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M 190 SPECIFICATIONS FOR MATERIALS
the test apparatus and centered under the diameter and 19.0 mm (¾ in.) in length. Multi-Laboratory Precision-Flow Test-
plunger, the hammer tripped to fall Two specimens shall be used for each The multi-laboratory coefficient of
through a height of 130 2 mm (5⅛ in.) test. These shall be made by pouring the variation of a single test result (a test
upon the head of thb plunger. Not more excess bituminous material from the result in this method has been defined as
than 8 seconds shall elapse from the time specimens for the shock test into split the measurements on two separate
each specimen is removed from the bath brass molds coated with a suitable release specimens) has been found to be 97
until the hammer strikes the plunger. agent (Note 1). percent (Note 2). Therefore, results of
5.3.1.3 Precision-The shock test two properly conducted tests in different
NOTE 1-Mixtures of glycerine and dextrin or
described in this method is defined as a talc, Dow-Corning Stop Cock Grease and laboratories on the same bituminous
determination that at least three of four castor oil-Versamid 900 (100:1 mixture by coating should not differ by more than
separate specimens comprising a single mass heated to 204-232°C (400-450°F) and 275 percent (Note 2) of their average.
test sample will exhibit no cracking to stirred until homogeneous, have proven
NOTE 2-These numbers represent
yield an acceptable result. Analysis of an suitable. Other release agents may be used
respectively the (1S percent) and (D2S
provided results obtained are comparable to
inter-laboratory study (a blind study those obtained when using one of the above.
percent) limits described in ASTM C 670.
carried out by 9 laboratories on 4
NOTE 3-Calculated as described in the
different materials with 3 replicates -of 5.3.2.2 With the corrugated plate held at paragraph on precision of individual
each material) reveals a pass/fail ratio for an angle of 45 degrees with the measurements averaged to obtain a test result
tests on the same material ranging from horizontal, lay each test specimen in a in ASTM C 670.
0.22 to 1.45, with an overall pass/fail corrugation so that its lower end will rest
NOTE 4-These precision statements are based
ratio for all 108 samples (27 samples of exactly along the line scribed 152.4 mm
on results of an interlaboratory test program
each of 4 materials) of 0.54. Further in (6 in.) from the bottom edge of the plate using three replicates of each of four materials.
each of 11, out of the total of 36 cases, and place the test apparatus in an oven Nine laboratories participated in the tests.
where 3 replicate samples of the same maintained at a temperature of 65.5 ±
material were tested in the same 1°C (150 ± 2°F). After 4 hours in the 5.3.2.4 Bias-Since there is no accepted
laboratory, the same laboratory obtained oven, remove the apparatus and reference material suitable for
passing results on one of the 3 replicate specimens and allow to cool to room determining the bias for the procedure in
samples and failing results on the other 2 temperature. Measure the distance from the test method for measuring flow, no
replicate samples or vice versa. the bottom of the corrugated plate to the statement on bias is being made.
5.3.1.4 Bias-Since there is no accepted lower edge of the test specimens. This 5.3.3 Imperviousness Test-A 25percent
reference material suitable for distance subtracted from 152.4 mm (6 solution of sulphuric acid, a 25percent
determining the bias for the procedure in in.) determines the amount of flow. solution of sodium hydroxide, and a
the test method for measuring shock, no 5.3.2.3 Precision: saturated solution of sodium chloride
statement on bias is being made. shall be held in separate valleys of the
Single Operator Precision-Flow Test-The
coated corrugations for a period of 48
5.3.2 Flow Tests-The apparatus for single operator coefficient of variation
hours during which time no loosening or
making the test shall consist of _for a single test result (a test result in
separation of the bituminous material
corrugated brass plate approximately 0.8 this method has been defined as the
from the galvanizing shall have taken
mm (0.03 in.) thick, 203.2 mm (8 in.) measurements on two separate
place. This test may be made on an uncut
long and 101.6 nun (4 in.) wide, with specimens) has been found to be 65
section of pipe provided provision is
corrugations running lengthwise of the percent (Note 2). Therefore, two properly
made to prevent excessive evaporation of
plate, and a metal support to hold the conducted tests by the same operator
the three test solutions.
plate on a 45-degree angle with the (each consisting of measurements on two
horizontal. The corrugations shall have a specimens from the same sample) should 5.3.3.1 Precision and Bias-No statement
crest to crest dimension of 15.9 mm (⅝ not differ by more than 184 percent (Note is made about either the precision or the
in.) and a depth of 4.8 mm (3/16 in.). A 2) of their average. The range (difference bias of the imperviousness test since the
line shall be scribed 152.4 mm (6 in.) between the highest and lowest) of the result only states whether there is
from the lower edge. two individual measurements comprising conformance to the criteria for success
a test result should not exceed 260 specified in the procedure.
5.3.2.1 Test specimens shall be in the
form of cylinders 9.5 mm (⅜ in.) in percent (Note 3) of the average of the
two.
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