Technical Data Sheet

LOCTITE® 222
April-2004

PRODUCT DESCRIPTION Cure Speed vs. Bond Gap

LOCTITE® 222 provides the following product characteristics: The rate of cure will depend on the bondline gap. Gaps in
Technology Acrylic threaded fasteners depends on thread type, quality and size.
Chemical Type Dimethacrylate ester The following graph shows shear strength developed with time
on steel pins and collars at different controlled gaps and tested
Appearance (uncured) Purple liquidLMS according to ISO 10123.
Fluorescence Positive under UV lightLMS
Components One component - requires no mixing 100

% of Full Strength on Steel

Viscosity Low, thixotropic
Cure Anaerobic
75
Secondary Cure Activator

m
m

m
Application Threadlocking 5m

05
2

m
0.

0.

m
Strength Low 50

15
0.
LOCTITE® 222 is designed for the locking and sealing of
threaded fasteners which require easy disassembly with 25
standard hand tools. The product cures when confined in the
absence of air between close fitting metal surfaces and 0
prevents loosening and leakage from shock and vibration. 1min 5min10min 30min 1h 3h 6h 24h 72h
Particularly suitable for applications such as adjustment of Cure Time
set screws, small diameter or long engagement length Cure Speed vs. Temperature
fasteners, where easy disassembly is required without The rate of cure will depend on the temperature. The graph
shearing the screw. The thixotropic nature of LOCTITE® 222 below shows the breakaway strength developed with time at
reduces the migration of liquid product after application to the different temperatures on M10 steel nuts and bolts and tested
substrate. according to ISO 10964.

TYPICAL PROPERTIES OF UNCURED MATERIAL 100

% of Full Strength on Steel

Specific Gravity @ 25 °C 1.05

Flash Point - See MSDS
75
Viscosity, Brookfield - RVT, 25 °C, mPa·s (cP): C
40°

Spindle 3, speed 2.50 rpm ≥3,500LMS

Spindle 3, speed 20 rpm 900 to 1,500LMS

5°C
°C
50
Viscosity, EN 12092 - MV, 25 °C, after 180 s, mPa·s (cP):
22

Shear rate 277 s-1 135

25
TYPICAL CURING PERFORMANCE
Cure Speed vs. Substrate 0
The rate of cure will depend on the substrate used. The graph 1min 5min10min 30min 1h 3h 6h 24h 72h
below shows the breakaway strength developed with time on Cure Time
M10 steel nuts and bolts compared to different materials and
Cure Speed vs. Activator
tested according to ISO 10964.
Where cure speed is unacceptably long, or large gaps are
100 present, applying activator to the surface will improve cure
% of Full Strength on Steel

speed. The graph below shows breakaway strength developed

with time using Activator 7471 and 7649 on M10 zinc
e

75 dichromate steel nuts and bolts and tested according to ISO

at
l
ee

10964.
ro
St

ch
Di

50
nc
Zi

l
t ee
25 as
s sS
Br es
ainl
St
0
1min 5min10min 30min 1h 3h 6h 24h 72h
Cure Time
 TDS LOCTITE® 222, April-2004

% of Full Strength on Steel 100 Heat Aging

Aged at temperature indicated and tested @ 22 °C
No Activator 125
75

% Initial Strength at RT
1 120°C
47 100
7
50 or
at
49ctiv 75
to r 76 A
iva
25 Act
50
150°C

0 25
1min 5min10min 30min 1h 3h 6h 24h 72h
Cure Time
0
0 1000 2000 3000 4000 5000
TYPICAL PROPERTIES OF CURED MATERIAL Hours
Physical Properties:
Coefficient of Thermal Expansion, ASTM D 696, K-1 80×10-6 Chemical/Solvent Resistance
Coefficient of Thermal Conductivity, ASTM C 177, 0.10 Aged under conditions indicated and tested @ 22 °C.
W/(m·K) % of initial strength
Specific Heat, kJ/(kg·K) 0.30
Environment °C 100 hr 500 hr 1000 hr 5000 hr
Motor Oil 125 100 95 90 85
TYPICAL PERFORMANCE OF CURED MATERIAL
Leaded Petrol 22 95 95 95 95
Adhesive Properties
Brake fluid 22 95 95 95 90
After 24 hours @ 22 °C Water Glycol 50/50 87 80 80 80 80
Breakaway Torque, ISO 10964: Acetone 22 100 90 90 90
M10 steel nuts and bolts N·m 6
(lb.in.) (50) Ethanol 22 95 95 90 90

Prevail Torque, ISO 10964: GENERAL INFORMATION

M10 steel nuts and bolts N·m 4 This product is not recommended for use in pure oxygen
(lb.in.) (35) and/or oxygen rich systems and should not be selected as
a sealant for chlorine or other strong oxidizing materials.
Breakloose Torque, ISO 10964, Pre-torqued to 5 N·m:
M10 steel nuts and bolts N·m 14 For safe handling information on this product, consult the
(lb.in.) (120) Material Safety Data Sheet (MSDS).
Max. Prevail Torque, ISO 10964, Pre-torqued to 5 N·m: Where aqueous washing systems are used to clean the
M10 steel nuts and bolts N·m 14 surfaces before bonding, it is important to check for
(lb.in.) (120)
compatibility of the washing solution with the adhesive. In
Compressive Shear Strength, ISO 10123: some cases these aqueous washes can affect the cure and
Steel pins and collars N/mm² ≥2.50LMS performance of the adhesive.
(psi) (≥360)
This product is not normally recommended for use on plastics
(particularly thermoplastic materials where stress cracking of
TYPICAL ENVIRONMENTAL RESISTANCE the plastic could result). Users are recommended to confirm
Cured for 1 week @ 22 °C compatibility of the product with such substrates.
Breakloose Torque, ISO 10964, Pre-torqued to 5 N·m:
M10 zinc phosphate steel nuts and bolts
Directions for use
Hot Strength For Assembly
Tested at temperature 1. For best results, clean all surfaces (external and internal)
100 with a Loctite cleaning solvent and allow to dry.
2. If the material is an inactive metal or the cure speed is to
slow, spray all threads with Activator 7471 or
75 7649 and allow to dry.
% RT Strength

3. Shake the product thoroughly before use.

4. To prevent the product from clogging in the nozzle, do not
50
allow the tip to touch metal surfaces during application.
5. For Thru Holes, apply several drops of the product onto
25 the bolt at the nut engagement area.
6. For Blind Holes, apply several drops of the product down
the internal threads to the bottom of the hole.
0 7. Assemble and tighten as required.
0 50 100 150 8. For Sealing Applications, apply a 360° bead of product
Temperature, °C

Henkel Loctite Americas Henkel Loctite Europe Henkel Loctite Asia Pacific
+860.571.5100 +49.89.9268.0 +81.45.758.1810
For the most direct access to local sales and technical support visit: www.loctite.com
 TDS LOCTITE® 222, April-2004

to the leading threads of the male fitting, leaving the first Note
thread free. Force the material into the threads to The data contained herein are furnished for information only
thouroughly fill the voids. For bigger threads and voids, and are believed to be reliable. We cannot assume
adjust product amount accordingly and apply a 360° bead responsibility for the results obtained by others over whose
of product on the female threads also. methods we have no control. It is the user's responsibility to
determine suitability for the user's purpose of any production
For Disassembly methods mentioned herein and to adopt such precautions as
1. Remove with standard hand tools. may be advisable for the protection of property and of persons
2. In rare instances where hand tools do not work because against any hazards that may be involved in the handling and
of excessive engagement length, apply localized heat to use thereof. In light of the foregoing, Henkel Corporation
nut or bolt to approximately 250 °C. Disassemble while specifically disclaims all warranties expressed or implied,
hot. including warranties of merchantability or fitness for a
particular purpose, arising from sale or use of Henkel
For Cleanup Corporation’s products. Henkel Corporation specifically
1. Cured product can be removed with a combination of disclaims any liability for consequential or incidental
soaking in a Loctite solvent and mechanical abrasion damages of any kind, including lost profits. The discussion
such as a wire brush. herein of various processes or compositions is not to be
interpreted as representation that they are free from
Loctite Material SpecificationLMS domination of patents owned by others or as a license under
LMS dated May-18, 1999. Test reports for each batch are any Henkel Corporation patents that may cover such
available for the indicated properties. LMS test reports include processes or compositions. We recommend that each
selected QC test parameters considered appropriate to prospective user test his proposed application before repetitive
specifications for customer use. Additionally, comprehensive use, using this data as a guide. This product may be covered
controls are in place to assure product quality and by one or more United States or foreign patents or patent
consistency. Special customer specification requirements may applications.
be coordinated through Henkel Loctite Quality.
Trademark usage
Storage LOCTITE is a trademark of Henkel Corporation
Store product in the unopened container in a dry location.
Reference 0.3
Storage information may be indicated on the product container
labeling.
Optimal Storage: 8 °C to 21 °C. Storage below 8 °C or
greater than 28 °C can adversely affect product properties.
Material removed from containers may be contaminated during
use. Do not return product to the original container. Henkel
Corporation cannot assume responsibility for product which
has been contaminated or stored under conditions other than
those previously indicated. If additional information is required,
please contact your local Technical Service Center or
Customer Service Representative.
Conversions
(°C x 1.8) + 32 = °F
kV/mm x 25.4 = V/mil
mm / 25.4 = inches
N x 0.225 = lb
N/mm x 5.71 = lb/in
N/mm² x 145 = psi
MPa x 145 = psi
N·m x 8.851 = lb·in
N·mm x 0.142 = oz·in
mPa·s = cP

Henkel Loctite Americas Henkel Loctite Europe Henkel Loctite Asia Pacific
+860.571.5100 +49.89.9268.0 +81.45.758.1810
For the most direct access to local sales and technical support visit: www.loctite.com