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Wear
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a r t i c l e i n f o a b s t r a c t
Article history: This paper describes future trends in surface metrology. Measurement techniques are briefly mentioned.
Received 23 April 2010 A special attention was paid to tactile and optical methods. Selected problems of surface topography
Received in revised form 31 May 2010 characterization are described. The effects of sampling and filtering on surface topography representation
Accepted 2 June 2010
are analysed. Structured surfaces are becoming both technologically and economically critical. Therefore
Available online 11 June 2010
their description is a problem of a great practical importance. Multi-process textures are very important
from functional point of view. Various methods of their description are compared. Surface texturing as
Keywords:
a means for enhancing tribological properties of frictional pairs started to be extremely popular from
Surface topography
Measurement
for about last 10 years. The effects of surface texturing on improving tribological properties of sliding
Analysis assemblies are analysed. The other influences of surface topography are mentioned in this paper.
Applications © 2010 Elsevier B.V. All rights reserved.
1. Introduction 2. Metrology
The last half century of geometrical aspects of surfaces metrol- 2.1. Measurement techniques
ogy was extremely rich in events related to equipments design
as well as data treatments dealing with parameters and standard- Despite a great development of optical and other techniques a
ized rules. Therefore it is difficult, pretentious and also dangerous tactile profilometer is still the most common roughness measuring
to tempt the reliable prediction a fortiori to be counterpart of device in mechanical industry. Yet, since Abbott and Firestone’s [1]
the 12th International Conference on Metrology and Properties construction from 1933 it has gone a long way. First of all mod-
of Engineering Surfaces. Specific contributions of British, German, ern software allows computing of approximately 300 parameters
United States of America, Russian, French and Polish schools caused of roughness profile and dozens of topography parameters. Rough-
considerable progress of techniques of measurement, methods of ness can be measured on 200 mm length and 100 mm width with
characterization with development of European Union and Inter- the deviation of guide equal to the fraction of micrometers, and fur-
national standards. ther software support of accuracy can be applied. In this case the
Standardization processes will be probably increased in terms of slide is measured by a laser interferometer and its errors are col-
methods of measurements and data treatments for specific appli- lected in the microprocessor’s system and used for the correction of
cations due to the externalization, diversification of products and indication. Besides the measuring instruments often offer simulta-
under contractor’s strategies. Particular attention is paid to cre- neously measurement of roughness and outline with greater range
ative process of new sensors for explicit applications in terms of – even above 2 mm with 0.6 nm resolution. The interesting element
better or less known transfer functions due to materials natures of this device is a probe – magneticically fixed, which prevents
and range of topographical features. The scanning systems of dif- damage (break), because during any impact or overload of the part,
ferent device designs and assemblies will be analyzed in context of the diamond needle is separated from the body on a three points
precision and reliability taking into account especially the contri- magnetic holder.
butions of tribology. The new applications of surface metrology in Additionally the probe is equipped with an AM transmitter and
traceability of surfaces, bionics, criminology and medicine will be a receiver, which are used for communication with a central pro-
analyzed. cessing unit, and a simple memory chip. All of these assemblies of
construction are together called an intelligent probe. In the mem-
ory the parameters of the probe are stored and sent to the controller
after connecting to the holder. The memory contains also the data
∗ Corresponding author. Tel.: +33 478433383. which are used to protect the probe during so called soft lowering. It
E-mail address: Thomas.Mathia@ec-lyon.fr (T.G. Mathia). limits the speed of the free falling of the measurement arm. Thanks
0043-1648/$ – see front matter © 2010 Elsevier B.V. All rights reserved.
doi:10.1016/j.wear.2010.06.001
T.G. Mathia et al. / Wear 271 (2011) 494–508 495
to this, the probe does not strike at the end of a rapid fall, which
could cause damage. Immediately after the probe is in contact with
the lower measuring surface, the function of soft dropping is auto-
matically turned off and the device continues the measurement.
Next possible solution is the application of the measurement probe Fig. 3. Principle of a vertical scanning interferometry [11].
with bidirectional pressure force – up and down. It allows to mea-
sure, using the same probe, the roughness on the upper and lower
surface of a hole, and in conjunction with an incremental linear
encoder in a measuring column allows measurement of small inside can be used successfully in roughness measurements in preven-
diameters in a vertical axis. It is especially useful in the automobile tive inspection, and their vertical measuring range reaches one
industry, in the production of pumps and injectors, where with- micrometer.
out fears for probe damage CNC procedures to measure roughness, Modern interferometers, used in roughness measurements,
waviness and outline in small holes could be used (Fig. 1). are systems which are applying white light. In contradiction to
As a result from the analysis presented above, the principle of monochromatic light it distinguishes discontinuity of the surface
contact measurement and the methods of its making have not been for example deep valleys or high steps. The most popular interfero-
changed for years. However development of microelectronics and metric measurement techniques are phase-shifting interferometry
computer techniques creates opportunities to increase the range PSI, vertical scanning interferometry VSI and enhanced vertical
and the resolution of devices and to introduce facilities for opera- scanning interferometry EVSI. PSI uses a monochrome light source
tors to reduce their chances to make mistakes. It seems likely that and generally is applied to analysis of a very smooth surface,
it will be the trend in development of stylus surface measurement because this method is characterized by sub-nanometer resolu-
in the next years. tion. On the other hand it suffers from phase-ambiguity problems,
Measurements based on a stylus profilometer in 3D surface which limits PSI usability to a surface discontinuity not higher
topography of the surface are time consuming, which is a signif- than /4, where is the wavelength of the light used. Besides, the
icant limitation. A possibility of overcoming this inconvenience is monochrome light source limits using PSI to ranges where contin-
spiral sampling [3] (see Fig. 2). uous fringes can be obtained. In order to overcome this difficulty a
Irrespective of the contact devices, constructions based on opti- new technique called Multiple Wavelength Interferometry (MWI)
cal phenomena are being developed. Therefore the optical methods has been developed which has extended high-difference limitation
have been described in-depth in the scientific literature, e. g. in successfully. In this method two wavelengths are selected, which
Bennett’s [5,6] Tiziani’s [7], Leonhardt’s [8] and others articles. allow the user to increase the dynamic range and at the same time
New solutions have introduced CCD lines and arrays to detect the to keep the resolution constant. Further increasing of the dynamic
light signal, used i.e. in light scattering methods. These techniques range is possible when white light is applied (VSI).
Then the continuity of fringes is not so crucial also, more impor-
tant is finding a focus. The principle of vertical scanning is presented
in Fig. 3. Unfortunately, the resolution of VSI is in the nanometers
range, not in fractions of nanometers. The advantages of PSI and VSI
are combined in the EVSI technique, also called white light inter-
ferometery with phase-shifting [9]. First of all every pixel is found
in the optimal position of the objective for which this point of the
surface is in the focus of the optical system, so in this position the
distribution of intensity of the interference signal has a maximum.
Secondly, to analyse the intensity around the point of focus a PSI
technique is used, which allows to obtain better resolution than in
VSI [10].
Interferometers and microscopes are combined in interferomet-
ric microscopy. Through that connection very good resolution and
significant vertical range can be obtained. The interferometer is
responsible for scanning on a nano scale, and the microscopy head
is displaced on a micro-scale giving a vertical range even above
1 mm.
Descriptions of the operation of initial construction of scientific
interferometric microscopes can be found in Wyant’s et al. [12] and
Fig. 2. Application of spiral sampling [4]. Forman’s [13] articles.
496 T.G. Mathia et al. / Wear 271 (2011) 494–508
Fig. 11. Dependencies between height parameters: (a) Rvk and Rvq and (b) Rpq and Rk [78].
lated [69]. This method attempts to approximate this curve by three correlated with honing variables (Rpq with grit size of plateau hon-
straight lines (Fig. 10a). The straight line is fitted to the central 40% ing stone, Rvq with grit size of coarse honing stones, Rmq with
of the material ratio curve. The distance between the intercepts plateau honing time) than parameters from ISO 13565-2 stan-
of this line with the height axes is defined as the Rk parameter. dard (Rk family). The authors of Ref. [77] found that increasing
This arbitrary construction is in general use in Europe and seems plateau honing time decreased plateau roughness, while increas-
to produce satisfactory results. The parameter Rk is a measure ing pressure during coarse honing increased valley roughness, but
of roughness height after a running-in process, but the parame- these changes could not be correlated with roughness parame-
ters Rvk and Mr2 are measures of capacity of oil accumulation in ters. In slide honing research the effect of honing parameters on
the honing valleys. Decreasing Rk, oil consumption decreases, but cylinder liner surface topography was studied [78]. Surface topog-
increasing Rvk the seizure resistance increases. The honing process raphy parameters were response variables. It was found from the
could be controlled by Rk parameters according to Nielsen [70]. experiment that the coarse honing pressure pv is an important
In Zipin’s opinion [71], this approach can be misleading since the parameter of the honing process. It almost defines the final val-
material ratio curve of normally distributed random surface profiles ley depth. The plateau honing time t is the second substantial
exhibits a variation of slope. In addition some parameters found machining parameter. The effect of plateau honing pressure on
in this standard are non-synonymous [72]. It is always difficult to cylinder liner profile roughness parameters is negligible. The Rk
achieve all the parameters from ISO 13565-2 standard within a cer- and Rvk parameters depend on both applied machining parame-
tain range and the operator’s experience is relied upon. In practice, ters; they are proportional to pv , but inversely proportional to t.
Mr2 is considered as an important parameter among the bearing Increasing plateau honing time decreases plateau roughness Rpq,
area parameters and is assigned a higher weighting of 50%, while but increasing coarse honing pressure decreases valley roughness
Rk, Rvk, Rpk and Mr1 are assigned 30%, 15%, 4% and 1% respec- Rvq. Increasing plateau honing time and decreasing coarse honing
tively [73]. The work described in Reference [74] is an investigation pressure causes increases of Rmr2 and Rmq. The presented results
carried out to identify the significant honing parameters and their [77,78] suggest that the optimum parameter set has not been yet
values for different honing operations. It was found that honing found.
pressure played an important role in controlling the liner finish. The statistical connections among parameters from the two
The Ra parameter is important in all stages of the honing process, analysed standards were analysed using linear correlation coeffi-
while it can be replaced by Rk in finish honing and plateau honing cients [78–81]. However it is hardly possible to find what parameter
operations. The Mr2 parameter is to be controlled in the finish and set is the best. For example, it was found that within the Rk fam-
plateau honing operations. Data mining approach was used in the ily, the independent pairs of parameters were Rpk and Rvk, Rk and
investigation to select significant honing parameters and their lev- Rmr1, Rk and Rmr2 [78]. The Rk parameter was correlated with
els considering two important bearing area parameters Rk and Mr2 Rpk ( = 0.72), but correlation between Rmr1 and Rmr2 was the
together to achieve the required surface topography [75]. greatest ( = 0.97). Within the Rq family, the absolute values of cor-
The ISO committee incorporated another alternative way of relation coefficients were smaller than 0.5. Between the parameter
characterising a two-process surface [76,50] with a sounder the- families, Rmr1 and Rmr2 were highly correlated with Rmq, and the
oretical basis. Honing is a process which is known to produce a respective peak and valley parameters are also highly correlated
Gaussian distribution of surface heights. A process of coarse honing (see Fig. 11).
followed by fine honing will superimpose one Gaussian distribu- Other parameters from the Abbott curve exist in the CNOMO
tion on another. If the resulting cumulative distribution is plotted standard. These are: the parameter Cr: running-in criterion calcu-
on a normal probability scale, it is shown as two straight lines of lated between the material ratios 1 and 33%, Cf: operating criterion
different slopes. The Rpq parameter is the slope of a linear regres- calculated between the material ratios 15 and 75% and Cl: lubri-
sion performed through the plateau region, but Rvq is similarly cation criterion calculated between the material ratios 45 and 99%
defined for the valley region. The intersection point on the normal [80].
probability graph of abscissa Rmq defines the separation of plateau Image-processing technique has also been used to characterise
and base textures (see Fig. 10b). Since this approach independently plateau-honed surfaces [81–83] but it is not used in industry to
characterises the components of the multi-process texture, pro- control the honing process.
cess control can be much more specific. This method can be used to
study the running-in process. It is conceptually simpler and more 4. Applications
elegant than the method described previously (ISO 13565-2), but
there is difficulty in computing the parameters Rpq, Rvq and Rmq. 4.1. The effect of surface texturing on improving tribological
Connections among parameters contained in ISO 13565-2 and properties of sliding assemblies
ISO 13565-3 standards and plateau honing machining parameters
have been analysed [72,77]. Malburg and Grant [72] found that Surface texturing as a means for enhancing tribological prop-
parameters contained in ISO 13565-3 (Rq family) were more highly erties of frictional pairs is well known for many years. However it
502 T.G. Mathia et al. / Wear 271 (2011) 494–508
Fig. 12. Schematic presentation of various variants of cylinder structures; from left to right: one-process honing, plateau honing, helical honing, laser honing, oil pockets
[99].
started to be extremely popular for about the last ten years. Since bore [92]. The increased presence of cold work material on cylinder
then a growth of the number of publication has been observed. liners due to the introduction of diamond honing is undesirable.
They deal with a variety of aspects of surface texturing from the- However in the engine tests, the diamond honed liners showed
oretical predictions to experimental research. Various techniques good performance [93]. The relative basic honing fluting with con-
were employed including machining, ion beam texturing, etch- ventional surfaces (honing angle about 45◦ ) was considered to be
ing techniques and laser texturing. The dimples (also known as sensible for many decades. However, it was found that the reduc-
micropits, holes, oil pockets or cavities) can serve either as a tion of wear and scuffing tendency can be achieved by altering
micro-hydrodynamic bearing in cases of full or mixed lubrication, the geometry of basic honing valleys. The honing grooves were
a micro-reservoir for lubricant in cases of starved lubrication con- arranged in the direction of the piston in an elongated spiral (heli-
ditions or a micro-trap for wear debris in either lubricated or dry cal honing–honing angle about 140◦ ) [94]. Various endurance tests
sliding [84,85]. The most familiar and earliest commercial applica- on 6-cylinder production engines of up to 3000 running hours have
tion of surface texturing is that of cylinder liner honing. At first, the proved the advantages of helical honing. The wear in the reversal
recommended cylinder surface after honing was very smooth since zone was reduced by approximately 40% as compared to the pre-
it showed high wear resistance during running-in. Considerable vious production plateau honing process [95]. The other proposal
progress in engine construction caused a great scuffing inclination is the creation of cylinder surface structures by a modified honing
of the smooth cylinder surface. Only rough surfaces have a higher process followed by laser texturing. This represents a very promis-
load-carrying capacity [86]. Running-in wear studies, conducted by ing approach for reducing both wear and friction losses without
the authors of Ref. [87] on a compression ignition engine showed an increase of the oil consumption. It was found that volumet-
that the linear wear of the cylinder increased with increase in its ric wear of the laser-textured surface was reduced in comparison
initial surface roughness height. Rough surfaces wear rapidly with- to the standard plateau-honed surface [96]. Laser texturing on a
out seizure during running-in to promote quick performance, so an cylinder surface was used in order to minimise risk of seizure [97].
initial surface finish of the cylinder of 0.8 m Ra was recommended. Another possibility is the creation of a deterministic cylinder struc-
Scientists made efforts to find an optimum geometrical cylinder ture by laser honing. It ensures 2–3 times smaller oil consumption
structure. A plateau-honed cylinder surface ensures simultane- and smaller wear of piston rings and cylinder during test of 330 h
ously the sliding properties of a smooth surface and a great ability duration in comparison to plateau honing [98].
to maintain oil on a porous surface. It was found that plateau sur- Fig. 12 presents schemes of different cylinder liner surfaces.
faces ensured shortening of the running-in and lower wear in this Fig. 13 shows the effect of surface texturing on volumetric wear
period. Campbell [88] compared two honed surfaces. They were of cylinder from internal combustion engine.
characterised by the same roughness height and various shapes The other possibility is the laser texturing of piston rings. Exper-
of the ordinate distribution. Analysis indicated that to achieve a imental tests, which were performed on a laboratory reciprocating
30% material ratio in the running engine twice the volume of metal test rig showed that a friction reduction of up to 25% can be obtained
would be worn from a typical (one-process) surface than from a by partial texturing of cylindrical face rings in comparison to un-
plateau surface. Pawlus [89] analysed the effect of surface topogra- textured rings of barrel shape [100]. It was found that partial laser
phy of honed cylinders on their wear resistance during running-in. texturing piston rings produced up to 4% lower fuel consumption
He found that the values of the local linear wear of cylinders hav- in an internal combustion engine, while no traceable change in the
ing the same roughness height were proportional to the emptiness exhaust gas composition or smoke level was observed [101].
coefficient Rp/Rt. An increase in the initial roughness height also The applications of texturing include also: piston pin, disk
caused an increase in cylinder wear intensity. Jeng [90] found that brakes, thrust bearings, journal bearings, mechanical face seals, gas
plateaued surfaces more quickly obtained constant wear intensity
than Gaussian surfaces of the same height standard deviation, so
wear of plateaued surfaces during steady-state should be smaller.
These results were confirmed by the investigation of Grabon et al.
[91].
In order to reduce engine oil consumption and running-in wear
a high percentage contact area of cylinder liner is needed. It can
be done by reducing the base honing valleys depth (slide honing).
The main objectives in developing this technique were: productiv-
ity comparable with that of conventional honing or plateau honing,
a high degree of reliability of the process itself and in mass produc-
tion conditions, long tool life, minimum deformation in the honed
surfaces, i.e. minimal dislocations in the boundary layer and the cre-
ation of a uniform and consistent surface over the whole cylinder Fig. 13. The effect of kind of machining on volumetric wear (after [96]).
T.G. Mathia et al. / Wear 271 (2011) 494–508 503
Fig. 18. Comparison of bottom side of cross-country (a) and downhill (b) skies [152].
It is worth showing some more examples of surface measure- scattering, although acoustic sensors [153] or AFM are also used.
ment application. Let’s start with asphalt pavement analysis [144]. These methods allow for testing of paper for special applications,
In this case roughness conventionally includes wavelengths in the analysis of old prints and marks of physicochemical impurity or
range 0.1–100 m and amplitudes from 1 to 100 mm. Lower com- analysis connected with the deposition of a drop of ink from the
ponents are called texture macro and micro. Pavement roughness printer. Roughness of the paper has influence on the deposition of
has influence on the vehicles using it, therein on correctness of tire the ink component, which causes non-uniformity of colour print-
functioning, their friction and vibration [145]. Pavement conditions ing [154]. On paper with higher roughness uniformity and quality
affect also the distribution of stresses in the subsurface layer, and of printing is worse. Fig. 19 shows a surface of rough paper. Applica-
this is the result of e.g. roughness of the road-metal used [146]. Dif- tion of the topography parameters of the surface allows to ascertain
ferent techniques are used for asphalt roughness analysis. A review
was published in article [147] and it refers to highways. Therefore
– similarly to machine engineering – profilometers with different
accuracies depending on the requirements can be used and opti-
cal systems instead of stylus heads, for example autofocus laser
systems or sensors dependent on sonic wave reflection.
Another possibility is using an acoustic transducer or an image
analysis system [148], which can be for example an optical scanner.
An image of the surface topography of asphalt pavement obtained
with the help of this device is shown in Fig. 17. In this case, red
fields are up to 7 mm above mean plane, while blue ones are 3 mm
below.
Equally important as a road in asphaltic concrete are roads
of steel, i.e. rails. Papers [145,146,149,150] are devoted to their
roughness analysis. Especially important are places, where vio-
lent braking – contact of the brake block with the rail occurs. This
causes formation of roughness, which has an influence on the phe-
nomenon proceeding on the surface and on the subsurface layer of
the rail during its contact with the wheel band. Just as a result of
roughness local exceeding of boundaries conditions of mechanical
strength and cracking of the material can occur, which can have
an effect with very serious consequences including accident. It was
observed that roughness of the wheel band is one of the factors,
Fig. 19. Surface of rough paper [155].
which cause locomotive derailment during switching tracks, if the
value of the roughness parameters after switching does not meet
the requirements.
The next important branch in this context is cloth and material
manufacturing, where roughnesses are analyzed especially when
special requirements are placed on them, for example keeping
warm or ensuring the aesthetic properties of a car interior. In such
tests stylus profilometry does not find an application, whereas opti-
cal techniques are used for example a laser sensor [151]. In sports
popularity was gained by an analysis of the roughness of the under-
side of skis [152]. Fig. 18 presents the surface of the underside of
cross-country (a) and downhill (b) skis. In this second case as a
result of contact of skis with snow at high speed a lot of heat is pro-
duced and snow is melted, hence grooves should quickly remove
water in order that the speed of the downhill run does not decrease.
Surface topography analysis is often used in the paper industry.
Because of the delicacy of the investigated surface stylus mea-
surements are replaced by other techniques mainly based on light Fig. 20. Topography image of a banknote.
506 T.G. Mathia et al. / Wear 271 (2011) 494–508
Fig. 21. Profiles represents marks of the same gun on two different shots [158].
that surfaces with similar values of some parameters may have Other effects of surface topography are mentioned in this paper.
totally different appearances and performances. Examples are only a selection of applications of the analysis of the
On banknote surfaces except overprint also three-dimensional surface topography, which gains bigger and bigger popularity both
special marks are plotted, which make it difficult to counterfeit in mechanical engineering as well as in other branches which are
banknotes and allow to evaluate their authenticity. An image of not connected with traditional engineering experience. Its increas-
the 50D banknote fragment is shown in Fig. 20. ing availability and commonality favors searching further areas of
The next application is analysis of the surface of shot fired from application and possibilities of interdisciplinary researches, often
the gun, which is used for gun identification [156]. In this branch very attractive for workers from distant branches of science.
the American National Institute of Standards and Technology (NIST)
has the lead e.g. It leads a program of model gun cartridge produc- References
tion, where it is fired from each gun directly after manufacturing
and on which each gun leaves individual marks [157]. This car- [1] E.J. Abbott, F.A. Firestone, Specifying surface quality, Mech. Eng. 55 (1933)
569–572.
tridge is used for the identification of guns, because the marks of
[2] 8000T Nanoscan, Hommel-Etamic Jenoptik, Schwenningen, 2008.
the gun barrel are impressed on its surface. The marks are measured [3] M. Wieczorowski, Spiral sampling as a fast way of data acquisition in surface
as the roughness of each gun which is as adequate as identification topography, Int. J. Mach. Tools Manuf. 41 (2001) 2017–2022.
[4] J. Song, The effect of Gaussian filter long wavelength cutoff c in topography
as finger prints are for people [158]. Marks from the same gun for
measurements and comparisons, in: Proc XXI ASPE AM, 2006, pp. 387–390.
two different shots are shown in Fig. 21. Both profiles are compat- [5] J.M. Bennett, Overview: sensitive techniques for surface measurement and
ible with each other, so we can assume that the shots were fired characterization, Proc. SPIE 1573 (1991) 152–158.
from the same gun. Saving this profile in the database allows fast [6] J.M. Bennett, Recent developments in surface roughness characterization,
Meas. Sci. Technol. 3 (1992) 1119–1127.
identification in future. For correct estimation of the profiles of the [7] H.J. Tiziani, Optical methods for precision measurements, Opt. Quant. Elec-
identified shots the influence of the filtration of the waviness on tron. 21 (1989) 256–282.
the result of the comparison of two shots [4] is also analyzed. [8] K. Leonhardt, et al., Optical methods of measuring rough surfaces, Proc. SPIE
1009 (1988) 22–29.
[9] M. Zecchino, Enhanced Vertical Scanning Interferometry a Novel Solution for
5. Summary Difficult to Measure Samples, Veeco, Tucson, 2005.
[10] A. Harasaki, et al., Improved vertical scanning interferometry, Appl. Opt. 39
(2000) 2107–2115.
It seems likely that stylus methods of surface topography mea- [11] J.C. Wyant, Optical Testing and Testing Instrumentation, College of Optical
surement will be replaced by optical methods which make it Sciences, University of Arizona, 2009.
[12] J.C. Wyant, et al., An optical profilometer for surface characterization of mag-
possible to measure surface stereometry in a short time. White light
netic media, ASLE Trans. 27 (1984) 101–113.
interferometry and confocal microscopes are the most promising [13] P.F. Forman, The ZYGO interferometer system, Proc. SPIE 129 (1979) 41–48.
techniques. However because of known susceptibility to measure- [14] J. Schmit, J.C. Wyant, Large Field of View High Spatial Resolution Surface
Measurements, Veeco, Tucson, 2002.
ment errors the stylus technique will be in future treated as a
[15] M. Conroy, Advances in thick and thin film analysis using interferometry, in:
reference technique. The Ideal solution is a combination of tactile Proc. 11th Conf. Met&Props, Huddersfield, 2007, pp. 35–39.
and optical methods. Scanning probe microscopes and among them [16] M. Zecchino, Optical profiling: applications expand, Photonics Spectra 37
especially atomic force microscopy (AFM) are the best techniques (2003) 68–72.
[17] M. Zecchino, et al., Advances in Optical Profiling Open New Applications,
to measure very smooth surfaces. Veeco, Tucson, 2003.
There are still problems in surface topography characterization. [18] J. Armstrong, Talysurf CCI – How it Works, Taylor Hobson, Leicester, Anglia,
Support is expressed for current standard proposals for a consoli- 2005.
[19] T. Wilson, Confocal Microscopy, Academic Press, San Diego, 1990.
dated 3D parameters set. Multi-process textures are becoming very [20] D.K. Hamilton, T. Wilson, Surface profile measurement using the confocal
important from the tribological point of view. Various methods of microscope, J. Appl. Phys. 53 (1982) 5320–5322.
their description are included in ISO standards. It was concluded [21] H. Perrin, et al., Profilometry by spectral encoding of the optical axis, Proc.
SPIE 2340 (1994) 366–374.
that an optimum parameter set was not found yet. The problems [22] H.J. Tiziani, H.-M. Uhde, Three dimensional image sensing by chromatic con-
of sampling and filtering of multi-process structures, especially focal microscopy, Appl. Opt. 33 (1994) 1838–1843.
those having wide valleys are not solved yet. Structured surfaces [23] G. Molesini, Focus-wavelength encoded optical profilometer, Opt. Commun.
49 (1984) 229–233.
are becoming both technologically and economically critical. They
[24] ISO/TC 213N 792, 2005.
should be described by special parameters, where a segmentation [25] Confocal white light sensor, Hommel-Etamic Jenoptik, Schwenningen, 2007.
method can be helpful. [26] G. Binning, et al., Atomic force microscope, Phys. Rev. Lett. 56 (1986) 930–933.
[27] G. Binning, et al., Surface studies by scanning tunneling microscopy, Phys.
The effects of surface texturing on improving tribological prop-
Rev. Lett. 49 (1982) 57–61.
erties of sliding assemblies are very important. The oil pockets can [28] M. Stedman, Limits of surface measurement by optical probes, Proc. SPIE 1009
serve either as a micro-hydrodynamic bearing in cases of full or (1988) 62–67.
mixed lubrication, a micro-reservoir for lubricant in cases of starved [29] M. Stedman, K. Lindsey, Limits of surface measurement by stylus instruments,
Proc. SPIE 1009 (1988) 56–61.
lubrication conditions or a micro-trap for wear debris in either [30] D.J. Whitehouse, J.F. Archard, The properties of random surface of significance
lubricated or dry sliding. in their contact, Proc. R. Soc. A 316 (1970) 97–121.
T.G. Mathia et al. / Wear 271 (2011) 494–508 507
[31] T. Tsukada, S. Sasajima, An optimum sampling interval for digitising surface [66] C.J. Evans, B.J. Bryan, “Structured”, “textured” or “engineered” surfaces, CIRP
asperity profiles, Wear 83 (1982) 119–128. Ann. 48/2 (1999) 541–556.
[32] D.Y. Yim, S.K. Kim, Optimum sampling interval for Ra surface measurement, [67] L. Blunt, X. Jiang, P. Scott, Structured surfaces: a new paradigm in surface
Proc. Inst. Mech. Eng. C205 (1991) 139–142. metrology, in: XII International Colloquium on Surfaces, Chemnitz, 2008, pp.
[33] J.-J. Wu, Spectral analysis for the effect of stylus tip curvature on measuring 403–410.
rough surfaces, Wear 230 (1999) 194–200. [68] X. Jiang, P. Scott, D. Whitehouse, L. Blunt, Paradigm shifts in surface metrology,
[34] T.Y. Lin, L. Blunt, K.J. Stout, Determination of the proper frequency bandwidth part II: the current shift, Proc. R. Soc. 463 (2005) 2049–2071.
for 3-D topography measurement using spectral analysis. Part I: isotropic [69] H.J. Bohm, Parameters for evaluating the wearing behaviour of surfaces, Int.
surface, Wear 166 (1993) 221–232. J. Mach. Tools Manufact. 32 (1/2) (1992) 109–113.
[35] W.P. Dong, E. Mainsah, K.J. Stout, Determination of appropriate sampling con- [70] H.S. Nielsen, New approaches to surface roughness evaluation of special sur-
ditions for three-dimensional microtopography measurement, Int. J. Mach. faces, Precision Eng. 10 (1988) 209–213.
Tools Manufact. 36/12 (1996) 1347–1362. [71] R.B. Zipin, Analysis of the Rk surface roughness parameter proposals, Precision
[36] P. Pawlus, D.G. Chetwynd, Efficient characterization of surface topography in Eng. 12/2 (1990) 106–108.
cylinder bores, Precision Eng. 19 (1996) 164–174. [72] M.C. Malburg, M.B. Grant, The Characterization of Two-process Surface Tex-
[37] R. Ohlsson, B.-G. Rosen, T. Pulkkinen, M. Jonasson, Practical consideration ture Using the Cumulative Gaussian Probability Distribution, ISO Paper, 1992.
when measuring 3D surface roughness, Zagadnienia Eksploatacji Maszyn [73] C.X. Feng, X. Wang, Z. Yu, Neural network modeling of honing surface rough-
99–100 (1994) 422–429. ness parameters defined by ISO 13565, J. Manuf. Syst. 21/5 (2003) 395–408.
[38] T.R. Thomas, B.-G. Rosen, Determination of the optimum sampling interval [74] M. Kanthababu, M.S. Shunmugam, M. Singaperunal, Identification of signif-
for rough contact mechanics, Tribol. Int. 33 (2000) 601–610. icant parameters and appropriate levels in honing of cylinder liners, Int. J.
[39] P. Pawlus, Digitisation of surface topography measurement results, Measure- Mach. Mach. Mater. 5/1 (2009) 80–96.
ment 40 (2007) 672–686. [75] M. Kanthababu, M.S. Shunmugam, M. Singaperunal, Selection of plateau hon-
[40] B.-G. Rosen, Towards optimised sampling in surface roughness, in: XII Inter- ing parameters using data mining approach, in: International Conference
national Colloquium on Surfaces Chemnitz (Germany), 2008, pp. 383–392. on Computational & Experimental Engineering Sciences, Indian Institute of
[41] S. Brinkmann, H. Bodschwinna, Advanced Gaussian filters, in: L. Blunt, X. Jiang Technology, Madras, Chennai, India, 2005, pp. 3328–3333.
(Eds.), Advanced Techniques for Assessment Surface Topography, Kogan Page [76] M.C. Malburg, J. Raja, Characterization of surface texture generated by
Science, London/Sterling, 2003, pp. 62–89. plateau-honing process, CIRP Ann. 42/1 (1993) 637–640.
[42] M. Krystek, Discrete linear profile filters, in: X International Colloquium on [77] C. Anderberg, P. Pawlus, B.-G. Rosen, T.R. Thomas, Alternative description of
Surfaces, Chemnitz, Germany, 2000, pp. 145–152. roughness for cylinder liner production, J. Mater. Process. Technol. 209 (4)
[43] M. Numada, T. Nomura, K. Yanagi, K. Kamiya, H. Tashiro, High-order spline (2009) 1936–1942.
filter and ideal low-pass filter at the limit of its order, Precision Eng. 31 (2007) [78] P. Pawlus, T. Cieslak, T. Mathia, The study of cylinder liner plateau honing
234–242. process, J. Mater. Process. Technol. 209 (20) (2009) 6078–6086.
[44] H. Hanada, T. Saito, M. Hasegawa, K. Yanagi, Sophisticated filtration tech- [79] B.-G. Rosen, C. Anderberg, R. Ohlsson, Parameter correlation study of cylinder
nique for 3D surface topography data of rectangular area, Wear 264 (2008) liner roughness for production and quality control, Proc. IMechE, Part J. J. Eng.
422–427. Manuf. 222 (2008) 1–13.
[45] P. Dobrzański, P. Pawlus, Gaussian regression robust filtering on the surface [80] L. Sabri, M. El Mansori, Process variability in honing of cylinder liner with
topography measurement, in: Proceedings of 10th International Conference vitrified bonded diamond tools, Surf. Coatings Technol. 204 (6–7) (2009)
“Metrology and Properties of Engineering Surfaces”, Saint-Etienne (France), 1046–1050.
2005, pp. 133–143. [81] E. Mainsah, J.A. Greenwood, D.G. Chetwynd (Eds.), Metrology and Properties
[46] F.R. Hampel, E.M. Ronchetti, P.J. Rousseeuw, W.A. Stahel, Robust Statistics, J. of Engineering Surfaces, Springer-Verlag, Berlin, 2001.
Wiley & Sons, New York, 1985. [82] F. Puente Leon, Evaluation of honed cylinder bores, Ann. CIRP 51 (2002)
[47] H. Li, X. Jiang, Z. Li, Robust estimation in Gaussian filtering for engineering 503–506.
surface characterization, Precision Eng. 28 (2004) 186–193. [83] E. Decencierre, D. Jeulin, Morphological decomposition of the surface topog-
[48] H. Li, C.F. Cheung, X.Q. Jiang, W.B. Lee, S. To, A novel Gaussian filtering method raphy of an internal combustion engine cylinder to characterize wear, Wear
for the characterization of surface generation in ultra-precision machining, 249 (2001) 482–488.
Precision Eng. 30 (2006) 421–430. [84] B. Nilsson, B.-G. Rosen, T.R. Thomas, D. Wiklund, L. Xiao, Oil pockets and
[49] J. Kumar, M.S. Shunmugam, Fitting of robust reference surface based on least surface topography: mechanism of friction reduction, in: XI International
absolute deviations, Precision Eng. 31 (2007) 102–113. Colloquium on Surfaces, Chemnitz (Germany), 2004 (Addendum).
[50] D.J. Whitehouse, Assessment of surface finish profiles produced by multi- [85] I. Etsion, State of the art in laser surface texturing, ASME J. Tribol. 125 (2005)
process manufacture, Proc. Inst. Mech. Eng. 199/4 (1985) 263–270. 248–253.
[51] A.A. Torrance, A simple datum for measurement of the Abbott curve of a [86] L. Wiemann, Die Bildung von Brandspuren auf den Lauflachen der Paarung
profile and its first derivative, Tribol. Int. 30/3 (1997) 239–244. Kolbenring-Zylinder in Verbrennungsmotoren, Motortechnische Zeitschrift
[52] L. Tholath, V. Radhakrishnan, Three-dimensional filtering of engineering sur- 32 (2) (1971) 43–49.
faces using envelope system, Precision Eng. 23 (1999) 221–228. [87] A.V. Sreenath, N. Raman, Running-in wear of a compression ignition engine:
[53] V. Srinivasan, Discrete morphological filters for metrology, in: Proceedings factors influencing the conformance between cylinder liner and piston rings,
of the 6th IMEKO ISMQC Symposium on Metrology and Quality Control in Wear 38 (1976) 271–289.
Production, TU Wien, Austria, 1988, pp. 623–628. [88] J.C. Campbell, Cylinder bore surface roughness in internal combustion
[54] P.J. Scott, Scale-space technique, in: X International Colloquium on Surfaces, engines: its appreciation and control, Wear 19 (1972) 163–168.
Chemnitz, Germany, 2000, pp. 153–161. [89] P. Pawlus, A study on the functional properties of honed cylinder surface
[55] M. Dietzsch, C. Frenzel, M. Gerlach, S. Groeger, D. Hamann, Consequences of during running-in, Wear 176 (1994) 247–254.
the GPS standards to the assessment of surface topography, in: XI Interna- [90] Y. Jeng, Impact of plateaued surfaces on tribological performance, Tribol.
tional Colloquium on Surfaces, Chemnitz, Germany, 2004, pp. 1–12. Trans. 39/2 (1996) 354–360.
[56] M. Krystek, Morphological filters in surface texture analysis, in: XI Interna- [91] W. Grabon, P. Pawlus, J. Sep, The study of the tribological properties of two-
tional Colloquium on Surfaces, Chemnitz, Germany, 2004, pp. 43–55. process textures, in: 36th Leeds-Lyon Symposium on Tribology, Lyon (France),
[57] J. Kumar, M.S. Shunmugam, A new approach for filtering of surface profiles 2009.
using morphological operations, Int. J. Mach. Tools Manuf. 46 (2006) 260–270. [92] G. Haasis, U.-P. Weigmann, New honing technique reduces oil consumption,
[58] X. Chen, J. Raja, S. Simanapalli, Multi-scale analysis of engineering surfaces, Ind. Diam. Rev. 3 (1999) 205–211.
in: Proceedings of 6th International Conference on Metrology and Properties [93] Z. Dimkovski, C. Anderberg, B.-G. Rosen, R. Ohlsson, T.R. Thomas, Quantifica-
of Engineering Surfaces, Birmingham, UK, 1994, pp. 231–239. tion of the cold worked material inside the deep honing grooves on cylinder
[59] S.-H. Lee, H. Zahouani, R. Caterini, T.G. Mathia, Morphological characterisation liner surfaces and its effect on wear, Wear 267 (12) (2009) 2235–2242.
of engineered surfaces by wavelet transform, in: Proceedings of 7th Inter- [94] J. Schmid, Honing technology for optimal cast-iron cylinder liners, Eng. Tech-
national Conference on Metrology and Properties of Engineering Surfaces, nol. Int. 1/2 (1999) 108–109.
Gothenburg, 1997, pp. 182–190. [95] J. Schmid, Optimized honing process for cast iron running surfaces, in: VDI
[60] X.Q. Jiang, L. Blunt, K.J. Stout, Recent development in the characterisation Symposium “Piston Running Surfaces, Pistons and Conrods”, Boblingen, Ger-
technique for bioengineering surfaces, in: Proceedings of 7th Int. Conference many, 2006.
on Metrology and Properties of Engineering Surfaces, Gothenburg, 1997, pp. [96] S. Brinkmann, H. Bodschwinna, Characterisation of automotive bore perfor-
182–190. mance using 3D surface metrology, in: L. Blunt, X. Jiang (Eds.), Advanced
[61] L. Blunt, X. Jiang (Eds.), Advanced Techniques for Assessment Surface Topog- Techniques for Assessment Surface Topography, Kogan Page Science, Lon-
raphy, Kogan Page Science, London/Sterling, 2003. don/Sterling, 2003, pp. 307–347.
[62] X. Jiang, L. Blunt, Third generation wavelet for the extraction of morphological [97] G. Duffet, P. Sallamand, A.B. Vannes, Improvement in friction by cw Nd: YAG
features from micro and nano scalar surfaces, Wear 257 (2004) 1235–1240. laser surface treatment on cast iron cylinder bore, Appl. Surf. Sci. 205 (2003)
[63] X. Jiang, W. Zeng, P. Scott, J. Ma, L. Blunt, Linear feature extraction based on 289–292.
complex ridgelet transform, Wear 264 (2008) 428–433. [98] U. Klink, Laserhonen fur Zylinderlaufbahnen, MTZ 58/9 (1997) 554–556.
[64] H. Zahouani, S. Mezghami, R. Vargiolu, M. Dursapt, Identification of manufac- [99] P. Pawlus, Surface Topography – Measurement, Analysis, Influence, Rzeszow
turing signature by 2D wavelet decomposition, Wear 264 (2008) 480–485. University of Technology, 2005 (in Polish).
[65] D.J. Whitehouse, The parameter rash – is there a cure? Wear 83 (1982) [100] G. Ryk, I. Etsion, Testing piston rings with partial laser surface texturing for
75–78. friction reduction, Wear 261 (7–8) (2006) 792–796.
508 T.G. Mathia et al. / Wear 271 (2011) 494–508
[101] I. Etsion, E. Sher, Improving fuel efficiency with laser textured piston rings, [131] D. Slop, J. Arends, Surface roughening of human enamel after toothbrushing,
Tribol. Int. 42 (2009) 52–547. J. Biol. Buccale 15 (1987) 159–162.
[102] L. Rapoport, A. Moskovith, V. Perfilyev, I. Lapsker, G. Halperin, Y. Itovich, I. [132] J.C. Keller, et al., Characterizations of titanium implant surfaces, III, J. Biomed.
Etsion, Friction and wear of MoS2 films on laser textured steel surfaces, in: Mater. Res. 28 (1994) 939–946.
Proceedings of NORDTRIB 2008 Symposium, Tampere (Finland), 2008. [133] M.M. Shalabi, et al., The effects of implant surface roughness and surgical
[103] W. Koszela, L. Galda, A. Dzierwa, P. Pawlus, The effect of surface texturing on technique on implant fixation in an in vitro model, Clin. Oral Implants Res. 17
seizure resistance of steel-bronze assembly, in: 36th Leeds-Lyon Symposium (2006) 172–178.
on Tribology, Lyon (France), 2009. [134] D.W. Murray, et al., The influence of the surface energy and roughness of
[104] L. Galda, A. Dzierwa, J. Sep, P. Pawlus, The effect of oil pockets shape and implants on bone resorption, J. Bone Joint Surg. Brit. 71 (1989) 632–637.
distribution on seizure resistance in lubricated sliding, Tribol. Lett. 37 (2) [135] L. Blunt, T.R. Thomas, Wear ranking of hard on hard bearings for prosthetic
(2010) 201–211. hip joints using a modified “plasticity index”, in: Proc. 9th Conf. Met&Props,
[105] E. Gualtieri, A. Borghi, L. Calabri, N. Pugno, S. Valeri, Increasing nanohardness 2003, pp. 158–164.
and reducing friction of nitride steel by laser surface texturing, Tribol. Int. 42 [136] P. Charlton, L. Blunt, Surface and form metrology of polished “freeform” bio-
(2009) 699–705. logical surfaces, in: Proc. 10th Conf. Met&Props, 2005, pp. 415–421.
[106] L. Galda, P. Pawlus, J. Sep, Dimples shape and distribution effect on charac- [137] I. Hilerio, et al., 3D measurements of the knee prosthesis surfaces applied in
teristics of Stribeck curve, Tribol. Int. 42 (2009) 1505–1512. optimising of manufacturing process, in: Proc. 9th Conf. Met& Props, 2003,
[107] L.M. Vilhena, M. Sedlacek, B. Podgornik, J. Vizintin, A. Babnik, J. Mozina, Surface pp. 151–157.
texturing by pulsed Nd:YAG laser, Tribol. Int. 42 (2009) 1496–1504. [138] M. Szubert, M. Wieczorowski, et al., Comparison of microtopography and pro-
[108] W. Koszela, P. Pawlus, L. Galda, The effect of oil pockets size and distribution filometry – two methods of skin surface analysis, Les Nouv. Derm. 24 (2005)
on wear in lubricated sliding, Wear 263 (2007) 1585–1592. 68.
[109] M. Mosleh, B.A. Khemet, A surface texturing approach for cleaner disc brake, [139] Y. Xie, et al., Morphological and spectral analysis of human skin surface topog-
Trib. Lub. Tech. December (2006) 32–37. raphy, Innov. Technol. Biol. Med. 14 (1993) 575–587.
[110] P. Stepien, Fundamentals of Regular Surface Topography Formation in Grind- [140] P. Nardin, et al., Automation of a series of cutaneous topography measure-
ing, Koszalin University of Technology Press, Koszalin, 2006 (in Polish). ments from silicon rubber replicas, Skin Res. Technol. 8 (2002) 112–117.
[111] F.-P. Ninove, C. Rapiejko, T.G. Mathia, 3D Morphological behaviour of hetero- [141] E. Piche, et al., Neue Ansätze zur 3-D-Rauhigkeitsanalyse menschlicher Haut,
geneous model material in finishing abrasive process–case of nodular cast Zeitschrift für Hautkrankheiten 77 (2002) 140–146.
iron, in: J. Sladek, W. Jakubiec (Eds.), Advances in Coordinate Metrology, Uni- [142] M. Rohr, K. Schrader, Fast optical in vivo topometry of human skin (FOITS):
versity of Bielsko-Biala, 2010, pp. 456–462 (ISBN 978-83-62292-56-1). Vergleichende Untersuchungen zur Laserprofilometrie, SÖFW J. 124 (1998)
[112] T. Sata, Surface finish in metal cutting, Ann. CIRP 12 (1963) 190–197. 52–59.
[113] S. Shimada, Surface roughness of machined surfaces, Jpn. J. Trib. 43 (1998) [143] C. Guinot, et al., Reference ranges of skin micro-relief according to age in
1395–1408. French Caucasian and Japanese women, Skin Res. Technol. 12 (2006) 268–278.
[114] X.D. Liu, et al., Direct single point diamond cutting of stavax assisted with [144] J.C. Wambold, et al., Evaluation of pavement surface texture significance and
ultrasonic vibration to produce optical quality surface finish, in: Proc. XVIII measurement techniques, Wear 83 (1982) 351–368.
ASPE AM, 2003, pp. 67–70. [145] S. Yildirim, I. Uzmay, Statistical analysis of vehicles’ vibration due to road
[115] T.A. Dow, et al., Elliptical vibration assisted diamond turning, in: Proc. XVII roughness using radial basis artificial neural network, Appl. Artif. Intell. 15
ASPE AM, 2002, pp. 115–119. (2001) 419–427.
[116] K. Ohashi, et al., Development of cavitation aided machining for finishing fine [146] J. Hansson, P. Svensson, Stress distribution in unbound aggregate of road
surface, in: Proc XVIII ASPE AM, 2003, pp. 587–590. structure: influence of surface roughness and particle shape, Bull. Eng. Geol.
[117] M. Pfestorf, et al., 3D-surface parameters and their application on determin- Environ. 60 (2001) 223–226.
istic textured metal sheets, Int. J. Mach. Tools Manuf. 38 (1998) 607–614. [147] J.C. Wambold, The measurement and data analysis used to evaluate highway
[118] J. Scheers, et al., Assessment of steel surface roughness and waviness in rela- roughness, Wear 57 (1979) 117–125.
tion with paint appearance, Int. J. Mach. Tools Manuf. 38 (1998) 647–656. [148] A.B. Slimane, et al., Characterization of road microtexture by means of image
[119] T.H. Lee, N.J. Mills, Surface roughness and impact strength of injection- analysis, in: Proc. 10th Conf. Met&Props, 2005, pp. 397–404.
moulded polystyrene, J. Mater. Sci. 29 (1994) 2704–2712. [149] T. Vernersson, Thermally induced roughness of tread-braked railway wheels,
[120] Y.Z. Dai, F.P. Chiang, Strain path and surface roughness, Mech. Mater. 13 (1992) 1: brake rig experiments, Wear 236 (1999) 96–105.
55–57. [150] T. Vernersson, Thermally induced roughness of tread braked railway wheels,
[121] K. Hasche, et al., Determination of the geometry of microhardness indenters 2: modelling and field measurements, Wear 236 (1999) 106–116.
with a scanning force microscope, Meas. Sci. Technol. 9 (1998) 1082–1108. [151] R.B. Ramgulam, et al., Measurement of fabric roughness by a non-contact
[122] J.G.F. Song, et al., Microform calibrations in surface metrology, Int. J. Mach. method, J. Textil. Inst. 84 (1993) 99–106.
Tools Manuf. 35 (1995) 301–310. [152] T.G. Mathia, et al., Topography, wear and sliding functions of ski, Int. J. Mach.
[123] P.J. Sullivan, et al., The topographical characteristics of microindentations and Tools Manuf. 32 (1992) 263–266.
their relevance to microhardness testing, Surface Topogr. 1 (1988) 357–369. [153] J. Stor-Pellinen, M. Luukkala, Paper roughness measurement using airborne
[124] http://www.altimet.fr (accessed 15.05.2010). ultrasound, Sens. Actuators A 49 (1995) 37–40.
[125] H. Jackowiak, Scanning electron microscopy study of the lingual papillae in [154] J.S. Preston, et al., Investigation into the distribution of ink components on
the European mole, J. Vet. Med. C 35 (2006) 190–195. printed coated paper, 1: optical and roughness considerations, Colloid Surf.
[126] H. Jackowiak, S. Godynicki, The distribution and structure of the lingual papil- A 205 (2002) 183–198.
lae on the tongue of the bank vole, Folia Morphol. 64 (2005) 326–333. [155] M. Zecchino, Characterizing surface quality: why average roughness is not
[127] H. Jackowiak, S. Godynicki, Light and scanning electron microscopic study of enough, Adv. Mater. Proc. 161 (2003) 25–28.
the tongue in the white tailed eagle, Ann. Anat. 187 (2005) 251–259. [156] N. Senin, et al., Three-dimensional surface topography acquisition and anal-
[128] V. Briones, et al., Effect of surface topography on color and gloss of chocolate ysis for firearm identification, J. Forensic Sci. 51 (2006) 282–295.
samples, J. Food Eng. 77 (2006) 776–783. [157] E.P. Whitenton, et al., Manufacturing and quality control of the NIST reference
[129] K.J. Stout, L.S. Blunt, Application of 3-D topography to bio-engineering, Int. J. material 8240 standard bullet, in: Proc. XVIII ASPE AM, 2003, pp. 99–102.
Mach. Tools Manuf. 35 (1995) 219–229. [158] J. Song, et al., SRM 2460/2461 standard bullets and casings project, J. Res. Nat.
[130] M. Quirynen, et al., The influence of surface free energy and surface roughness Inst. Stand. Technol. 109 (2004) 533–542.
on early plaque formation. An in vivo study in man, J. Clin. Periodont 17 (1990)
138–144.