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Abstract
In this experimental investigation the influence of the applied tow tension during filament winding on the physical and mechanical
properties of glass-fibre reinforced polymeric composite tubulars, was studied. Pressure retaining tubular products used in the
transportation/storage of fluids are generally subjected to a variety of loading conditions during their service life; thus tubular specimens were
tested under different biaxial loading ratios. The stress/strain response was recorded and functional and structural failure envelopes were
developed. These envelopes indicate the leakage and final failure characteristics of the components, respectively. The mechanical properties
were analysed in conjunction with the measured physical properties: ‘fibre volume fraction’ and ‘effective wall thickness’. Experimental
findings demonstrate that the component strength depends on the degree of fibre tensioning. Under fibre-dominated loading conditions,
higher winding tension leads to an improved resistance against failure of tubular components, whereas under matrix-dominated loading
failure is delayed by reduced fibre tensioning.
q 2002 Published by Elsevier Science Ltd.
Keywords: E. Filament winding; B. Physical properties; B. Mechanical properties; Fibre-reinforced composites
study are presented. The focus is to investigate the influence 2.2. Determination of the fibre volume fraction
of the primary processing parameter ‘winding tension’ on
the performance of pressurised tubular components. First, The fibre volume fraction was determined by a resin
the effect of tow tensioning on the physical properties ‘fibre burnout test. Ring samples of 25.4 mm length were taken
volume fraction’ and ‘effective wall thickness’ are from several locations along the length of a tubular. It is
described. Using a unique tow tensioning system [7], important to point out that the outside surface of these
specimens were produced applying different winding sections was machined to three-fourth of their individual
tensions. In this study an angle-ply lay-up of [^ 6083]T average wall thickness, exposing the fibres of the top cover
was chosen, which is typical of pressurised composite of the fibre bed. This preparation step was necessary for the
structures such as piping that usually incorporate lay-up following reason: Excess resin accumulates on the outside
configurations with winding angles between 55 and 708. The surface during the winding process building a resin cover
investigation on physical properties was then extended to that strongly affects a weight-based determination of the
the mechanical properties of the components. Structures in fibre volume fraction. It was found that measurements
industrial applications are generally subjected to complex without removing the resin cover do not result in an useful
loading states; thus, monotonic tests were conducted parameter, as only the ‘local’ fibre volume fraction (nf )
applying several biaxial loading ratios. The experimental within the fibre bed significantly influences mechanical part
set-up was designed to facilitate testing for functional and properties.
structural failure, i.e. the loss of the fluid containment After machining, several sample sections from a single
capability and the structural integrity. Functional and tubular were subjected to an elevated temperature of 540 8C
structural failure envelopes were developed and analysed for three hours leaving the pure glass fibre bed behind.
qualitatively, providing an insight into the material Knowing the weight of each section before and after the
behaviour for a wider range of structures and loading burnout procedure, and the densities of the constituents, an
configurations. average fibre volume fraction was determined for each
manufactured tubular batch.
2. Testing program and experimental procedures 2.3. Experimental procedures for the determination
of mechanical properties
2.1. Specimen material system and fabrication method
Mechanical testing was done under stress control using a
Tubular specimens were produced by the wet filament facility for multiaxial loading of tubular specimens [10].
winding method. A four axis, computer controlled winding Different biaxial loading ratios (given by the ratio of Hoop
system was used for the fabrication. The winding machine to Axial stress [H:A]) were applied by internal pressuris-
was equipped with a unique numerically controlled ation and axial loading of the specimens. These ratios were:
tensioning system that allows for accurate tension control [1H:0A], i.e. a pure hoop loading, [3H:1A], i.e. a loading
of each individual tow [7]. Eight tows of an Owens-Corning condition in which—based on netting analysis—the result-
E-glass fibre material of 0.735 g/m weight were tensioned, ing stress coincides with the applied fibre direction,
and guided through a drum-type resin bath. As matrix [2H:1A], i.e. an unconstrained loading condition (‘pressure
material, Resolution Performance’s EPON826/EPI- vessel loading’), and [1H:15A], i.e. an effectively pure axial
CURE9551 two-component resin system was used, which loading condition (note that a low internal pressurisation
was kept at a constant temperature of 30 8C in the resin tank. was necessary to facilitate the investigation of leakage
Wet tows were finally combined to a fibre band while events).
passing though the pay-out eye of the winding machine and Tubular specimens were provided with aluminium end
placed in an helical pattern onto chrome-plated steel tabs resulting in a 102 mm gauge section. A strain gauge
mandrels with a diameter of 38.1 mm. Six layers were rosette with a perpendicular grid was aligned in axial and
deposited creating a [^ 6083]T interwoven angle-ply lay-up. hoop direction of the tubular and bonded at the mid-length
Two batches of specimens were produced by applying of the specimen. Hoop and axial stresses (sH and sA ) were
uniform tow tension of 26.7 and 44.5 N, respectively. computed according to Eqs. (1) and (2) from the recorded
After completion of the winding sequence, excessive internal pressure pi and the applied axial load FA. Together
built-up of liquid resin on the surface of the parts was with the hoop and axial strain gauge readings (1H and 1A )
removed using a foam brush. Parts were then cured in a two- the global stress –strain response was obtained
stage curing cycle at 80 and 120 8C for 1 and 2.5 h,
respectively, (excluding ramping times of 15 min) and IDðpi 2 po Þ 2 2spo
sH ¼ ð1Þ
afterwards allowed to cool down to room temperature. 2s
Finally, mandrels were extracted from the tubulars, and
specimens of a specified length were machined from the ID2 ðpi 2 po Þ 2 4po sðID þ sÞ FA
sA ¼ þ ð2Þ
parts. 4sðID þ sÞ psðID þ sÞ
P. Mertiny, F. Ellyin / Composites: Part A 33 (2002) 1615–1622 1617
the overall average specimen thickness including the resin loading condition was applied (i.e. zero axial load).
cover was found to be 1.38 mm Consequently, the actual loading ratios deviate from the
TEX TOW C
tðCOVER#nÞ ¼ ð3Þ
nf rf pððID=2Þ þ tðCOVER#1Þ þ · · · þ tðCOVER#n 2 1ÞÞcosðaÞ
Fig. 2. Biaxial stress–strain response for a pure hoop [1H:0A] loading ratio, Fig. 3. Biaxial stress–strain response for a [3H:1A] loading ratio, 1A, 1H:
1A, 1H: axial and hoop strain (measured); 1T, 1P (calculated) transverse and axial and hoop strain (measured); 1T, 1P (calculated) transverse and parallel
parallel to fibre strain. to fibre strain.
P. Mertiny, F. Ellyin / Composites: Part A 33 (2002) 1615–1622 1619
axial stress value. At this point the specimen also lost its
load-bearing capability, consequently, the functional and
structural failure coincide in this loading case.
Fig. 5. Biaxial stress– strain response for an effectively pure axial [1H:15A] Fig. 6. Photograph of specimens failed under (a) [3H:1A], (b) [2H:1A] and
loading ratio, 1A, 1H: axial and hoop strain (measured); 1T, 1P (calculated) (c) [1H:15A] loading conditions, and (d) undamaged specimen (from left to
transverse and parallel to fibre strain. right).
1620 P. Mertiny, F. Ellyin / Composites: Part A 33 (2002) 1615–1622
5. Discussion
Fig. 10. Mohr’s circle illustration for comparison of the [3H:1A] and
[2H:1A] structural failure behaviour.
Fig. 9. Mohr’s circle illustration for comparison of the [3H:1A] and the specimen end tabs. Depending on the amount of strength
[1H:0A] structural failure behaviour. reduction, axial stresses at failure, sA, can be higher or
parallel to the fibres at structural failure under [3H:1A] lower than the corresponding axial stresses in the [3H:1A]
loading is assumed to be the maximum tensile strength of loading case; thus explaining the intersection of the
the fibre/matrix structure, sPmax. structural failure envelopes for the high and low fibre
Mohr’s circles were chosen to illustrate the conditions volume fraction.
under pure hoop loading, see Fig. 9. The [3H:1A] loading
condition is represented by the top circle acting as a scale for
comparison with the circle for the [1H:0A] loading case 6. Conclusions
(shown below). The second circle was constructed using the
maximum tensile strength of the fibre/matrix structure, In this investigation the effect of the primary manufac-
sPmax, and the given loading ratio. It can be observed that turing parameter ‘winding tension’ on physical and
the hoop stress, sH, is necessarily greater than that in the mechanical properties of filament wound [^ 6083]T compo-
first circle. This corresponds with the behaviour shown in site tubulars was studied. Specimens were manufactured
the structural failure envelope (Fig. 7). Moreover, the using different winding tensions, and mechanical testing
transverse stress, sT, for the pure hoop loading case is was conducted under different loading ratios. Results from
shown to be considerably less than that under [3H:1A] the mechanical testing were compiled into functional and
loading. This then supports the assumption that significant structural failure stress envelopes, and the observed
matrix cracking did not occur under the pure hoop loading. mechanical behaviour was analysed qualitatively to show
Comparing the failure behaviour under [3H:1A] and the plausibility of the experimental findings. Linking the
[2H:1A] loading using a similar approach as presented applied winding tension to the physical properties of a part,
above supports the assumption of a localised load as well as to the mechanical response at failure, led to the
concentration in the fibre structure (see Section 4.2). In following conclusions.
the bottom part of Fig. 10, a Mohr’s circle for the [2H:1A]
loading was constructed using a fibre angle of 558, which is † Increasing the filament winding tow tension significantly
the limit case for fibre realignment after matrix breakdown increased fibre compaction; thus the primary processing
(found by conducting netting analysis for the particular parameter ‘winding tension’ is suited for controlling the
loading ratio). Matching the stresses parallel to the fibre fibre volume fraction of the manufactured components.
direction (i.e. sP ¼ sPmax ) for the two considered loading † Mechanical testing revealed that stresses at functional
ratios, resulted in nearly identical hoop stress values sH. and structural failure depend on the applied winding
This does not correspond with the experimental results, tension.
where the hoop stress is found to be less in the [2H:1A] † Comparison of test results from specimens wound with a
loading case. However, incorporating a decreased maxi- low and high tow tension indicated that the mechanical
mum strength of the fibre structure (i.e. sP , sPmax) gave a properties do not follow a simple unidirectional trend.
representation that quantitatively matched the experimental Generally, an increase in winding tension has a beneficial
findings. Such a decrease was already suggested in Section effect on the component strength in the case of a fibre
4.3 based on the presence of additional bending loads near dominated loading, whereas under a matrix dominated
1622 P. Mertiny, F. Ellyin / Composites: Part A 33 (2002) 1615–1622
loading condition a slight decrease in the failure strength [5] Cohen D. Influence of filament winding parameters on composite
was obtained by increasing fibre compaction. vessel quality and strength. Composites Part A 1997;28A:
1035–47.
[6] Cohen D, Mantell SC, Zhao L. The effect of fibre volume fraction on
filament wound composite pressure vessel strength. Composites Part
Acknowledgements B 2001;32B:413–29.
[7] Wolodko J, Mertiny P, Meijer G, Martens M, Ellyin F. Development
This research was made possible by the contributions of a facility for filament winding GFRP tubulars. In: Proceedings of
from TransCanada Pipelines Limited, the Alberta Intellec- 46th International SAMPE Symposium. Long Beach; May 2001.
p.1271–82.
tual Infrastructure Partnership Program (IIPP), the Canadian
[8] Soden PD, Leadbetter D, Griggs PR, Eckold GC. The strength of a
Foundation for Innovation (CFI), the Natural Sciences and filament wound composite under biaxial loading. Composites 1978;
Engineering Research Council (NSERC) and the University 9(4):247–50.
of Alberta. In addition, the authors would also like to [9] Soden PD, Kitching R, Tse PC. Experimental failure stresses for ^558
acknowledge the contributions made by the members of the filament wound glass fibre reinforced plastic tubes under biaxial
ACME group and the technical staff at the Department of loading. Composites 1989;20(2):125–35.
[10] Ellyin F, Wolodko J. Testing facilities for multiaxial loading of
Mechanical Engineering (J. Wolodko, G. Meijer and B. tubular specimens. In: Kalluri S, Bonacuse PJ, editors. Multiaxial
Faulkner). fatigue and deformation testing techniques. ; 1997. p. 7–24. ASTM
STP 1280.
[11] Wolodko J. Biaxial fatigue and leakage characteristics of fiber
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