4.

---- PROCESSING PARAMETERS ----

sexp( 0.2[Hz], 0.0[s] )
trapezoid( 0[%], 0[%], 80[%], 100[%] )
zerofill( 1 )
fft( 1, TRUE, TRUE )
machinephase
ppm

Derived from: 190617-1254-POLYOL_Proton-1-1.j

3.0

Filename = 190617-1254-POLYOL_Pr
Author = delta
Experiment = proton.jxp
Sample_Id = 190617-1254-POLYOL
Solvent = METHANOL-D4
Actual_Start_Time = 20-JUN-2019 10:54:11
Revision_Time = 28-JUN-2019 09:44:13

Comment = single_pulse
Data_Format = 1D COMPLEX
2.0

Dim_Size = 13107
X_Domain = Proton
Dim_Title = Proton
Dim_Units = [ppm]
Dimensions = X
Spectrometer = JNM-ECZ500R/S1

Field_Strength = 11.7473579[T] (500[MH

X_Acq_Duration = 1.74587904[s]
X_Domain = Proton
X_Freq = 500.15991521[MHz]
X_Offset = 7.0[ppm]
X_Points = 16384
X_Prescans = 1
1.0

X_Resolution = 0.57277737[Hz]
X_Sweep = 9.38438438[kHz]
X_Sweep_Clipped = 7.50750751[kHz]
Irr_Domain = Proton
Irr_Freq = 500.15991521[MHz]
Irr_Offset = 5.0[ppm]
Tri_Domain = Proton
Tri_Freq = 500.15991521[MHz]
Tri_Offset = 5.0[ppm]
Blanking = 2[us]
abundance

H2O Clipped
Scans
=
=
FALSE
80
CD3OD Total_Scans = 80
0

Relaxation_Delay = 5[s]
Recvr_Gain = 26
14.0 13.0 12.0 11.0 10.0 9.0 8.0 7.0 6.0 5.0 4.0 3.0 2.0 1.0 0 Temp_Get = 20.5[dC]
X_90_Width = 8[us]
X_Acq_Time = 1.74587904[s]
X_Angle = 45[deg]
4.928

3.674
3.664
3.611
3.601
3.588
3.578
3.538
3.525
3.515
3.502
X_Atn = 8.9[dB]
X_Pulse = 4[us]
Irr_Mode = Off
X : parts per Million : Proton Tri_Mode = Off
 4.0

---- PROCESSING PARAMETERS ----

sexp( 0.2[Hz], 0.0[s] )
trapezoid( 0[%], 0[%], 80[%], 100[%] )
zerofill( 1 )
fft( 1, TRUE, TRUE )
machinephase
ppm

Derived from: 190617-1254-POLYOL_Proton-1-1.j

3.0

Filename = 190617-1254-POLYOL_Pr
Author = delta
Experiment = proton.jxp
Sample_Id = 190617-1254-POLYOL
Solvent = METHANOL-D4
Actual_Start_Time = 20-JUN-2019 10:54:11
Revision_Time = 28-JUN-2019 09:44:13

Comment = single_pulse
Data_Format = 1D COMPLEX
2.0

Dim_Size = 13107
X_Domain = Proton
Dim_Title = Proton
Dim_Units = [ppm]
Dimensions = X
Spectrometer = JNM-ECZ500R/S1

Field_Strength = 11.7473579[T] (500[MH

X_Acq_Duration = 1.74587904[s]
X_Domain = Proton
X_Freq = 500.15991521[MHz]
X_Offset = 7.0[ppm]
X_Points = 16384
X_Prescans = 1
1.0

X_Resolution = 0.57277737[Hz]
X_Sweep = 9.38438438[kHz]
X_Sweep_Clipped = 7.50750751[kHz]
Irr_Domain = Proton
Irr_Freq = 500.15991521[MHz]
Irr_Offset = 5.0[ppm]
Tri_Domain = Proton
Tri_Freq = 500.15991521[MHz]
Tri_Offset = 5.0[ppm]
Blanking = 2[us]
abundance

H2O Clipped
Scans
=
=
FALSE
80
CD3OD Total_Scans = 80
0

Relaxation_Delay = 5[s]
Recvr_Gain = 26
5.0 4.9 4.8 4.7 4.6 4.5 4.4 4.3 4.2 4.1 4.0 3.9 3.8 3.7 3.6 3.5 3.4 3.3 Temp_Get = 20.5[dC]
X_90_Width = 8[us]
X_Acq_Time = 1.74587904[s]
X_Angle = 45[deg]
4.928

3.696
3.686
3.683
3.674
3.664
3.652
3.611
3.601
3.588
3.578
3.557
3.538
3.525
3.515
3.502

3.313
3.310
X_Atn = 8.9[dB]
X_Pulse = 4[us]
Irr_Mode = Off
X : parts per Million : Proton Tri_Mode = Off
 3.0

---- PROCESSING PARAMETERS ----

sexp( 0.2[Hz], 0.0[s] )
trapezoid( 0[%], 0[%], 80[%], 100[%] )
zerofill( 1 )
fft( 1, TRUE, TRUE )
machinephase
ppm

Derived from: 190617-1254-POLYOL_Proton-1-1.j

Filename = 190617-1254-POLYOL_Pr
Author = delta
2.0

Experiment = proton.jxp
Sample_Id = 190617-1254-POLYOL
Solvent = METHANOL-D4
Actual_Start_Time = 20-JUN-2019 10:54:11
Revision_Time = 28-JUN-2019 09:45:53

Comment = single_pulse
Data_Format = 1D COMPLEX
Dim_Size = 13107
X_Domain = Proton
Dim_Title = Proton
Dim_Units = [ppm]
Dimensions = X
Spectrometer = JNM-ECZ500R/S1

Field_Strength = 11.7473579[T] (500[MH

X_Acq_Duration = 1.74587904[s]
X_Domain = Proton
1.0

X_Freq = 500.15991521[MHz]
X_Offset = 7.0[ppm]
X_Points = 16384
X_Prescans = 1

1.98

1.97
X_Resolution = 0.57277737[Hz]
X_Sweep = 9.38438438[kHz]
X_Sweep_Clipped = 7.50750751[kHz]
Irr_Domain = Proton
Irr_Freq = 500.15991521[MHz]
Irr_Offset = 5.0[ppm]
Tri_Domain = Proton

1.00
Tri_Freq = 500.15991521[MHz]
Tri_Offset = 5.0[ppm]
H2O Blanking = 2[us]
abundance

Clipped = FALSE
Scans = 80
CD3OD Total_Scans = 80
0

Relaxation_Delay = 5[s]
Recvr_Gain = 26
5.0 4.9 4.8 4.7 4.6 4.5 4.4 4.3 4.2 4.1 4.0 3.9 3.8 3.7 3.6 3.5 3.4 3.3 Temp_Get = 20.5[dC]
X_90_Width = 8[us]
X_Acq_Time = 1.74587904[s]
X_Angle = 45[deg]
4.928

3.696
3.686
3.683
3.674
3.664
3.652
3.611
3.601
3.588
3.578
3.557
3.538
3.525
3.515
3.502

3.313
3.310
X_Atn = 8.9[dB]
X_Pulse = 4[us]
Irr_Mode = Off
X : parts per Million : Proton Tri_Mode = Off
 3.0

---- PROCESSING PARAMETERS ----

sexp( 0.2[Hz], 0.0[s] )
trapezoid( 0[%], 0[%], 80[%], 100[%] )
zerofill( 1 )
fft( 1, TRUE, TRUE )
machinephase
ppm

Derived from: 190617-1254-POLYOL_Proton-1-1.j

Filename = 190617-1254-POLYOL_Pr
Author = delta
2.0

Experiment = proton.jxp
Sample_Id = 190617-1254-POLYOL
Solvent = METHANOL-D4
Actual_Start_Time = 20-JUN-2019 10:54:11
Revision_Time = 28-JUN-2019 09:45:53

Comment = single_pulse
Data_Format = 1D COMPLEX
Dim_Size = 13107
X_Domain = Proton
Dim_Title = Proton
Dim_Units = [ppm]
Dimensions = X
Spectrometer = JNM-ECZ500R/S1

Field_Strength = 11.7473579[T] (500[MH

X_Acq_Duration = 1.74587904[s]
X_Domain = Proton
1.0

X_Freq = 500.15991521[MHz]
X_Offset = 7.0[ppm]
X_Points = 16384
X_Prescans = 1

1.98

1.97
X_Resolution = 0.57277737[Hz]
X_Sweep = 9.38438438[kHz]
X_Sweep_Clipped = 7.50750751[kHz]
Irr_Domain = Proton
Irr_Freq = 500.15991521[MHz]
Irr_Offset = 5.0[ppm]
Tri_Domain = Proton
1.00

Tri_Freq = 500.15991521[MHz]
Tri_Offset = 5.0[ppm]
Blanking = 2[us]
abundance

Clipped = FALSE
Scans = 80
Total_Scans = 80
0

Relaxation_Delay = 5[s]
Recvr_Gain = 26
3.7 3.6 3.5 Temp_Get = 20.5[dC]
X_90_Width = 8[us]
X_Acq_Time = 1.74587904[s]
X_Angle = 45[deg]
3.696
3.686
3.683
3.674
3.664

3.652

3.611
3.601

3.588
3.578

3.557

3.538

3.525
3.515

3.502

X_Atn = 8.9[dB]
X_Pulse = 4[us]
Irr_Mode = Off
X : parts per Million : Proton Tri_Mode = Off
 60.0

---- PROCESSING PARAMETERS ----

sexp( 2.0[Hz], 0.0[s] )
trapezoid( 0[%], 0[%], 80[%], 100[%] )
zerofill( 1 )
fft( 1, TRUE, TRUE )
50.0

machinephase
ppm
40.0

Filename = 190617-1254-POLYOL
Author = delta
Experiment = carbon.jxp
Sample_Id = 190617-1254-POLYOL
Solvent = METHANOL-D4
Actual_Start_Time = 21-JUN-2019 08:24:
Revision_Time = 28-JUN-2019 09:48:

Comment = single pulse decou

30.0

Data_Format = 1D COMPLEX
Dim_Size = 26214
X_Domain = Carbon13
Dim_Title = Carbon13
Dim_Units = [ppm]
Dimensions = X
Spectrometer = JNM-ECZ500R/S1

Field_Strength = 11.7473579[T] (500

20.0

X_Acq_Duration = 0.82837504[s]
X_Domain = Carbon13
X_Freq = 125.76529768[MHz]
X_Offset = 100[ppm]
X_Points = 32768
X_Prescans = 4
X_Resolution = 1.20718268[Hz]
X_Sweep = 39.55696203[kHz]
X_Sweep_Clipped = 31.64556962[kHz]
10.0

Irr_Domain = Proton
Irr_Freq = 500.15991521[MHz]
Irr_Offset = 5.0[ppm]
Blanking = 2[us]
(thousandths)

Clipped = FALSE
Scans = 5120
Total_Scans = 5120

Relaxation_Delay = 2[s]
CD3OD Recvr_Gain
Temp_Get
=
=
36
21.2[dC]
0

X_90_Width = 11.3[us]
X_Acq_Time = 0.82837504[s]
220.0 210.0 200.0 190.0 180.0 170.0 160.0 150.0 140.0 130.0 120.0 110.0 100.0 90.0 80.0 70.0 60.0 50.0 40.0 30.0 20.0 10.0 0 X_Angle = 30[deg]
X_Atn = 11[dB]
X_Pulse = 3.76666667[us]
Irr_Atn_Dec = 30.11[dB]
73.778
64.276
49.618
49.446
49.273
49.100
48.937
48.764
48.591

Irr_Atn_Dec_Calc = 30.11[dB]
Irr_Atn_Dec_Default_Calc = 30.11[dB]
Irr_Atn_Noe = 30.11[dB]
X : parts per Million : Carbon13 Irr_Dec_Bandwidth_Hz = 5.97826087[kHz]
 60.0

---- PROCESSING PARAMETERS ----

sexp( 2.0[Hz], 0.0[s] )
trapezoid( 0[%], 0[%], 80[%], 100[%] )
zerofill( 1 )
fft( 1, TRUE, TRUE )
50.0

machinephase
ppm
40.0

Filename = 190617-1254-POLYOL
Author = delta
Experiment = carbon.jxp
Sample_Id = 190617-1254-POLYOL
Solvent = METHANOL-D4
Actual_Start_Time = 21-JUN-2019 08:24:
Revision_Time = 28-JUN-2019 09:48:

Comment = single pulse decou

30.0

Data_Format = 1D COMPLEX
Dim_Size = 26214
X_Domain = Carbon13
Dim_Title = Carbon13
Dim_Units = [ppm]
Dimensions = X
Spectrometer = JNM-ECZ500R/S1

Field_Strength = 11.7473579[T] (500

20.0

X_Acq_Duration = 0.82837504[s]
X_Domain = Carbon13
X_Freq = 125.76529768[MHz]
X_Offset = 100[ppm]
X_Points = 32768
X_Prescans = 4
X_Resolution = 1.20718268[Hz]
X_Sweep = 39.55696203[kHz]
X_Sweep_Clipped = 31.64556962[kHz]
10.0

Irr_Domain = Proton
Irr_Freq = 500.15991521[MHz]
Irr_Offset = 5.0[ppm]
Blanking = 2[us]
(thousandths)

Clipped = FALSE
Scans = 5120
Total_Scans = 5120

Relaxation_Delay = 2[s]
CD3OD Recvr_Gain
Temp_Get
=
=
36
21.2[dC]
0

X_90_Width = 11.3[us]
X_Acq_Time = 0.82837504[s]
74.0 73.0 72.0 71.0 70.0 69.0 68.0 67.0 66.0 65.0 64.0 63.0 62.0 61.0 60.0 59.0 58.0 57.0 56.0 55.0 54.0 53.0 52.0 51.0 50.0 49.0 X_Angle = 30[deg]
X_Atn = 11[dB]
X_Pulse = 3.76666667[us]
Irr_Atn_Dec = 30.11[dB]
73.778

64.276

49.618
49.446
49.273
49.100
48.937
48.764
48.591
Irr_Atn_Dec_Calc = 30.11[dB]
Irr_Atn_Dec_Default_Calc = 30.11[dB]
Irr_Atn_Noe = 30.11[dB]
X : parts per Million : Carbon13 Irr_Dec_Bandwidth_Hz = 5.97826087[kHz]