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Vapour Stream
H2 3676.707 0.630744121 2.015 0.0899
CH4 130.107 0.0223201156 16.04 0.717
N2 283.114 0.0485685139 14.01 1.25
CO2 1727.985 0.296438279 44.01 0.00197
CO 11.244 0.0019289706 28.01 1.25
Total 5829.157
Liquid Stream
CH3OH 125815.502 0.6910189732 32.04 0.791
H2O 56256.926 0.3089810268 18.01 1
Total 182072.428
Uperm
Ac
Diameter
Height
Molar Flow Rate
1824.6683052513
8.111437807
20.208
39.2634703164
0.4014377965
1892.6526099664
3926.8259031824
3123.6493964072
7050.4752995896
181.3070750607 ft/s
141.0389383737 ft^2
13.4040082594 ft
40.2120247783 ft
FEED Tbubble 337.9061129492 K
Componnet Mass Flow Rate Molar Flow Rate Fraction
Methanol 126987.691944409 3963.4111093761 0.9905158656
Water 683.4694366236 37.949441234 0.0094841344
Total 127671.161381032 4001.36055061 1
LK Methanol
HK Water
di dj bj bi
0.9989372479 0.0010627521 0.0793376203 0.9206623797
Nmin 2.9205646118
DISTRIBUSI NONKEY
Feed Distilat
Component
Kmol/jam Xi Kmol/jam
Methanol 3963.4111093761 0.994646642 3567.0699984385
Water 37.949441234 0.005353358 3.7949441234
Total 4001.36055061 3570.8649425619
PERHITUNGAN R MIN
KOMPONEN alfa avg xi,f alfa avg x Xi,f
Methanol 4.5026107706 0.9905158656 4.4599074049
Water 1 0.0094841344 0.0094841344
Total
Rm
R/Rm
R
JUMLAH STAGE
R/(R+1) 0.2029283854
Rm/(Rm+1) 0.1627212369
Nm/N 0.31
N 9.4211761671
Komponen A B C
Methanol -9.0562 1.25E+03 0.0224
Water -10.2158 1.79E+03 1.77E-02
P 395.1864995074 mmHg
Pi K xi
395.6917370441 1.0012784787 1.000214368
87.4978159925 0.2214089198 0.0002353028
1.0004496707
P 395.1864995074 mmHg
Pi K yi
421.3178458182 1.0661240866 0.9815403386
93.9811622701 0.2378147087 0.0188676531
1.0004079916
α(bot) α(avg)
4.4830031428 4.5026107706
1 1
αm (di/dj)*(bj/bi)
4.5026107706 81
Distilat Bottom
xi,d Kmol/jam xi,b
0.9989372479 396.3411109376 0.9206623797
0.0010627521 34.1544971106 0.0793376203
3570.8649425619 430.4956080482
(alfai.xi,f)/(alfai-teta) q
0.4905158656 θ
-0.4905158656 1-q
0
(alfai.xi,d)/(alfai-teta)
1.0356701124
0.1586752407
1.1943453531
0.1943453531
1.31
0.2545924126
Tavg 322.7184139967
D
-2.35E-05
-1.26E-05
0.4246818781
B C
3.89E-01 -6.28E-05
4.29E-01 -1.62E-05
Component A
Methanol 45.617
Water 29.8605
Molecular Weight
Methanol 32.04
Water 18.01
7,2 psia
Density
Methanol 792
Water 997
dr/br 0.11111111
1
0.5
0
molar average viscosity (cp)
4.01E-01
5.17E-03
4.06E-01
B C D E
-3244.7 -13.988 6.6365E-03 -1.0507E-13
-3.1522E+03 -7.3037E+00 2.4247E-09 1.8090E-06
+B/T+C*log10(T)+D*T+E*T^2
MECHANICAL DESIGN
1. Menghitung Tinggi Kolom
Column Height= 54 ft
DISTILAT PRODUCT
LIQUID
Mass Flow Rate
Komponen Molar Flow Rate Fraction
Kg/h Kg/S
Methanol 29097.0925718331 8.0825257144 908.1489566739 0.9989372
Water 17.4006132781 0.0048335037 0.9661639799 0.0010628
Total 8.0873592181 909.1151206538
VAPOR
Mass Flow Rate
Komponen Molar Flow Rate Fraction
Kg/h Kg/S
Methanol 143386.015321801 39.8294487005 1.2431163764 0.9989372
Water 85.7475569405 0.0238187658 0.00132253 0.0010628
Total 39.8532674663 1.2444389064
BOTTOM PRODUCT
LIQUID
Mass Flow Rate
Komponen Molar Flow Rate Fraction
Kg/h Kg/S
Methanol 15931.7794802001 4.4254943001 497.246550568 0.9206624
Water 771.7280124643 0.2143688924 42.8499729297 0.0793376
Total 4.6398631924 540.0965234978
VAPOR
Mass Flow Rate
Komponen Molar Flow Rate Fraction
Kg/h Kg/S
Methanol 3233.0102857592 0.8980584127 100.9054396304 0.9206624
Water 156.6055195031 0.0435015332 8.6954758192 0.0793376
Total 0.9415599459 109.6009154496
Flooding Velocity
Flv Top 0.0055547772
Flv Bot 0.1316368384
Capacity Parameter
C top
C bot 0.35 ft/s
Superficial Velocity
Uf top
Uf bot 13.0976323331 ft/s 3.9921583342 m/s
Diameter
DT top
DT bot 2.4463477484 m
Drum Volume
Vv 3.4816555575
H 26.5431542719 H>4DT
Dt 1.0346716067 m
f 12650
c 0.125
E 0.8
t 0.0173977748
ts 0.1875 inch
4. Menghitung Tebal Head
OD 41.1100211561
icr 1.25
rc 42
w 0.7931290975
th 0.1392211097
thead standar 0.1875
sf 1,5-2,5
sf yang dipakai 2
a 20.3675105781
b 6.0127343454
AB 19.1175105781
BC 40.75
AC 35.9872656546
OA 8.2002343454 inch
T
32.0059494236 0.0404115523
0.0191401649 1.919775812568E-05
32.0250895884 0.0404307501 792.0973402771
29.4980226442 0.0372449781
1.4288705424 0.0014331701
30.9268931866 0.0386781481 799.5960167409
29.4980226442
1.4288705424
30.9268931866 0.5705728568
Ad/A 0.1035152043
FEED
T 181.1012493822 K
IN %mass kg/jam kmol/jam
Methane 0.0082052143 694.2587905847 43.2748731898
Ethylene 0.0451286802 3818.4234833905 136.1097698507
Propylene 0.4471841968 37837.1056414592 899.1493938228
Butene 0.2502590459 21174.8939850015 377.4019994832
Pentene 0.1476938632 12496.6587452547 178.1826039475
Hexene 0.0519663593 4396.9725214785 52.2447751509
Heptene 0.0341883943 2892.7450799201 29.4612893624
H2O 0.0153742461 1300.844212006 72.1889129859
total 1 84611.9024590952 1788.0136177933
di dj bj bi
0.2575004449 0.0017230268 0.6421599529 0.0099999467
NMIN 6.5092577122
DISTRIBUSI NONKEY
Feed Distilat
Component
Kmol/jam Xi Kmol/jam
Methane 43.2748731898 0.0242027649 42.9601955585
Ethylene 136.1097698507 0.0761234526 135.1200338487
Propylene 899.1493938228 0.5028761442 892.611137773
Butene 377.4019994832 0.2110733362 374.6576825506
Pentene 178.1826039475 0.0996539412 176.8869310635
Hexene 52.2447751509 0.0292194504 51.8648719674
Heptene 29.4612893624 0.0164771057 29.2470586075
H2O 72.1889129859 0.0403738049 71.6639839804
Total 1788.013617793 1775.0118953497
PERHITUNGAN R MIN
KOMPONEN alfa avg xi,f alfa avg x Xi,f
Methane 1226.2588049977 0.0242027649 29.6788535368
Ethylene 134.2668161723 0.0761234526 10.2208536143
Propylene 18.900515803 0.5028761442 9.5046185097
Butene 4.0903860683 0.2110733362 0.8633714338
Pentene 1 0.0996539412 0.0996539412
Hexene 0.2441506221 0.0292194504 0.007133947
Heptene 0.0613857379 0.0164771057 0.0010114593
H2O 0.0196555734 0.0403738049 0.0007935703
Total
θ 2.0817410359
q 0
1-q 1
KOMPONEN alfa avg xi,d alfa avg x xi,d
Methane 1226.2588049977 0.0290287824 35.5968000611
Ethylene 134.2668161723 0.093377511 12.5375011059
Propylene 18.900515803 0.6183665932 11.6874475675
Butene 4.0903860683 0.2575004449 1.0532762324
Pentene 1 0.0017230268 0.0017230268
Hexene 0.2441506221 3.6252787620268E-06 8.85114065191E-07
Heptene 0.0613857379 1.63754631782119E-08 0.000000001
H2O 0.0196555734 0 0
Total
Rm
R/Rm
R
PERHITUNGAN STAGE
R/(R+1) 0.307523354
Rm/(Rm+1) 0.2546264855
Nm/N 0.33 From Graph
N 19.7250233702
PERHITUNGAN N AKTUAL
Component A B C
Methane 3.844 4.01E-01 -1.43E-04
Ethylene -3.985 3.87E-01 -1.12E-04
Propylene -7.23 3.42E-01 -9.45E-05
Butene -9.143 3.16E-01 -8.42E-05
Pentene -2.903 2.71E-01 -6.83E-05
Hexene -2.118 2.48E-01 -6.06E-05
Heptene -0.16 2.26E-01 -5.10E-05
H2O -36.826 4.29E-01 -1.62E-05
Total
µgas * xi 7.82E-03
αavg 4.0903860683
αavgµ 3.20E-02
Log(αavgµ) -1.4950862053
Eo 99.5903016722 0.9959030167
Naktual 18.8020550754
Nr + Ns 18.8020550754
Ns 11.5301657423 dari bawah
Nr 7.2718893332 dari atas
P 760 mmHg
fraksi Pi K yi
0.0242027649 25608.8796712246 33.6958943042 0.8155338072
0.0761234526 1446.7218674797 1.9035814046 0.1449071888
0.5028761442 58.2882170584 0.0766950224 0.0385680972
0.2110733362 3.4596611219 0.0045521857 0.000960845
0.0996539412 0.2856438059 0.0003758471 3.745465E-05
0.0292194504 0.0232746125 3.062449E-05 8.948308E-07
0.0164771057 0.0016415196 2.1598942E-06 3.55888E-08
0.0403738049 0.0001054187 1.3870877E-07 5.600201E-09
1 1.0000083288
P 760 mmHg
fraksi Pi K xi
0.0290287824 139258.200372487 183.234474174 0.0001584242
0.093377511 15046.4079180043 19.7979051553 0.0047165349
0.6183665932 1684.846402894 2.2169031617 0.2789326137
0.2575004449 282.6603041775 0.3719214529 0.6923516858
0.0017230268 55.6370498182 0.0732066445 0.0235364806
3.6252787620268E-06 10.5384537287 0.0138663865 0.0002614437
1.63754631782119E-08 2.0313089511 0.0026727749 6.126765E-06
0 0.4278609159 0.0005629749 0
0.9999633098
P 760 mmHg
fraksi Pi K yi
0 607721.345480474 799.633349316 0
0 67431.9224617297 88.7262137654 0
2.22365063134909E-07 11932.9546292131 15.7012560911 3.491411E-06
0.0099999467 3331.3845761293 4.3834007581 0.043833774
0.6421599529 1011.5722297701 1.3310160918 0.8547252309
0.1906748166 318.3462725546 0.4188766744 0.0798692331
0.1571650614 104.4046809292 0.1373745802 0.0215904843
0 50.8194326717 0.0668676746 0
1.0000222136
αm (di/dj)*(bj/bi)
4.0903860683 9596.9115301875
Distilat Bottom
xi,d Kmol/jam xi,b dr/br 0.0142255
0.0242027649 0.3146776313 0.0242027649
0.0761234526 0.9897360019 0.0761234526
0.5028761442 6.5382560499 0.5028761442
0.2110733362 2.7443169326 0.2110733362
0.0996539412 1.295672884 0.0996539412
0.0292194504 0.3799031836 0.0292194504
0.0164771057 0.2142307549 0.0164771057
0.0403738049 0.5249290055 0.0403738049
13.0017224436
(alfai.xi,f)/(alfai-teta)
0.0242439222
0.0773222968
0.5651195549
0.4298277794
-0.092123658
-0.0038822291
-0.0005006344
-0.0003848387
1.0000070318
(alfai.xi,d)/(alfai-teta)
0.0290781465
0.094848084
0.694904815
0.5243715118
-0.0015928274
-4.81671028852342E-07
-4.97546095609927E-10
0
1.3416092477
0.3416092477
1.3
0.444092022
Tavg 277.9988769845 K
µgas (micropoise) µgas (poise) Feed Fraction µgas * xi
1.04E+02 1.04E-02 0.0242027649 2.52E-04
9.50E+01 9.50E-03 0.0761234526 7.23E-04
8.05E+01 8.05E-03 0.5028761442 4.05E-03
7.21E+01 7.21E-03 0.2110733362 1.52E-03
6.70E+01 6.70E-03 0.0996539412 6.68E-04
6.21E+01 6.21E-03 0.0292194504 1.81E-04
5.88E+01 5.88E-03 0.0164771057 9.69E-05
8.12E+01 8.12E-03 0.0403738049 3.28E-04
7.82E-03
KONST
Molecular Weight Density
A
16.043 0.656 14.667
28.054 1.18 18.796
42.081 1.74 24.539
56.107 620 27.312
70.134 640 36.274
84.161 673 33.449
98.188 697 38.126
18.02 997 29.8605
(Yaws,1977) (PubChem)
log10(P)=A+B/T+C*log10(T)+D*T+E*T^2
MECHANICAL DESIGN
Column Height= 52 ft
DISTILAT PRODUCT
LIQUID
VAPOR
BOTTOM PRODUCT
LIQUID
Mass Flow Rate
Komponen
Kg/h Kg/S
Methane 0.000 3.6089987402251E-19
Ethylene 0.000 1.39028293988504E-13
Propylene 0.004 0.000001029
Butene 222.124 0.0617012419
Pentene 17830.089 4.952802372
Hexene 6353.103 1.7647508356
Heptene 6109.365 1.6970459141
H2O 0.000 0
TOTAL 8.4763013926
VAPOR
Mass Flow Rate
Komponen
Kg/h Kg/S
Methane 3.995465E-16 1.10985139700826E-19
Ethylene 1.5391601E-10 4.27544472617889E-14
Propylene 0.0011392325 3.16453483167651E-07
Butene 68.308462227 0.0189745728
Pentene 5483.16862889 1.5231023969
Hexene 1953.72754507 0.5427020959
Heptene 1878.77250471 0.5218812513
H2O 0 0
TOTAL 2.6066606334
Drum Volume
Vv 7.7375187314 m3
H-Dt Ratio
H 1594.54738679 H > 4DT
Dt 1.3466408407 m
f 12650
c 0.125
E 0.8
t 0.0462421949
ts 0.1875 inch
w 0.8113316727
th 0.1631799014
thead standar 0.1875 inch
sf 1,5-2,25
sf yang dipakai 2
a 26.50862495
b 8.8934720308
AB 23.25862495
BC 50.75
AC 45.1065279692
OA 11.0809720308 inch
KONSTANTA VAPOR PRESSURE
B C D E
-570.97 -3.3373 2.1999E-09 1.3096E-05
-999.62 -4.5788 9.9746E-11 6.7880E-06
-1507.2 -6.48 -4.2845E-11 5.4982E-06
-1923.5 -7.2064 7.4852E-12 3.6481E-06
-2445.2 -10.405 -7.4629E-11 5.4070E-06
-2622.1 -9.1784 3.0930E-12 3.6780E-06
-3064 -10.679 1.2244E-10 3.6680E-06
-3.1522E+03 -7.3037E+00 2.4247E-09 1.8090E-06
MECHANICAL DESIGN
ODUCT
Molar Flow Rate Fraction MwL VL
BOTTOM PRODUCT
53.0172499 inch
26.50862495 inch
14.6959 psi
17.63508 psi
Brownell 13.1
Brownell 13.2
Appendix F Brownell
2.4388429587
Densitas Liquid
657.2883390758
FEED T 177.5078048702 K
IN %mass kg/jam kmol/jam fraksi
Methane 0.011 626.849 39.0730664608 0.0272536796
Ethylene 0.060 3769.236 134.3564668062 0.0937143776
Propylene 0.596 36992.204 879.0714208869 0.6131571709
Butene 0.331 20542.507 366.13091356 0.2553783342
Pentene 0.003 1054.990 15.042491459 0.0104922209
Hexene 0.000 0.508 0.0060416713 4.214099114E-06
Heptene 0.000 0.000 3.7044413128E-06 2.583868274E-09
H2O 0.000 0.000 0 0
total 1433.6804045487
DISTILAT T 171.7378608739 K
OUT %mass kg/jam kmol/jam fraksi
Methane 0.161 676.8888132064 42.192159397 0.2523357774
Ethylene 0.818 3446.8665495722 122.865422028 0.7348128711
Propylene 0.021 90.4245763212 2.1488219463 0.0128513132
Butene 0.000 0.0003592861 6.403588305E-06 3.829750494E-08
Pentene 0.000 3.150624797952E-10 4.4922930361E-12 2.686675135E-14
Hexene 0.000 5.071056539217E-17 6.0254233424E-19 3.603583948E-21
Heptene 0.000 3.323649237798E-24 3.3849851691E-26 2.024435052E-28
H2O 0.000 0 0 0
total 167.2064097748
BOTTOM T 248.9487322267 K
OUT %mass kg/jam kmol/jam fraksi
Methane 0.000 0.0061564348 0.0003837459 2.983409231E-07
Ethylene 0.006 360.6690191094 12.8562422153 0.0099950087
Propylene 0.637 37731.0932493479 896.6301477947 0.697079749
Butene 0.354 20999.1050475115 374.2688977759 0.2909731175
Pentene 0.003 175.7048484774 2.5052734548 0.0019477099
Hexene 0.000 0.4436441274 0.0052713742 4.098198394E-06
Heptene 0.000 0.0023379358 2.3810810236E-05 1.851157209E-08
H2O 0.000 0 0 0
total 1286.2662401716
di dj bj bi αm
0.7348128711 0.0128513132 0.697079749 0.0099950087 14.9833619743
DISTRIBUSI NONKEY
Feed Distilat
Component
Kmol/jam Xi Kmol/jam xi,d
Methane 39.0730664608 0.0272536796 3.7011983998 0.0272536796
Ethylene 134.3564668062 0.0937143776 12.726923812 0.0937143776
Propylene 879.0714208869 0.6131571709 83.2700893739 0.6131571709
Butene 366.13091356 0.2553783342 34.681771208 0.2553783342
Pentene 15.042491459 0.0104922209 1.4249008425 0.0104922209
Hexene 0.0060416713 4.214099113758E-06 0.0005722977 4.214099114E-06
Heptene 3.7044413127915E-06 2.583868274295E-09 3.5090340997E-07 2.583868274E-09
H2O 0 0 0 0
Total 135.8054562847
PERHITUNGAN R MIN
P 760 mmHg
Pi K yi
22737.2617969508 29.9174497328 0.8153605909
1201.578151704 1.5810238838 0.1481646693
44.3016132022 0.0582915963 0.0357419103
2.4101505015 0.0031712507 0.0008098687
0.1845409369 0.000242817 2.54768982820487E-06
0.0140905475 1.8540194091499E-05 7.81302154898853E-11
0.0009140482 1.2026949755014E-06 3.10760539085193E-15
0.000053926 0.000000071 0
1.0000795869
P 760 mmHg
Pi K xi LK Ethylene
18628.3295664659 24.5109599559 0.0102948142 HK Propylene
876.1626103359 1.1528455399 0.6373905659
27.7373632073 0.0364965305 0.3521242442
1.3003150732 0.0017109409 2.23838855343631E-05
0.0874406857 0.0001150535 2.33515220922285E-10
0.0059833868 7.8728773028925E-06 4.57721339887598E-16
0.0003364376 4.4268106120028E-07 4.57312324756695E-22
1.723239901192E-05 2.2674209226216E-08 0
0.9998320084
P 760 mmHg
Pi K yi
23999.3077244897 31.5780364796 0.000009421
6471.6779447733 8.5153657168 0.0851111541
910.5795582958 1.1981309978 0.8351928551
208.4928807652 0.2743327378 0.079823452
33.2444919583 0.0437427526 8.51981910483879E-05
8.4094896556 0.011065118 4.53470486911592E-08
1.7025519211 0.0022401999 4.14696218816956E-11
0.4993880412 0.0006570895 0
1.0002221258
α(avg)
133.0438422291
14.9833619743 Nminimum 3.0628616364
1
0.1036044426
0.0107281563
0.0014114543
0.0001505951
1.845866997659E-05
(di/dj)*(bj/bi)
3987.7556318699
Bottom
Kmol/jam xi,b dr/br 0.0023966
35.371868061 0.0272536796
121.6295429942 0.0937143776
795.801331513 0.6131571709
331.449142352 0.2553783342
13.6175906166 0.0104922209
0.0054693737 4.214099113758E-06
3.353537902821E-06 2.5838682742949E-09
0 0
1297.874948264
KONSTANTA VAPOR PRESSURE
Molecular Weight Density
A B
16.043 0.656 14.667 -570.97
28.054 1.18 18.796 -999.62
42.081 1.74 24.539 -1507.2
56.107 620 27.312 -1923.5
70.134 640 36.274 -2445.2
84.161 673 33.449 -2622.1
98.188 697 38.126 -3064
18.02 997 29.8605 -3.1522E+03
(Yaws,1977) (PubChem)
log10(P)=A+B/T+C*log10(T)+D*T+E*T^2
KONSTANTA VAPOR PRESSURE
C D E
-3.3373 2.1999E-09 1.3096E-05
-4.5788 9.9746E-11 6.7880E-06
-6.48 -4.2845E-11 5.4982E-06
-7.2064 7.4852E-12 3.6481E-06
-10.405 -7.4629E-11 5.4070E-06
-9.1784 3.0930E-12 3.6780E-06
-10.679 1.2244E-10 3.6680E-06
-7.3037E+00 2.4247E-09 1.8090E-06