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EXPERIMENTAL TECHNIQUES
Loading Rates
The loading rates usedduring the static confined(triaxial) and uneon-
fined (tensile and compressirestrength) testingwere lessthan 5 x 10a psi
per see, specifically, 1, 50, 500, and 2250 psi per see. Rates between
5 x 10• and 1 • 10* psi per see are defined as rapid-loading rates, while
rates greater than 1 • 10* psi per see are defined as shock-loadingrates.
Techniques
Static uneonfinedand confinedtestswere conductedusing a 440,000-1b
universal testing machine and a 10,000-psi-capacitytriaxial chamber.
The static tests,tensile splitting, compressirestrength, and triaxial shear
tests were conducted in accordancewith the standard procedures,•i.e.,
CRD-C 77-61, CRD-C 19-65, and CRD-C 93-64, respectively,with the
exceptionof lo.adingrates. CRD-C 93-64 was further modified slightly
to accommodatewave velocity equipment for purposes of determining
the effectsof axial and lateral pressureson compressionalwave velocities
parallel to the coreaxis. Confiningpressuresof 250, 1000, 4000, and 5000
psi were utilized during triaxial testing.
The method of triaxial testing as modified with compressionalwave
velocity equipment involved the use of a cylindrical specimenencasedin a
flexible membraneand placed in a triaxial chamber,subjectedto a con-
stant lateral fluid pressure,then loaded axially to failure.
Fig. 1 is a sketchshowingthe triaxial chamberand the accessories used
inside the chamberfor velocity determinations.End plates (housingthe
transducers) and bearing plates were used to allow for a size reduction
to the NX-size samples. Aluminum end plates and bearing plates were
]•FFECT OF RATE OF •LOADING ON STRENGTH
Loading
Head
I
Chamber Loading Ram
Transducer
End Plate
Bearing Plate
Membrane Sample
Bearing Plate
End Plate
Transducer
Base Plate
Piston
Ram
Specimen
Pedestal
Foundation
SCALESI MAGNETIC
POLE
I
• I
Fig. 3--Gas-operated gun and target configurationat muzzle end of gun barrel.
c•-1- P_t
p•
= U•_2
Us
(5)
Theseequations ar• basedonthe assumptionthat an equilibriumstateof
stressis reachedbehindthe shockwave. In thissimpleform,they are
validonlyin theregionof uniaxialstrain.Theseequations correspondto
the Hugoniot or the locusof shocked-endstatesreached.
Rock Specimens
The rocksstudiedall camefrom the U.S. AtomicEnergy Commission
's
NevadaTest Site (NTS) at Mercury,Nev. The granodiorite(granite)
camefrom the PILE DRIVER experiment,the basaltcamefrom Buck-
board Mesa, and the tuff came from the RED HOT-DEEP WELL ex-
periments.The graniteis a light-gray,dense,coarse-grained, unweath-
eredrockwith phenocrysts of orthoclasefeldsparpresent. The basaltis
a light-gray,dense,fine-grained, unweathered rockcomposed of plagio-
clasefeldsparand lesseramountsof pyroxene,olivine,and magnetite.
The tuff is a light greenish-yellow
to brownish-red,generallypoorlyin-
durate rock composedof volcanic ash.
Sample Preparation
Therockcoresusedfor staticand rapid testingwereNX (2•-in.-diam)
in size.Thecoreswerecutto havea length-to-diameter(L/D) ratioof 2
usinga diamondsaw. After cutting to propersize,the coreendswere
surface-ground
andlappedto obtainplaneendsurfaces.Theendsurfaces
were within 0.001 in. in planehess,were parallel to each other within
0.006 in., and the ends were perpendicular to the sides xvithin 0.5ø.
The samplesfor air-gun tests (Fig. 5) xverepreparedfrom NX cores
sawedinto disksand groundplane on a milling machineto a tolerance
of 0.01mmacross the 50-ramdiam. Thesediskswerethenhand-lapped to
a smoothfinish,and the thicknessmeasured.The aluminummounting
platewasapproximatelyL--in.thick,fiat, and parallelto within 0.001in.,
and had a hand-lappedand polishedsurface.
EFFECT OF RATE OF LOADING ON STRENGTH 9
SOLDER
TERMINALS
•1• • GRANITE
PLEXIGLAS•
ALIGNMENT
JIG
wIRES
Basal•
Granite
Trace of vertical
strain pulse
Time = msec/cm
Time = I msec/cm
wire as it propagates through the specimen, and the wire follows the
particle motion. Movement of the wire in the magnetic field generatesan
electromotive force (emf) by cutting lines of magnetic force. This emf
is proportional to the particle velocity in the specimen as shown by the
following equation:
E (6)
xvhereE is emf, volts; fi is •nagnetie-fieldstrength, webersper sq m; 1 is
effective length of wire, m; and U•, is particle velocity, m per see.
The magnetic-field strength fi was 775 x 10-* webers per sq m and the
wire length 1 was 6.35 x 10-:• m (0.25 in.) for all the tests. The shock-
propagation velocity can be determined from the time difference between
the particle velocity signalsand the known wire spacing.
The impedance mismateh between the wire and rock should not cause
a serious perturbation in the shock front since its transit time is small
compared to the rise of the shock front. Reflections within the wire,
which should have a frequency of about 40 MHz, should bring the wire
to equilibrium with the rock very rapidly. Thus, the assumption that the
induction wire follows the particle motion of the rock seemsto be justified.
Each induction wire was connectedto the input of a Hewlett-Packard
450A amplifier. The output signal from the amplifier was fed to the input
of a Type 545 Tektronix oscilloscopewith a Type CA preamplifier
through 100 ft of RG-SU cable. The cable was terminated in its character-
istic impedance (51 ohms) at the input to the oscilloscope.Another in-
duetion wire was positioned between the mounting plate and the rock
specimento trigger the oscilloscopes and the fidueial generator. The
fidueial signal was fed to the B input of the oscilloscopesand recorded on
each signal record. This provided a time reference which could be used to
compare all the signals.
Data Reduction
The stress-strain path followed by the material in each shot was de-
ducedfrom the measuredwave propagationand particle velocities. Each
continuousrecord of particle velocity was approximatedby straight-line
segments,which is equivalentto approximatingthe wave shapeby a series
of successiveincrements of pressure.
From the four induction wires placed in the material, signals similar
to thoseshownin Fig. 8 will be received.
A particle velocity U• of amplitude E• occurs at the time t•. The
magnitude in meters per second of U• at E1 is determined from the
equation
U•:E•(2.03xlO •) (7)
EFFECT OF RATE OF LOADING ON STRENGTH 13
e•(2 --SIGNAL
FROM
WIRE
1
(i)
1) •SIGNAi FROMWIRE2
• E1(2) • --SIGNAL
FROM
WIRE3
.• • i (3) SIGNAL
]_
iv
t,(3) _i
• I
••2(4) FROM
WIRE
4
]• tl(4) •
Pn----P•-I
+ po(U•n-U•,
n-•)
1__(U•n--
en_• U•, (9)
14 BASIC AND APPLIED ROCK MECHANICS
1--•--_ U•-•--•Y•,•'-x
' (10)
These equations are taken from Ref. 11, which also shows a com-
parison of a various number of n-line approximations. This indicates
that the calculation processis convergentto the actual ttugoniot, with
the accuracy depending on the number of straight-line segmentsused to
approximate the curved record.
Static
The averages of three tensile splitting tests for the three rocks are
given below. These results are used in conjunction with the triaxial shear
results on the plots of Mohr envelopes(Fig. 16).
œ;-4
T-J4 !50_•
psi 50psi/sec
0 2 4
T-20
T-21
00•
ps•50
50
psi/sec
6
psi 50 •si/sec
Fig. 11. Compressional wave velocity rs. deviator stress for tuff.
]•FFECT OF •:{ATE OF LOADING ON STRENGTH 17
4O
ß /•''•-500
225• 50
00
•
o 20
lO
•OTE: Loadi •g rates
•re l, 50, ] )0, and
2250 psi/sec
o
0 4000 0 4000 8000 0 4000 8000 12,000
Axial Strain, •in./in.
•3 = 500 •si
,,o
3=1500
si
J/ o=lOOO
The tuff was the only rock tested that showed a decrease in deviator
stresswith increasedconfining pressures. The rock was tested at natural
moisture contentof approximately 21% and in the undrained state. The
pore pressurebuildup due to confining pressureand axial loading prob-
ably causedthe pore pressureto break down someof the rock structure,
thereby causinglower strengthsat increasedconfiningpressure. Mogi
found a similar condition. In additionaltriaxial testing,the effectof pore
pressureshouldbe accountedfor in terms of effectivestresses(a• =a-
where rr• is effectivestresses.a is total normal stress,and • is pore pres-
sure. Young's modulus also decreasedwith increased rra's.
Basalt was testedin triaxial compression at loadingrates of 1, 50, 500,
and 2250 psi per see. Fig. 12 showsthat at •a's of 250 and 1000 psi, the
maximumdeviatorstress(•) increaseswith increasedloadingrate, with
the exceptionof the specimensloaded at 50 psi per see. At 5000 psi
the a increasesthrough the full range of loading rates used. Total axial
strain at failure increasesin all caseswith an increasein loading rate at
eachof the rr:•'susedexceptat 250 psi rr:•and at 50 psi per seeloadingrate.
Plotting • at maximum loading rate (•'n,•x)over a at minimum loading
rate (•'n,•n)for eachrr.•usedfor basaltresultsin a linear relation, with a
positiveslopeas shownin Fig. 15. This is to say that as rraincreases,the
effectof •' on strength becomesmore significant.
Generally,the straight-linerelationshipdescribedby Mohr's criterion,
EFFECT OF RATE OF I•OADING ON STRENGTH 19
Fig. 16--Mohr envelopesat various loading rates for basalt and granite.
20 BASIC AND APPLIED ROCK MECHANICS
Loading
Rates, Confining
Pressures,
Psi
Psi per See 250 1000 5000
I • 61 61
50 60 63 63
5OO 71 75 7O
2250 -- 74 72
EFFECT OF RATE OF I•OADING ON STRENGTI-I 21
XXXXX X XXX
22 BAsic AND APPLIED ROCK MECHANICS
It can be seenfrom Table 4 that the strength and modulus of the basalt
are not greatly affected by small increasesin loading rates. The ratios of
strength and modulus of specimenstested at 500 and 1 psi per sec are
1.04 and 1.10, respectively. However, the ratios of rapid to static
(F,./Fs) strength and modulus (E,./Es) are somewhat different; the
strength ratio is 1.48 and the modulus 1.17. In calculating E•./Es, the
toodull obtained from specimens tested at 2.06 x 10• psi per sec were
omitted for the following reasons. These specimenswere tested at the end
25
lJ
• L2
Static
50
ps
•/$ec
Rapid lO7 p;i $ec
3 2 '• q. • q,
Axial 5tra{ •, n.:ccc•nt
[] SLyess I'o•nt
i 3 ) 3 o:) 7H 3 1 r) 2J 30
can be stated that the weaker materials would increase in strength with
loading rates greater than 10• psi per seeinstead of remaining constant as
Atehley and Furr suggest. The maximum stresslevel for tuff is plotted
in Fig. 20. A stress level for basalt of 4.7 kb is also plotted in Fig. 20,
which appears to agree with the basalt curve presented by Kumar et al.1
if it were projected. These two stresspoints are plotted to indicate that
compressire strength does increase with increased loading regardless of
test geometry.
Total axial strain (Fig. 21) observed at failure in the rapid tests was
greater than the correspondingstrain in the static tests. Diametral strain
decreasedslightly with increasedrates of loading for the basalt (Fig. 22).
As mentionedpreviously, the Young's modulusof elasticity for the basalt
tested at 2.06 x l0 s psi per seewas suspectedto be low. For this reason,
these values are not included in the plot of Young's modulus rs. loading
rate (Fig. 23). The method of least squareswas usedto obtain a straight-
line equation of best fit for the data in Figs. 21-23.
Shoek Loading
The shock-loading work was accomplishedas part of a different re-
search program from that in which the static and rapid work was done.
(o.52!
>)(x)
..
1 l) 10 • 10 • 10 10
• , psi/see
• y = •.67,0• (-0.16'•2)
(^)
J.
--
--
(Log S'-a:e)
Therefore, a few of the figures in this portion of this chapter include data
for quartzite which will not be discussed.
Fig. 24a is a plot of pressure rs. particle velocity computed from a
single impact test on granite. Three curves were computed from the four
records obtained for the particle velocity wires, which were separated by
¬ in. The scatter in the data is probably causedby local inhomogeneities
within the specimen. Fig. 24b shows a comparison of stress-strain data
for granite obtained from two separate tests. The maximum stress
reached in Shot I was 3.2 kb and in Shot 2, 13.8. As can be seenfrom the
figure, the computed stress-straincurvesfroin thesetwo tests are identical
within experimental error. The modulus,which can be computed from
thesedata points, is a constrainedmodulus.
Fig. 25a shows a plot of pressure rs. particle velocity, or the shock
impedance, for all materials tested. Each curve was computed from a
single experiment. Fig. 25b shows the stress-strain relation for all the
materials tested. The maximum stressonly represents the stress reached
in the respectivetests and doesnot indicate elastic failure. Under condi-
tions of one-dimensionalstrain thesematerials, with the exceptionof tuff,
would not be expectedto fail in compressionat these pressure levels. For
DD
12
SINGLE SHOT
LEGEND
DATA COMPUTED fROM
LEGE
0 SHOT 2
D
SHO
1
O SIGNAL WIRES 1 AND 2
A SIGNAL WIRES 1 AND 3
i"l SIGNAL WIRES I AND 4
o
2 4 6 @ lO 0 0 4 0 8 1.2 1.6 2.0
LEGEND
•
LEGEND
GRANITE p GRANITE
QUARTZITE
BASALT BASALT
QUARTZITE
/
PLEXIGLAS PLEXIGLAS
TUFF TUFF
/
/
______._..Q.____-------O------'---
2 3 4 5 6 7 0 02 04 06 08 10 12 •4
PARTICLE V•LOC(TY 10-• MM/•SEC STRAIN PCT
SHOCKP•ESSUREVERSUS•ARTICLEVELOCITY b STRESS VERSUS STRAIN
Plexiglaswasusedas a reference
materialto verify the testmethod.
30 BASIC AND APPLIED I•0CK MECHANICS
! ¸
(2) .,- •
ß . ) •o o
As shown in Fig. 27a, these data correlate closely with the data points
reported by Wagner et al.; •3 however, this comparisonrequires extrap-
olation of their data from approximately 6 kb to the pressure (approxi-
mately 2 kb) achievedin the present tests. The Plexiglas data also seem
to correlate well with low-pressure stress-strain data from compressive
EFFECT OF RATE OF LOADING ON STRENGTH 31
?
7
SYM•DL STRAIN
RATE,IN/IN/SEC
0.005 --
0 0070
o o •o
• • •o
ß 1210 •0
•RoJg'r- GENERAL DATA -
WES I•,TA
WES
DATA,
PLEXIGLAS
SPECIMEN
2)25
INCHES
IN DIAMETER BY ) 25 IHCHES
m
0 2 4 8 8 I0 o ;• 4 8 8 io 12
STRAIN, PCT STRAIN ,• PCT
o. PLEXIGLAS b. LUCITE
,ooc
14
12 ooc
I
• io ioc
io
4
I.C /•// n LEGEND
- /
/'/ I•
o' IITRI DATA
LEGEND
o.
SRI DATA--
WES DATA
•], WES
DATA
(2SHOTS)
o.o -•r
'• • I IllIll I I I Illll I I illIll I I •lllll I I [ I IIIII
0o 0.5 1.0 I .S 2.0 0.001 0.01 0.1 I I0 I00
STRAIN • PCT STRAIN ,• PCT
c. QUARTZITE d. GRANITE
CONCLUSIONS
On the basis of results obtained from the static, rapid, and shock-
loading testsof the basalt, granite, and tuff, the following conclusionsare
drawn:
and for tuff 1.70. The F,./F8 of tuff is closeto the Fr/F8 of weak concrete
reported by several other investigators.½.7
6) For basalt the axial strain at failure increaseswith an increasein
the logarithmic rate of loading, while diametral strain at failure
decreases.
7) Young's modulus of elasticity increaseswith an increase in the
logarithmicrate of loadingup to about2 x •10TMpsi per sec. This is based
on a comparisonof the constrainedmoduluscalculatedfrom the shock-
loading data and unconstrainedmodulusof all three rocks.
8) Uniaxial stress-strain or Hugoniot equation of state data can be
determinedby the methoddescribedin this chapter for solid materials in
the pressurerange from 0 to 40 kb. The velocity of propagationcan be
the application of the conservationof massand momentumequations.
The data obtained from these equations correspondto the Itugoniot or
the locus of shocked-endstates reached. This method of obtaining con-
tinuous records of propagation velocity and particle velocity does not
dependon a prior knowledgeof the unloadingcharacteristicsof a mate-
rial as doesthe free-surfacetechnique. The shockresponseof the basalt
and granite was found to be linear. The tuff specimen exhibited an
unstable shock structure.
ACKNOWLEDGMENTS
REFERENCES
1. Kumar, A., Hausser, F. E., and Dorr, J. E., The Effect of Stress Rate and Tem-
perature on the Strength of Roelos,publisher unknown.
2. Stowe, lt. L., "Dynamic Properties of Granodiorite, Project PILE DRIYER, •
(Abstract only), Engineering Mechanics Division Specialty Conference Proceed-
ings, ASCE, Oct. 12-14, 1966.
3. Wucrker, R. G., •Influence of Stress ]late and Other Factors on the Strength and
Elastic Properties of ]locks," Quarterly of the ColoradoSchoolof Mines• vol. 54,
No. 3, July 1959.
34 BASIC AND APPLIED ]:•OCK MECHANICS
4. Phillips, D. W., "Tectonics of Mining," Colliery Engineering, Part II, ¾o1. 25,
No. 294, 1948.
5. Atchley, B. L., and Furr, H. L., "Strength and Energy Absorption Capabilities
of Plain Concreteunder Dynamic and Static Loading," ACI Proceedings,Vol.
64, No. 11, Nov. 1967, pp. 745-776.
6. Watsrein, D., "Effect of Straining I•ate on the Compressive Strength and Elastic
Properties of Concrete,' ' ACI Proceedi•igs,Vol. 49, No. 8, Apr. 1953, pp. 729-744.
7. Munson, D. E., and Barker, 14. M., "I)ynamically Determined Pressure-Volume
Relationships for Aluminum, Copper, and Lead," Jot•rnal of Applied Physics,
Vol. 37, No. 4, Mar. 15, 1966, pp. 1652-1660.
8. Karnes, C. H., "Stress-Strain Characteristics of Materials at High Strain Rates;
Part IV: Experimental and Theoretical Analysis of Plastic Impacts on Short
Cylinders," June 21, 1960, University of Texas, Austin.
9. U.S. Army Engineer Waterways Experiment Station, CE, Handbook for Con-
crete and Ceme•t, August 1949, Vicksburg, Miss. (with quarterly supplements).
10. Frasier, J. T., and Karpov, B.C., "The Transient Response of Wax Targets
Subjected to Hypervelocity Impacts," paper presented at Society for Experi-
mental Stress Analysis, Spring Meeting, Denver, Colo., May 5-7, 1965.
11. Dennen, R. S., '•Synthesis of Rock Hugoniots," DASA 1652, March 1965, IIT
Research Institute, Chicago, Ilk
12. Mogi, K., "Deformation and Fracture of Rocks under ConfiningPressure, (1)
Compression Tests on Dry Rock Sample," B•dletin of the Earthq•take Research
Instit2tte, Vol. 42, Pt. 3, September 1964.
13. Wagner, M. H., Waldorf, W. F., .lr., and Louie, N. A., "Determination of
Itugoniot Equations-of-State for Polymers and Reentry Vehicle Materials and
Investigations of Fracture Phenomena," AFSWC TDR-62-66, Vol. 1, August
1962, Aerojet-General Corp., Downey, Calif.
14. Maiden, C. J., and Green, S. J., "Compressire Strain-Rate Tests on Six Selected
Materials at Strain Rates from 10-:" to 10• In./In./Sec," Jo•trnal of Applied
Mechanics, Vol. 33, No. 3, Sep. 1966, pp. 496-504.
15. Dcnnen, R. S., "Hugoniot Determination for Granite and Other Geological
Samples," IIT-A6040-1, September 1963, lit Research Institute, Chicago, Ill.
16. Stowe, R. L., "Static and Dynamic Strength and Stress-Strain Properties of
Rocks of Four Types," U.S. Army Engineer Waterways Experiment Station,
CE, Vicksburg, Miss., in preparation.
17. Duvall, G. E., "Propagation of Plane Shock Waves in a Stress-Relaxing
Medium," Stress HZavesin Anelastic Solids (A SymposD•m), H. Kolsky and W.
Prager, eds., Springer-Verlag, Berlin, 1964, pp. 20-32.
18. Het•nyi, M., Handbook of Experimental Stress Analysis, 5th Printing, John
Wiley, Ne•v York, 1963, p. 442.