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INTRODUCTION
Clay roof tiles have been around for centuries proving their long lasting and
durability attributes. But there are many other benefits that have stamped clay roof
tiles as the best roofing material for housing construction. Clay roof tiles are a natural
thermal insulator, keeping the heat outside. The best way to illustrate this is to think
of clay tiles as energy savers.
On the other hand, it is already evident that the global warming has a huge
impact in our environment. Due to the effect of climate change dangerously hot
weather is already occurring more frequently than it did few decades ago and
scientists expect heat waves to become more frequent and severe as global warming
intensifies. The increase in heat waves creates serious health risk, and can lead to
heat exhaustion, heat stroke, and aggravate existing medical conditions. Scientists
say human activities such as abusive use of energy are largely responsible for the
continued increase in average global temperatures, which causes climate change
(Ranada, 2016).
The use of rice husk in the production of clay roof tiles helps enhance the
structural and thermal properties. This also provides a solution for environmental
damage caused by dumping of waste rice husk. Unlike the previous studies, instead
of using Rice Husk Ash (which is combusted) we are introducing the use of
pulverized rice husk to be more environmental friendly. Since this study addresses
environmental issues, we are trying to avoid burning in the process.
Research Objectives
The purpose of this study was to create a clay roof tile with pulverized rice husk as an
additive.
1. To investigate the thermal effect of pulverized rice husk on clay roof tiles.
2. To examine the water tightness, thermal properties and compressive strength of
clay roof tiles with pulverized rice husk.
The findings of this study will redound to the benefit of society considering that clay
roof tiles are commonly used as a replacement for galvanized iron sheets. The thermal
properties of the roof have high demands from the society especially on places where
too much heat occurs. Thus, people that would want to improve the properties of their
roof and reduce the heat transfer from their roof may already have a solution when the
result of this study will be finished. This research will contribute to the existing
knowledge by not only focusing on the properties of clay roof tiles with rice husk but
also on how it will help to reduce the use of electricity and how it will help to convert
agricultural waste into an economic and environmental material. Thus, a new effective
additive for clay roof tiles will be arrived at.
Today, more than 70 countries produce rice worldwide. The benefits of rice produce
high volumes of rice husk, which is low-density residue of the process. When
disposed of, this residue occupies large areas, where it can self-burn, spreading the
ashes and causing huge damages to the environment. The rice-producing countries
are challenged by the problem of disposing of the rice husk, and have been trying to
use it in an economical manner. Such attempts, however, have been somewhat
frustrating, because of the intrinsic properties of the rice husk, such as hardness,
fibrousness and abrasive nature (Goncalves, Bergmann, 2007).
Asbestos sheet roof covering becomes more popular among people mostly
because of easiness in handling, cost effectiveness, and high strength. It has been
found out that the use of asbestos as roofing material cause cancer of the lungs,
larynx and ovary, mesothelioma, and asbestosis. In addition, several thousands of
deaths and other diseases are related to asbestos. Clay roof tiles can be a better
alternative than the usual roofing material such as asbestos, considering several
advantages such as health favourability, better appearance, and thermal absorption
(WHO Publication, 2014).
Rice husk helps to solve the disposal and pollution problems of the rice milling
industry. In addition, small scale of pure silica powder can be widely used for thermal
insulator (Genieva, Turmanova, Dimitrova,and Vlaev, 2008). The use of rice husk in
clay brick production provides an economical contribution and also serves as the
energy efficiency materials for building. It is indicated that rice husk could be an
alternative raw material for production of clay bricks and friendly environments
(Gorhan, 2013).
Physical Properties
Bulk Density and True Density
The bulk density of ungrounded rice husks increased with the increase of
moisture, whereas the bulk density of grounded rice husks decreased. The bulk
density of ground husk was found to be 2.38 to 2.84 times more than that of
ungrounded rice husks. At the same time, the true density of ungrounded husks
increased and that of grounded husks decreased. Thus, ground rice husks swell
when moist. Density (bulk and true) of ungrounded husk increased with moisture
content whereas the density of grounded husk decreased. The same tendency was
observed by other authors, where it is pointed out that the relationship between the
moisture content and true density is linear within the limits of the moisture content in
both the ungrounded and grounded conditions of rice husks (Genieva, 2008).
Chemical Composition
Rice husk is an organic waste and it is a major byproduct of the rice milling
process and agro-based biomass produced in large quantities. Rice husk normally
consists of 20 % of silica, 60 - 65 % of volatile substances, 10 - 15 % of fixed carbon,
and approximately 10 - 15 % of ash (Janbuala, 2015). Moreover, Rice Husk has 40%
cellulose, 30% lignin group and 20% silica. It can absorb the water range from 5% to
16% and the unit weight of rice husk is 83–125 kg/m3 (Gorhan, 2013). According to
Chandarasekhar (2003), the silica present in Rice Husk is in hydrated amorphous
form, either opal or silica gel. However, RH (Rice Husk) on burning gives ash
containing more than 90% silica, which is normally in the crystalline form.
Because of these properties of rice husks, they provide important benefits in
brick production. These wastes reduce the unit weight and improve thermal
properties of the clay brick. While the use of rice husks increases pore volume in clay
structure, also provides environmental benefit by reducing the use of rich soils which
takes a long time to form in brick production (Gorhan, 2013).
A large quantity of husk is available as waste from rice milling industries. This
can be used as an industrial raw material, for example, as an insulating material,
fillers in plastics, building material, for making panel boards, and activated carbon.
The specific heat of ground husk increased linearly from 0.39 to 0.66kcalkg as its
moisture content increased from 10 to 21%. This behaviour is expected because of
the higher specific heat of water contained in it. The high specific heat of ground husk
offers it as a good insulating material for making insulation board and others. The
thermal conductivity of ground husk increased linearly from 0.056 to 0.085kcal has its
Compressive Strength
The result shows there was an increase in the compressive strength with the
addition of Rice Husk. The compressive strength of the rice husk/clay mix has been
found to increase with the rice husk content. Firing at 700 C yielded optimum
performance (Ibanga and Ahmed, 2007).
The 5% and 10% addition of rice husk to brick clay exhibit a compressive
strength of 7–10 MPa which means it passed because according to Disaster
Regulation, the minimum strength for building bricks is 5 MPa and the necessary
compressive strength for horizontal perforated brick in TS EN 771-1 is between 2.5
and 7.5 MPa (Gorhan and Simsek, 2012).
Thermal Conductivity
An increase of rice husk leads to an increase in the apparent porosity and this
effect decreased the unit weight and improved the thermal insulating properties
(Ibanga and Ahmed, 2007).It was mentioned that thermal conductivity coefficients
were related to unit weight and porosity in bricks. For this reason, it is thought that
when porosity in the structure increases, thermal conductivity coefficient will decrease.
Also, a decrease in unit weight is expected with increased porosity. Brick samples with
unground rice husk have lower unit weight and thermal conductivity coefficients
(Gorhan and Simsek, 2012).
Factors that affect the Performance of Clay Bricks with Rice Husk
Firing Temparature
The effect of weight percent rice husks (as an additive) in clay bricks fired at
500 C, 600C, 700 C and 800 C. The result shows there was an increase in the
compressive strength with the additive. It must also be pointed out that 700 C seems
to be the critical temperature for the firing.
At the temperature of 800 C, we observed a decrease in all the values of the
compressive strength. This may be due to the reactions of alumina, which when
completed made the brick brittle, shrink and warp.
Water absorption of all the bricks decrease with increasing temperature.
However, the density of the burnt bricks increased with increasing temperature and
peaked at 700 C. Observations suggested that firing at 700 C yields the optimum
performance (Ibanga and Ahmed, 20 07).
The addition of Rice Husk by 10 percent, resulting in the best piece of brick
and the properties of Thailand industry standard lightweight brick of C12 and when
adding Rice Husk Ash to 10 percent by weight, it resulted in the best piece of brick
and the properties of Thailand industry standard lightweight brick of C12. The
comparison between the sample with the addition of Rice Husk and Rice Husk Ash
found that the ones with addition of Rice Husk have a density slightly greater than the
ones with addition of Rice Husk Ash. However, the strength of the sample with
addition of Rice Husk was less than the ones with addition of Rice Husk Ash.
Because the amount of Rice Husk ash with a more resolution causes a more porosity
which also affects the density of the piece. However, the resolution makes the particle
distribution of the porosity is uniform and the strength of the piece that is filled with
Clay Roof Tiles with Pulverized Rice Husk| 6
Rice Husk Ash is greater .The addition of Rice Husk Ash caused the microstructure of
porous sample more evenly distributed than the addition of Rice Husk which also has
a larger pore. Finally, work pieces with the addition of Rice Husk production of rice
had a little more porosity and water absorption than the addition of Rice Husk Ash
(Janbuala, 2015).
Color Component
Rice husk mainly consists of silica, fixed carbon, cellulose, and lignin groups
all of which contribute to its significant water absorption and thermal dispersion.
Likewise, its high specific heat is also a relevant factor on its thermal insulation.
These properties found the theory of this study that Pulverized Rice Husk is a vital
additive to Clay Roof Tiles.
Preparation
and Moulding
Materials Purification of
proportionin
Preparation process g of roof tile Roof tile
specimen
Drying
Comparing Recording Testing of
of of of moulded
results test roof tile roof tile
results
Collection of materials
The samples of rice husk that were used in the study were obtained from a
rice mills around Tuguegarao City. The clay that was used is normal clay, collected
from Iguig, Cagayan where the clay is used for production of pots.
Purification Process
Before use, the rice husks were thoroughly washed – three times with tap
water to remove adhering soil, clay and dust, boiled for an hour to desorb any
impurities and finally, dried at 375±2 K overnight.
The lumps of the clay were crushed to make fine particles and then naturally
dried for several days to remove the inherent moisture
so that it cannot vary the moisture amount used for
making the specimen. The clay particles were
screened to avoid any unwanted foreign particles
like stones, large aggregates or other substances and
to get homogeneous fine clay.
The samples were pulverized and screened through an ASTM standard sieve
to obtain the desired grain sizes (325 mesh size). Clay, water and uniformly sized
GRH were first proportioned according to volume percentage. 5%, 10%, 15% and
20% of the total brick volume were taken and mixed with 95%, 90%, 85% and 80%
clay respectively. The mixture was ground, well mixed and became almost a
homogeneous material.
The moulded roof tile was placed in the sun for drying. The roof tile was
removed afterwards. After sun-drying, the tiles were subsequently weighed and the
weights of the samples were recorded again. Then, the tiles were fired in furnace at
temperatures of 500°C, to 800°C. In the furnace, the temperature was gradually
increased to the firing temperature and subsequently maintained for 2 hours. The
temperature of the furnace was gradually reduced to room temperature before
removal of the fired roof tiles.
The following tests are based from the previous study conducted by Subashi De
Silva, G.H.M.J and Surangi, M.L.C. (2017) entitled Effect of waste rice husk ash on
structural, thermal and run-off properties of clay roof tiles
Water tightness
The tile was blocked on either side by two lumps of wet mortar or clay. The pool
between the two weirs was filled with water. The tile is allowed to stand on supports
for one day. This exposure is equivalent to a continuous 24 hour rainfall. The under-
side of the tile was carefully examined. No free water (drips) should seep through the
Clay Roof Tiles with Pulverized Rice Husk| 10
tile. Signs of dampness are acceptable but the less the better. British Standards 473
and 550 specify that less than 25 percent of the under-side of the tile may show
dampness stains.
Water loss from each samples were measured by subtracting the weight of
sample before and after 24 hours. Dampness on the under-side of the tile was
measured.
Thermal properties
Compressive Strength
It was found out that all of the specimens showed signs of dampness. As
seen on the table above, the specimen with 0% Pulverized Rise Husk had the
least amount of water loss while the specimen with 20% Pulverized Rise Husk
had the highest amount of water loss. This is because of the voids present in
the specimens. These voids were obtained during the firing process of the tiles
where the PRH was burned causing these voids to appear. Meaning, the higher
the amount of PRH added on the roof tiles, the greater the chance of having
many voids. Therefore, clay roof tiles having no PRH mixed obtained the least
amount of water loss.
TIME OUTSIDE
Clay Roof Tiles with Pulverized Rice Husk| 14
(30 mins TEMPERATUR 0% 5% 10% 15% 20%
interval) E
( ֯C )
8:00 AM 33.3 33.5 33.1 32.9 32.2 32
8:30 AM 33.6 33.8 33.4 33.1 32.3 32.3
9:00 AM 34 34.1 33.6 33.3 33.1 32.4
9:30 AM 34.6 34.9 34.2 33.5 33.2 32.7
10:00 35.1 35.5 34.4 33.6 33.5 32.8
AM
10:30 35.8 35.9 34.6 33.8 33.7 33.2
AM
11:00 36.2 36.3 34.8 33.9 33.9 33.6
AM
11:30 37.4 37.5 34.9 34.3 34.0 33.8
AM
12:00 37.7 37.9 35.5 34.5 34.3 34.1
NOON
12:30 37.9 38.1 35.7 34.7 34.5 34.3
PM
1:00 PM 38.3 38.5 35.8 34.8 34.6 34.6
1:30 PM 38.8 38.8 36.0 34.9 34.8 34.9
2:00 PM 39.5 39.8 36.3 35.5 35.3 35.0
2:30 PM 39.8 40.2 36.8 35.7 35.4 35.3
3:00 PM 37.6 37.8 36.1 35.8 35.6 35.4
3:30 PM 37.3 37.5 35.7 35.1 34.9 34.6
4:00 PM 36.6 36.9 35.4 34.7 34.8 34.5
4:30 PM 36.2 36.8 35.2 34.4 34.2 34.1
5:00 PM 36.1 36.5 34.6 34.1 33.7 33.5
5:30 PM 35.9 36.3 34.5 33.7 33.2 33.1
6:00 PM 35.8 35.9 33.0 32.6 32.4 32.3
Compressive Strength
Thus, effective utilization of PRH in the production of clay roof tiles helps to
enhance the structural and thermal properties, while providing a solution for
environmental problems caused by open dumping and piling of Rice Husk as a
waste.
This study concludes that optimum usage of Pulverized Rise Husk is 10% while
enhancing the compressive, thermal, and water tightness performance of roof tiles.
The specimen with 10% Pulverized Rise Husk obtained a compressive strength of
4.9 MPa which is less than the strength of the 0% and 5% sample but according to
Gorhan and Simsek (2012), the standard strength for building bricks is between 4.5-5
MPa. This made the 10% PRH sample pass the minimum strength for building bricks.
Moreover, the dampness stain of the 10% sample is 14.4% making it acceptable to
use because as specified from the British Standards 473 and 550, less than 25% of
the under-side of the tile may show dampness stains but the less the better. Lastly,
the higher Pulverized Rise husk content of a brick, the higher cooling ability it could
give, thus reducing the temperature. Although the 20% specimen has the highest
percentage of cooling ability of the bricks, the 10% sample would be considered as
the model specimen since any of the specimens presented in this study would be
acceptable as long as there is PRH present.
Recommendation
In light of the results of the different test that has been conducted, the following are
recommended to further improve the product:
Appendix A
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Definition of Terms
Silica – a mineral that exists in various forms, including sand, quartz, and is used to
make glass and cement.
Thermal Conductivity - the degree to which a specified material conducts electricity,
calculated as the ratio of the current density in the material to the electric field that
causes the flow of current. It is the reciprocal of the resistivity.
Moisture Content – the quantity of water contained in a mineral, such as soil, rock,
ceramics, crops, or wood. It is used in a wide range of scientific and technical areas,
and is expressed as a ratio, which can range from 0 (completely dry) to the value of
the materials’ porosity at saturation.
Report
Roof tile (0%) No.
Basic information:
No.
specimen compressive
No. diameter
area(A)
1 152.400 18241.454
specimen destroy tensile
No.
load(F) strength(fcc)
1 208.913 11.5
200
100
0
0 20 40 60 80 100
Time(s)
Report
No.
Roof Tile (5%)
Basic information:
No.
No. diameter specimen compressive area(A)
1 152.400 18241.454
specimen destroy tensile
No.
load(F) strength(fcc)
1 128.845 7.1
1 : Load-Time Curve
150
Load(kN)
100
50
0
0 10 20 30 40
Time(s)
1 : Load-Time Curve
100
80
Load(kN)
60
40
20
0
0 10 20 30 40
Time(s)
Report
No.
Roof Tile (15%)
Basic information:
No.
No. diameter specimen compressive area(A)
1 152.400 18241.454
No. specimen destroy tensile
1 : Load-Time Curve
100
80
Load(kN)
60
40
20
0
0 10 20 30 40 50
Time(s)
Report
No.
Roof Tile (20%)
Basic information:
No.
1 152.400 18241.454
specimen destroy tensile
No.
load(F) strength(fcc)
1 75.149 4.1
Load(kN) 60
40
20
0
0 5 10 15 20 25 30 35
Time(s)