Penetration Test

INTRODUCTION

The consistency of bituminous materials varies depending upon several factors such as
constituents, temperature, etc. At temperature ranges between 25 and 50ºC most of the paving
bitumen grades remain in semi-solid or in plastic state and their viscosity is so high that they do
not flow as liquid and can not be mixed with aggregates. But some grades of cutback bitumen
and bituminous emulsion are in liquid state and the viscosity is sufficiently low at this temperature
range enabling these binders to be sprayed or to be mixed with aggregates without heating.
Determination of absolute viscosity of bituminous materials is not so simple. Therefore the
consistency of these materials are determined by indirect methods. Penetration test is one such
indirect test to determine the consistency of paving grade bitumen, which is a very simple test.
The viscosity of tars and cutback bitumen are determined indirectly using an orifice viscometer in
terms of time required for a specified quantity of material to flow through an orifice of specified
size at the specified temperature. There is a certain range of consistency of bituminous
materials, wherein the material is too soft for penetration test, but the viscosity is so high that the
material cannot flow through the orifice of the viscometer; the consistency of such materials is
measured by ‘float test’.
Various types and grades of bituminous materials are available depending on their origin and
refining process. The penetration test determines the consistency of these materials for the
purpose of grading them, by measuring the depth (in units of one tenth of a millimetre or one
hundredth of a centimetre) to which a standard needle will penetrate vertically under specified
conditions of standard load, duration and temperature. Thus the basic principle of the penetration
test is the measurement of the penetration (in units of one tenth of a mm) of a standard needle in
a bitumen sample maintained at 25ºC during five seconds, the total weight of the needle
assembly being 100 g. The concept of the penetration test on bitumen sample is illustrated in
Figure.1. The softer the bitumen, the greater will be the penetration.
The penetration test is widely used for classifying the bitumen into different grades. The BIS
has standardized the penetration test equipment and the test procedure. Even though it is
recognised that the empirical tests like penetration, softening point etc. cannot fully qualify the
paving binder for its temperature susceptibility characteristics, the simplicity and quickness of
operation of this test cannot be ignored for common use.

Apparatus

The apparatus for conducting penetration test on bitumen consists of penetrometer, container,
thermostatically controlled water bath, thermometer, stop watch and transfer dish. Following are
the standard specifications as per BIS.
Penetration test apparatus or Penetrometer : This apparatus consists of a penetration needle
assembly which is attached to a calibrated dial. On release, the penetration needle
penetrates into the bitumen specimen without appreciable friction. The penetration unit
consists of a straight, polished cylindrical stainless steel needle of total length 50 mm and
diameter 1.0 mm with a pointed end, the conical end of the penetration needle tapers from a
diameter of 1.0 mm to 0.15 mm through a length of 5 mm. The other end of the needle is rigidly
fixed to a shank of diameter 3 mm. The gross weight of the penetration needle assembly is
100 g. The dial of the penetrometer is calibrated to measure the penetration value in units of
one tenth of a mm. The specified standard test temperature is 25o C and duration of penetration
is 5 seconds.
 Fig. 1 Penetration Test Concept

Fig. 2 Penetrometer

Electrically operated automatic penetrometers are also available, in which the test duration is
automatically controlled, by releasing the test needle assembly for an exact duration of 5. 0
seconds. Typical sketch of penetrometer is shown in Figure 2

(b) Container : A flat bottomed cylindrical metal or glass container of diameter 55 mm and depth
35 mm is used to place the penetration test specimen of bitumen. A container of diameter 70
mm and depth 45 mm is used for testing bitumen binders with penetration values exceeding
225.
(c) Water Bath : A thermostatically controlled water bath containing not less than 10 litres of
water, maintained at 25 ± 1ºC so as to keep the containers with bitumen sample immersed in
water at a depth of 100 mm (or more) from the surface and supported on a perforated shelf
placed at 50 mm (or more) from the bottom of the water bath.
(d) Transfer tray : A small tray which can keep the bitumen container fully immersed in water at
25oC during the test.

(e) Thermometer : A thermometer to read up to 0.2oC

(f) Timer device : A timer device or stop watch, accurate to 0.1 of a second.

Procedure
The bitumen is heated to a pouring consistency, about 75 to 100ºC above the temperature at
which bitumen softens. The sample material is thoroughly stirred to make it homogeneous and
free from air bubbles and water. The bitumen sample is then poured into the containers of 35
mm depth (to a depth at least 15 mm more than the expected penetration). The sample
containers are placed on the transfer tray and cooled in atmosphere at temperature between 15
to 30oC for 60 to 90 minutes. Then the transfer tray, with the containers is placed in the
thermostatically controlled water bath maintained at a temperature of 25ºC for a period of 60 to
90 minutes. (For testing bitumen with penetration value between 225 and 350, the container of
depth 45 mm and diameter 70 mm is used and the cooling period in atmosphere and in the water
bath is 90 to 120 minutes each).
The transfer tray with the sample container and water is removed from the water bath and
placed under the needle of the penetrometer. Using the adjusting screw, the needle assembly is
lowered and the tip of the needle is made to just touch the top surface of the bitumen sample and
the needle assembly is clamped in this position. The contact of the tip of the needle is checked
using the mirror placed on the rear of the needle. The initial reading of the penetrometer dial is
either adjusted to zero or the initial reading is taken before releasing the needle. The needle is
released exactly for a period of 5.0 seconds by pressing the knob and the final reading is taken
on the dial. The needle assembly is then raised and the penetration needle is removed and
replaced by a clean, dry needle. The test is repeated on the same sample by conducting the
repeat test at a distance of not less than 10 mm. At least three such measurements are made on
this sample at testing distance of not less 10 mm apart. After each test the needle is disengaged
and cleaned with benzene and carefully dried. The test is repeated on the sample in the other
containers, after keeping in the water bath maintained at a temperature of 25ºC.

Results
The difference between the initial and final penetration readings is taken as the penetration
value. The mean value of not less than three consistent penetration measurements (which do not
differ by more than the values specified below) is reported as the penetration value.

Range of penetration value Maximum difference

0 - 49 2
50 – 149 4
150 - 249 6

The duplicate test results should not differ by more than the following limits :

Penetration value Repeatability Reproducibility

below 50 1 unit 4 units
Above 50 3 % of their mean 8 % of their mean
Discussion
It may be noted that the penetration value is influenced by any inaccuracy as regards :
(i) pouring temperature
(ii) size of needle
(iii) weight placed on the needle
(iv) test temperature
(v) duration of releasing the penetration needle
(vi) period of cooling
If the test temperature is higher than specified value of 25ºC, the penetration value obtained
will be much higher. The penetration value obtained will be higher, if the weight of the needle
assembly is higher than specified value of 100 g. Higher pouring temperature than that specified
value may cause hardening of bitumen and result in lower penetration values. The duration of
releasing the penetration needle should be exactly 5.0 seconds. It is also necessary to keep the
needle clean each time before testing in order to get consistent results. The penetration needle
should not be placed closer than 10 mm from the side of the dish or from earlier test location.

Hot air oven or sand bath may be used to avoid over heating of bottom of the container.
If the bitumen sample contains extraneous matter, it should be sieved through IS sieve No. 30

Applications of Penetration Test

Penetration test is the most commonly adopted test on bitumen to determine the grade of the
material in terms of its hardness because of its simplicity. The penetration grades of bitumen
binders are generally denoted as 80/100, 60/70 or 30/40 grade bitumen. 80/100 bitumen denotes
that the penetration value of the binder ranges between 80 and 100. The penetration values of
various types of bitumen used in pavement construction in this country range between 20 and
225. The appropriate grade of the bitumen binder to be used for road construction work is
decided depending upon the climatic condition of the project site, the type of construction /
specification and the pavement layer (base course / binder course / surface course). Harder
grade of bitumen binder with lower penetration value is generally chosen in warm regions. In
colder regions bitumen with higher penetration values are generally used. However binders
which become very stiff at low temperatures are not preferred for road construction in regions
with cold weather as the pavement may crack under traffic loads.
The penetration test is not intended to estimate the consistency of softer materials like cutback
or tar. These materials are usually graded by an indirect viscosity test such as orifice viscometer.
Some of the limitations of penetration test for grading of bitumen binders are :
Penetration test is an empirical test and there is no relation to the fundamental properties of the
binder ; the penetration test temperature of 25oC is not at all the actual pavement service
temperature, the service temperature of the pavement is much higher say, about 60oC for most
time of the day ; bitumen having the similar penetration value may have different performance
while in service, depending on its temperature susceptibility, because bitumen having the same
penetration value may have widely varying temperature-stiffness relationship.
In view of the above limitations, Viscosity Grading is currently recommended by the BIS for
paving applications.

It is to be stressed that the quality of the binder has a significant role on the performance of
the bituminous pavements. In developed countries, now-a-days, performance based binder and
mix specifications are generally adopted. Bitumen binders which are highly susceptible to
temperature changes may not be suitable for use in regions where the temperature variation
between summer and winter seasons are very high. Appropriate type of modified binders may be
chosen in such cases.
SELECTED REFERENCES

1. Bureau of Indian Standards, IS: 1203 –1978, Indian Standard Methods for Testing Tar and
Bituminous Materials : Determination of Penetration (First Revision)
3. Bureau of Indian Standards, IS-73-2006, Indian Standard Paving Bitumen - Specification
(Third Revision)
4. Road Research Laboratory, Bituminous Materials in Road Construction, H.M.S.O., London
5. Roberts, F.L, Kandhal, P.S, Brown E.R, Lee, D.Y and Kennedy, T.W, Hot Mix Asphalt
Materials, Mixture Design and Construction, (Second Edition 1996), NAPA Education
Foundation, Maryland

QUESTIONS

1. How is penetration test value of bitumen expressed ?

2. What are the standard load, time and temperature specified for penetration test ?
3. Briefly outline the penetration test procedure.
6. What do you understand by 80/100 bitumen ?
7. What are the common causes of errors during conduct of penetration tests ?
5. What are the effects of :the following on penetration tests results:
(i) higher test temperature (ii) higher pouring temperature (iii) exposed bitumen
6. What are the limitations of penetration test for grading of bitumen binders.
 OBSERVATION SHEET

Table 1, Results of Penetration Test

(i) Pouring temperature, ºC =

(ii) Period of cooling in atmosphere, minutes =
(iii) Room temperature, ºC =
(iv) Period of cooling in water bath, minutes =
(v) Actual test temperature, ºC =

Sample No. Sample No.

Readings Mean Mean
Test 1 Test 2 Test 3 Test 1 Test 2 Test 3
value value
Penetrometer dial
readings
(i) initial

(ii) final

Penetration value

Repeatability, percent

Mean penetration value =

Grade of bitumen =

Remarks :
Ductility and Elastic Recovery Tests

Ductility Test

INTRODUCTION

In the flexible pavement construction, it is desirable that the bitumen binders used in the
bituminous mixes form ductile thin films around the aggregates. This serves as a satisfactory
binder in improving the physical interlocking of the aggregates. The binder material which does
not possess sufficient ductility would crack and thus provide pervious pavement surface. This in
turn results in damaging effect to the pavement structure. It has been stated by some agencies
that the penetration and ductility properties go together; but depending upon the chemical
composition and the type of crude source of the bitumen sometimes it has been observed that the
above statement is incorrect. It may hence be mentioned that the bitumen may satisfy the
penetration value but may fail to satisfy the ductility requirements. Bitumen paving engineer
would however want that both test requirements are satisfied in the field jobs. Penetration test or
ductility test cannot in any case replace each other. The ductility value of bitumen binder is
expressed as the distance in centimetres to which a standard briquette of bitumen can be
stretched before the thread breaks. The test is conducted at 27 ± 0.5ºC and a rate of pull of 50 ±
2.5 mm per minute. The test has been standardized by the BIS. The ductility test concept is
shown in Figure 3.

Apparatus
The ductility test apparatus consists of items like sample (briquette) moulds water bath
square-end trowel or putty knife sharpened on end and ductility machine. Standard specifications
as per BIS re as follows:
(a) Briquette Mould : Mould is made of brass metal with shape and dimensions as indicated in
Figure 4. Both ends called clips possess circular holes to grip the fixed and movable ends of
the testing machine. When the side pieces are placed together in the briquette mould,
ductility test specimen of the following dimensions are obtained :

Length 75 mm

Distance between clips 30 mm

Width at mouth of clips 20 mm

Cross section at minimum width 10 mm × 10 mm

(b) Ductility Machine : It is an equipment which functions as constant temperature water bath
and a pulling device at a pre-calibrated rate. The central rod of the machine is threaded
and through a gear system provides movement to one end where the clip is fixed during
initial placement. The other clip end is hooked at the fixed end of the machine. Two clips
are thus pulled apart horizontally at a uniform speed of 50 ± 2.5 mm per minute. The
machine may have provision to fix two or more mould so as to test these specimens
simultaneously.
 Fig. 3 Ductility Test Concept

Fig. 4 Ductility Test Specimen and Mould

Procedure

The bitumen sample is melted to a temperature of 75ºC to 100ºC above the approximate
softening point until it is fluid. The molten bitumen is poured in the mould assembly and placed
on a brass plate, after a solution of glycerine and dextrine is applied at all surfaces of the mould
exposed to bitumen. Bitumen is poured into the moulds and the plate assembly along with the
sample is kept for air cooling in room temperature for 30 to 40 minutes. The air cooled specimen
is then placed in water bath maintained at 27ºC for 30 minutes. The sample and mould assembly
are removed from water bath and excess bitumen material is cut off by levelling the surface using
the hot knife. After trimming the specimen, the mould assembly containing sample, is replaced in
water bath maintained at 27ºC for 85 to 95 minutes. The sides of the mould are now removed
and the clips are carefully booked on the machine without causing any initial strain. Two or more
specimens may be prepared in the moulds and clipped to the machine so as to conduct these
tests simultaneously.
 The pointer is set to read zero or the initial reading of the pointer is noted. The machine is
started and the two clips are thus pulled apart horizontally. While the test is in operation, it is
checked whether the sample is immersed in water at depth of at least 10 mm. The distance at
which the bitumen thread of each specimen breaks, is recorded (in cm) to report as ductility
value.

Results

The distance stretched by the moving end of the specimen up to the point of breaking of
thread measured in centimetres is recorded as ductility value. The average of three tests is
reported as the ductility of the sample, provided the three values are within ± 5 percent of the
mean value. If the value is not within the above limits, but the two higher values are within ± 5
percent of the mean value, then the mean of the two values is considered as the test result.
During the test, if the stretched material of the specimen comes in contact with the bottom or top
surface of the bath, the test is not considered as normal. BIS specifies that the test results should
not differ by more than the following :

Repeatability 10 % of mean

Reproducibility 20 % of mean

Discussion

The ductility value gets seriously affected if any of the following factors are varied :
(i) Test temperature
(ii) Pouring temperature
(iii) Dimensions of briquette, particularly the cross section of the test sample at the minimum
width, which should be 10 x 10 mm
(iv) Improper level of briquette placement or the stretched thread of the specimen touching the
top or bottom surface of the water bath during the test
(v) Rate of pulling
(vi) Period of cooling

Increase in minimum cross section of 10 sq mm and increase in test temperature would record
increased ductility value.

Applications of Ductility Test

A certain minimum ductility value is considered essential for a bitumen binder for satisfactory
pavement performance. This is because of the temperature changes in the bituminous mixes
and the repeated deformations that occur in flexible pavements due to the traffic loads. If the
bitumen has low ductility value, the bituminous pavement may crack, especially in cold weather.
The ductility values of bitumen vary from 5 to over 100. Several agencies have specified the
minimum ductility values for various types of bituminous pavement. Often a minimum ductility
value of 50 or 75 cm is specified for bituminous construction.
The ductility value is determined on residue from thin film oven tests and the
requirements for paving bitumen as per BIS are as follows:
 Property VG 10 VG 20 VG 30 VG 40 Method of
Test Ref. No

Ductility at 25oC, cm min. 75 50 40 25 IS:1208 - 1978

after thin film oven test
VG is Viscosity Grading

It is to be noted that as per the current specifications for paving bitumen, the ductility
requirements are to be conducted on samples obtained after thin film oven test and not on
bitumen samples obtained from the refinery directly.

SELECTED REFERENCES

1. Bureau of Indian Standards, IS: 1208 -1978, Method for Testing Tar and Bituminous
Materials: Determination of Ductility (First Revision)
2. Bureau of Indian Standards, IS-73-2006, Indian Standard Paving Bitumen - Specification
(Third Revision)
3. Indian Roads Congress, Guidelines on the Use of Polymer and Rubber Modified Bitumen
in Road Construction,(First Revision), IRC : SP : 53 – 2002
4. Shell Butumen, Shell Bitumen Hand Book, (Fifth Edition), Thomas Telford Publishing,
London
5. Road Research Laboratory, Bituminous Materials in Road Construction, H.M.S.O., London.

QUESTIONS

1. Explain ductility of bitumen and its significance.

2. How is ductility value expressed ?
3. Outline the ductility test procedure.
4. What is the specified temperature for conducting the ductility tests?
5. What is the minimum area of cross section of the ductility specimen ?
6. What are the precautions to be taken while finding the ductility value ?
7. What are the factors affecting the ductility test results ?
8. What are the objectives of conducting elastic recovery test ?
9. How elastic recovery value is expressed?
10. What are the applications of elastic recovery test?
11. What are the desirable values of elastic recovery for different types of modified binders?
 OBSERVATION SHEET

Table Results of Ductility Test

(i) Grade of bitumen : =

(ii) Pouring temperature, ºC =
(iii) Test temperature ºC =
(iv) Periods of cooling, minutes,
(a) in air =
(b) in water bath before trimming =
(c) in water bath after trimming =

Sl No Briquette number
Test property Mean value
(i) (ii) (iii)
1 Ductility value (cm)
2 Repeatability percent
3 Reproducibility percent

Remarks :
Softening Point Test

INTRODUCTION

Bitumen does not suddenly change from solid to liquid state, but as the temperature
increases, it gradually becomes softer until it flows readily. All semi-solid state bitumen grades
need sufficient fluidity before they are used for application with the aggregate mix. For this
purpose bitumen is sometimes cut back with a solvent like kerosene. The common procedure
however is to liquefy the bitumen by heating. The softening point is the temperature at which the
substance attains particular degree of softening under specified condition of test. For bitumen, it
is usually determined by ring and Ball test. A brass ring containing the test sample of bitumen is
suspended in liquid like water or glycerine at a given temperature. A steel ball is placed upon the
bitumen and liquid medium is then heated at a specified rate. The temperature at which the
softened bitumen touches the metal plate placed at a specified distance below the ring is
recorded as the softening point of a particular bitumen. The apparatus and test procedure are
standardized by BIS. It is obvious that harder grades of bitumen possess higher softening point
than softer grades. The concept of determining the softening point by ring and ball apparatus is
shown in Figure 5.

Fig. 5 Softening Point Test Concept

Apparatus
It consists of Ring and Ball apparatus.
(a) Steel Balls : Two steel balls, each of diameter of 9.5 mm and weight 2.5 g ± 0.05 g.
(b) Brass Rings : Two rings of the following dimensions :
Depth 6.4 mm, inside diameter at top 17.5 mm, inside diameter at bottom 15.9,
outside diameter 20.6 mm
(c) Support : The metallic support is used for placing pairs of rings.
The upper surface of the rings is adjusted to be 50 mm below the surface or water or liquid
contained in the bath. A distance of 25mm between the bottom of the rings and top surface of the
bottom plate of support is provided. It has a housing for a suitable thermometer.

(d) Bath and stirrer : A heat resistant glass container of 85mm diameter and 120mm depth is
used. Bath liquid is water for material having softening point blow 80ºC and glycerin for materials
having softening point above 80ºC. Mechanical stirrer is used for ensuring uniform heat
distribution at all times throughout the bath.
Procedure
Sample material is heated to the temperature between 75 and 100ºC above the approximate
softening point until it is completely fluid and is poured in heated rings placed on a metal plate.
To avoid sticking of the bitumen to metal plate, coating is done to this with a solution of glycerine
and dextrine. After cooling the rings in air for 30 minutes, the excess bitumen is trimmed and
rings are placed in the support as discussed in item (c) above. At this time the temperature of
distilled water is kept at 5ºC. This temperature is maintained for 15 minutes after which the balls
are placed in position. The temperature of water is raised at uniform rate of 5ºC per minute with a
controlled heating unit, until the bitumen softens and touches the bottom plate by sinking of balls.
At least two observations are made. For material whose softening point is above 80ºC, glycerine
is used as a heating medium and the starting temperature is 35ºC instead of 5ºC.
Results
The temperature at the instant when each of the ball and sample touches the bottom plate of
support is recorded as softening value. The mean of duplicate determinations is noted. It is
essential that the mean value of the softening point (temperature) does not differ from individual
observations by more than the following limits.

Softening point Repeatability Reproducibility

40 to 60ºC 1.0ºC 5.5ºC
61ºC to 80ºC 1.5ºC 5.5ºC
81 to 100ºC 2.0ºC 5.5ºC

Discussion
As in the other physical tests on bitumen, it is essential that the specifications discussed
above are strictly observed. Particularly, any variation in the following point would affect the
result considerably:
(i) Quality and type of liquid in the bath
(ii) Weight of balls
(iii) Distance between bottom of ring and bottom base plate
(iv) Rate of heating
Impurity in water or glycerine has been observed to affect the result considerably. It is logical
to obtain lower softening point if the weight of ball is excessive. On the other hand, increase in
distance between the ring and bottom plate indicates higher value of the softening point.

Applications of Softening Point Test

Softening point is essentially the temperature at which the bituminous binders have an equal
viscosity. The softening point of the tar is therefore related to the equi-viscous temperature
(e.v.t). The softening point found by the ring and ball apparatus is approximately 20ºC lower than
the e.v.t.
 Softening point, thus gives an idea of the temperature at which the bituminous material attains
a certain viscosity. Bitumen with higher softening point may be preferred in warmer place.
Softening point is also sometimes used to specify hard bitumens and pitches.
As per the Bureau of Indian Standards, the requirements of softening point for paving bitumen
are as follows:

Property Paving Grades Method of

Test
VG 10 VG 20 VG 30 VG 40

Softening point 40 45 47 50 IS 1205 -

(R&B), oC, Min 1978

SELECTED REFERENCES

1. Bureau of Indian Standards, IS-1205-1978, Methods of Testing Tar and Bitumen:

Determination of Softening Point (First Revision)
2. Bureau of Indian Standards, IS-73-2006, Indian Standard Specification for Paving Bitumen
(Third Revision)
3. Road Research Laboratory, Bituminous Road Construction, H.M.S.O., London
4. Shell Bitumen, Shell Bitumen Hand Book, (Fifth Edition), Thomas Telford Publishing,
London

QUESTIONS

1. What is softening point ?

2. What does softening point of bituminous materials indicate ?
3. What are the applications of ring and ball tests results ?
5. What are the factors which affect the ring and ball tests results ?
6. Indicate the common range of softening point test values of the paving bitumen used in
bituminous mixes for road construction.
 OBSERVATION SHEET

Table Results of Softening Point Test

(i) Bitumen grade =

(ii) Approximate softening point =
(iii) Liquid used in the bath = water / glycerine
(iv) Period of air cooling, minutes =
(v) Period of cooling in water bath, minutes =
Rate of heating :

Time, Temperature, Time, Temperature,

minutes ºC minutes ºC
0 11
1 12
2 13
3 14
4 15
5 16
6 17
7 18
8 19
9 20
10

Test values observed :

Sample No. 1 Sample No. 2

Mean value,
Test property Ball No. 1 Ball No. 2
Softening point
(i) (ii) (i) (ii)
Temperature (ºC) at which
sample touches bottom plate
Repeatability

Reproducibility

Remarks :