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Specific Powder
Violent Resistivity:
1 MNG explosion- > 1 X1012 Ohm- 200 mJ
St 2H m
Resistive Exotherm 170°C
Specific Powder
Mild Resistivity:
2 MNMTI explosion > 1 X109 Ohm-m 4 mJ
St 1H Moderately Exotherm 149°C
Conductive
Endotherm 101°C
Exotherm 186°C
Endotherm 90°C
Residue after Distillation
7 NA NA NA
(Step-01)
Exotherm 182°C
Endotherm 164°C
Exotherm 190°C
Milled Tebu
その他 1.2mJ
DSC Analysis Fall Hammer Operating
Flash point
Peak Enthalpy Severity Test temperature
84°C 40 J/g
139°C 95 J/g
MNG having 5%
And 10% N.A 50 deg C
Moisture Test is
negative
205°C 997 J/g High
Negative NA 60 deg C
215°C 2228 J/g High
NA NA NA Negative NA 40 deg C
112°C 18 J/g NA NA
60 deg C
80 degC
80 degC
257°C 89 J/g Low NA NA
60 deg C
110°C 13 J/g NA NA
60 deg C
223°C 332 J/g Medium NA NA
Residue sample is
thick & non stirrable.
NA NA NA NA So Flash Point analysis
is not possible
Negative NA 90 deg C
Negative NA 90 deg C
ARC取得品については、
「TMRAD at 24 hour」が熱
源温度よりも低いことを確
認してください。
ARCを取得し、「TMRAD at
24 hour」が熱源温度よりも
低いことを確認してくださ
い。
固体の引火点測定方法も存
在するため、データ取得を
検討ください。(ASTM
D3278-1982: Standard Test
Methods for Flash Point of
Liquids by Setaflash Close-d-
Cup Apparatus参照)
メタノールが存在しない、
あるいは開放作業が無いの
であれば引火点の評価不要
です。
過去の住化での試験(IMO
燃速試験)では、窒素雰囲
気(酸欠雰囲気)下にて反応
伝播性はないことが確認さ
れています。
気(酸欠雰囲気)下にて反応
伝播性はないことが確認さ
れています。
粉砕後の粒径を現状よりも
大きめに調製し、着火感度
を低く(MIEを大きく)できな
いか検討してください。
爆発放散設備の開口面積に
ついて、NFPA68を基に適切
か確認してください。
Reaction mass
STEP-01.
The material starts decomposing at 147.5 °C.
2. Overall Heat of Reation (ΔH) is 143.8 J/g.
3. Temperature for TMRAD 8 hours (Time for maximum rate under adiabatic codition at 8 hou
is approximately 130 °C.
4. Temperature for TMRAD 24 hours (Time for maximum rate under adiabatic codition at 24 h
is approximately 124 °C.
5. Maximum Pressure reached during exothermic decomposition is 28 bar.
6. At 30°C, Residual Pressure is 11 bar.
Reaction mass
STEP-02
1. The material starts decomposing at 166.5 °C.
2. Overall Heat of Reation (ΔH) is 645.7 J/g.
3. Temperature for TMRAD 8 hours (Time for maximum rate under adiabatic codition at 8 hou
is approximately 162 °C.
4. Temperature for TMRAD 24 hours (Time for maximum rate under adiabatic codition at 24 h
is approximately 156 °C.
5. Maximum Pressure reached during exothermic decomposition is 119 bar.
6. At 30°C, Residual Pressure is 21 bar.
Reaction mass
STEP-03
The material starts decomposing at 126.1 °C.
2. Overall Heat of Reation (ΔH) is 346.98 J/g.
3. Temperature for TMRAD 8 hours (Time for maximum rate under adiabatic codition at 8 hou
is approximately 105 °C.
4. Temperature for TMRAD 24 hours (Time for maximum rate under adiabatic codition at 24 h
is approximately 83 °C.
5. Maximum Pressure reached during exothermic decomposition is 47 bar.
6. At 30°C, Residual Pressure is 7 bar.
adiabatic codition at 8 hours)