −α ): (σ dev−α ) −σy.
2 (7)
2. The interaction between graphite particle and ferritic matrix
3. Non-spherical shape of graphite particle Therein, σ dev
is the deviatoric part of the stress tensor and α denotes the
4. Damage inside the matrix due to the presence of defects back-stress tensor. The isotropic hardening is included in the evolution
of the yield stress σy as
These potential reasons are explained in detail and their influence
pl
on the strain-life behavior is investigated. σy = σ0 + Q∞ (1−e−bε ). (8)
Hück et al.[25]
Pusch et al.[26]
Ricotta et al. [27]
10 0
10 -1
10 0 10 1 10 2 10 3
Number of Cyclles to failure, N f
Fig. 10. The strain-life plot from the simulation results contrasted with experimental data.
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For the micromechanical modeling of NCI, most of the investigators 4.4. Graphite particle shape
assumed graphite particle as a void [28,29]. In contrast, Rabold et al.
[10], Bonora et al. [30] and Collini et al. [31] have modeled graphite It can be observed from Fig. 3 that not all the graphite particles in
particle as a rigid particle. the matrix are perfectly spherical. To consider a graphite particle as
In the previous sections, the graphite particle has been modeled as a nodular, classification by shape factor can be used as mentioned earlier.
void. Now, the graphite is modeled as a rigid particle as shown in Here, the cell model with the non-spherical shape of the particle shall
Fig. 13. The black arc represents the graphite particle which is modeled be used as shown in Fig. 5. The orientations of semi-major and semi-
as a rigid line. The cell model with graphite particle is subjected to the minor axes are also given in Fig. 5. The major axis of ellipsoidal void is
cyclic loading of load ratio Rε = −1 and material property is elastic–- normal to the direction of loading.
plastic with isotropic hardening (n = 0.2). The deformation of the The unit cell model is simplified by assuming that all the particles
matrix can be seen in Fig. 13. The interaction between the graphite are non-spherical in shape and have same orientations of major and
particle and matrix is defined as a frictionless contact. The graphite minor axes. The results of strain-life studies are shown in Fig. 15. It is
particle is fixed at the lines of symmetry. evident that the cell model with ellipsoidal void predicts the strain-life
The strain-life curve resulting from the simulations is shown in behavior of NCI more accurately than the cell model with a spherical
Fig. 14 in comparison to the previous results with graphite as a void and void. This approach is conservative for fatigue life prediction. Another
compared with experimental data. If the graphite particle is modeled as observation from Fig. 15 is that the shape of graphite has a high in-
a rigid particle, then it requires a lower number of cycles to failure in fluence on the strain-life behavior.
comparison of graphite as a void. The reason for this behavior can be If the non-spherical shaped graphite particles would be considered
explained by the interaction of the matrix with the rigid particle. If the as rigid, then it may give even more realistic strain-life behavior.
graphite particle is a rigid inclusion (in the cell model), then it favors Considering S = 0.70 and rigid graphite particles, an improved cell
void growth [10]. This faster void growth leads to fewer cycles to model is prepared. The results of this model are shown in Fig. 16. It can
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10 1
The metallographic characteristic of the experimental data used for the reference have been mentioned in Table A1. The nodularity (ratio of
number of nodular graphite particles to the number of graphite particles) of material varies between 73.4% and 92.5%. The graphite particles are in
form V and VI. The volume fraction of graphite is between 10% and 13%. The graphite nodule diameter varies between 5 and 30 μm.
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M. Lukhi et al. International Journal of Fatigue 113 (2018) 290–298
DI400
Supplementary data associated with this article can be found, in the
290
27
EN-GJS-400-18U-LT (main online version, at http://dx.doi.org/10.1016/j.ijfatigue.2018.04.019.
V (34.0%), VI (65.3%)
Bleicher et al. [22]
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