452827447.

xlsx

Destilación mediante el metodo McCabe-Thiele Tabulación de Datos

F 25,000 Kg/Hora

Axis Title
by Mark Burns and James Sung
Department of Chemical Engineering at the University of Michigan 1.2 PM Comp más volatil 72
PM Comp menos volatil 86
1.0
Alimentación
D= 122 mol/hr 0.8 %Masa Comp más Volatil 0.4
Xd = 0.98 %Masa Comp menos Volatil 0.6
L= 304 mol/hr 0.6

0.4 Destilado
%Masa Comp más Volatil 0.95
R= 2.5 0.2 %Masa Comp menos Volatil 0.05
F= 307.66 mol/hr f= 1 0.0
E(ML) = 1 0.0 0.2 0.4 0.6 0.8 1.0 Residuo
Xf = 0.4 %Masa Comp más Volatil 0.08
Axis Title %Masa Comp menos Volatil 0.92

V= 426 mol/hr λ Promedio de la Mezcla 80 cal/mol

W= 186 mol/hr λ Vapor de agua Saturado 533.6 cal/mol
Xw = 0.02 Number of Stages Required 17

Caudal Másico de vapor de Agua en la Caldera 0 Kg/h Equilibrium Data Entry

Point No. X Y
0 0.000 0.000
1 0.017 0.039
2 0.130 0.261
3 0.258 0.456
4 0.411 0.632
5 0.581 0.777
6 0.780 0.900
7 1.000 1.000
8
9
10
11
12
13
14

Graphical Representation of Successive Substitution

Enriching Line
y = 0.714 x + 0.280
Distillate
121.78 mol/hr
0.98 Desired Xd Stripping Line
Tray x y
1 0.95593 0.98 y= 1.436 x + -0.009
2 0.91805 0.96281
3 0.85843 0.93575
4 0.76876 0.89317 q line
5 0.66550 0.82912 y= x+
6 0.55596 0.75536 x= 0.400
7 0.46414 0.67711
Feed 8 0.39336 0.61153
307.66 mol/hr 9 0.34512 0.55617 Intersection (q,enriching)
0.4 Xf 10 0.28474 0.48690 x= 0.400
11 0.22111 0.40019 y= 0.566
12 0.16096 0.30881
13 0.10999 0.22244
14 0.07286 0.14923
15 0.04582 0.09591
16 0.02612 0.05707
17 0.01251 0.02879
18 - done
19 - -
20 - -
Bottoms
185.88 mol/hr
Reflux Ratio 2.5 0.02 Desired Xw
f 1
E(ML) 1
# of Stages 17

Data Points - Only one decimal place used for the sake of clarity
x 45 Degree line Equilibrium line f line Stripping line Enriching line Stage Steps
0.0 0.0 0.0 0.0 0.0
0.0 0.0 0.0 0.0 0.0
0.1 0.1 0.3 0.0 0.0
0.3 0.3 0.5 0.0 0.0
0.4 0.4 0.6 0.0 0.0
0.6 0.6 0.8 0.0 0.0
0.8 0.8 0.9 0.0 0.0
1.0 1.0 1.0 0.0 0.0
0.0 0.0 0.0 0.0 0.1
0.0 0.0 0.0 0.0 0.1
0.0 0.0 0.0 0.0 0.1
0.0 0.0 0.0 0.1 0.1
0.0 0.0 0.0 0.1 0.1
0.0 0.0 0.0 0.1 0.1
0.0 0.0 0.0 0.1 0.2
0.4 0.6 0.2 0.2
0.4 0.4 0.2 0.3
0.4 0.6 0.2 0.3
0.0 0.0 0.2 0.4
0.4 0.6 0.3 0.4
1.0 1.0 0.3 0.5
0.3 0.5
0.3 0.6
0.4 0.6
0.4 0.6
0.5 0.6
0.5 0.7
0.6 0.7
0.6 0.8
0.7 0.8
0.7 0.8
0.8 0.8
0.8 0.9
0.9 0.9
0.9 0.9
0.9 0.9
0.9 1.0
1.0 1.0
1.0 1.0
1.0 1.0

Notation

(1) Color convention

Black line in plot denotes y=x line

Blue-colored values denote spreadsheet-calculated values
Blue line in plot denotes stage steps
Green line in plot denotes equilibrium line
Magenta line in plot denotes q line
Red line in plot denotes operating line
Yellow boxes denote required data entry

(2) Variable Descriptions

b_e Y-axis intersect of enriching line

b_q Y-axis intersect of q line
column_x Vector of x_i values
column_y Vector of y_i values
D Distillate flowrate
E_ML Murphree tray efficiency based on the liquid phase
equil_x_i Equilibrium x data point number i
equil_y_i Equilibrium y data point number i
F Feed flowrate
m_e Slope of enriching line
m_q1 Slope of q line if q is not equal to 1
m_q2 X-position of q line if q=1 (i.e., Xf)
m_s Slope of stripping line
plot_x_i Point number i for x-axis plotting
q Feed quality
R Reflux ratio
stage_number Stage number vector used to determine number of required stages
stages Number of stages required to achieve desired Xw
step_equil_i Equilibrium line point number i used for stage step plotting
step_op_i Operating line point number i used for stage step plotting
Xd Fraction of lower boiling component in distillate
Xf Fraction of lower boiling component in feed
x_i Mole fraction of lower boiling component in liquid leaving stage i
Xint_q_enrich X-intersect of q and enriching lines
Xw Fraction of lower boiling component in bottoms
y_i Mole fraction of lower boiling component in vapor leaving stage i
Yint_q_enrich Y-intersect of q and enriching lines
W Bottoms flowrate

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Se desea diseñar una columna de rectificación para separar 25.000kg/h de una mezcla
fin de obtener un producto de cabeza (destilado) con 95% de pentano y un product
porcentajes están en peso. Se utilizará una relación de reflujo externa de 5,5. El calor
tolueno, puede tomarse igual a 7675 cal/mol. El calor latente del vapor de agua saturad