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ABSTRACT: Brittleness is considered a key parameter for hydraulic fracturing initiation and propagation in low permeability rock,
like gas shale. Plasticity, which in general increases with reduced brittleness, plays an important role in assessment of the mud weight
window for borehole stability during drilling in shale. There is no unique definition of brittleness, rather a variety of index parameters
that can be obtained from laboratory or field data, and which do not necessarily represent a coherent picture. This is digested here by
analysis of rock mechanical test data mainly on high porosity, high clay content North Sea shale. Brittleness, defined by the amount of
linear strain as part of the total strain before failure, and as the stress drop relative to peak stress after failure, was found to decrease
with increasing stress level (as expected). Brittleness was also found to decrease with increasing temperature and with exposure to
brine containing KCl. Experiments furthermore demonstrate that pore pressure evolution contributes strongly to undrained plasticity,
whereas the drained shale response is largely brittle. In practical field situations, one needs to address the situation closely to find
which definition of brittleness that is the most appropriate.
1. INTRODUCTION
but also a common source rock. In oilfield language,
Brittleness is a common term used to describe how rocks terminology is sometimes sloppy, describing low
fail. The brittle regime is characterized by a stress drop permeability formations as shales even if they strictly
when the rock is deformed after failure (beyond peak should not be defined as such.
stress). It is well-known that most rocks deform in a
brittle manner at low confining stresses, and become There is also no unique definition of a brittleness
ductile above a certain stress level. Brittleness is thus parameter, as pointed out already more than 35 years ago
detrimental to ductility (plasticity), which implies that by Hucka and Das [1]. The aim of this paper is to
the material can be deformed with non-declining or even summarize practical indices of brittleness that exist,
increasing ability to carry load. Brittleness during derive some of them from laboratory data, discuss their
compression is often associated with dilatancy, while relevance, and see how they relate to the field
rocks compact volumetrically when they are in the applications mentioned above.
ductile regime.
Brittle vs. plastic behavior has a profound influence on 2. BRITTLENESS PARAMETERS
borehole stability during drilling in shale, and thus on Hucka and Das [1] listed a number of measurement
how the mud weight program should be designed for principles that could serve as brittleness indicators.
wells to facilitate efficient and safe drilling. It also These were based on the conceptual understanding of
impacts fracturing behavior in shales, be it during brittleness as associated with “rupture or fracture with
reinjection of e.g. cuttings in shale intervals, or when little or no plastic flow”, or as fracture formation
enabling gas production from gas shales where occurring at or only slightly beyond the yield stress.
additional fracturing is imperative to production.
Below is listed a few suggested brittleness indices,
These are applications that have motivated the study starting with a definition which relates brittleness to
presented here. Hence, our focus is on shale, which is
elastic (reversible) strain (εel) normalized by total strain
often defined on basis of clay mineral content, or on
grain size, or on fissility. Shale is a common cap rock,
at failure (εtot= εel+εpl), where εpl is plastic strain at In the field of geotechnical engineering, a definition
failure (as illustrated in Figure 1): based on the residual strength was introduced by Bishop
[2]:
ε el
B1 = (1) τ max − τ res
ε tot B5 =
τ max
The Figure implies that the transition from elasticity to (5)
plasticity is associated with a deviation from linearity. In Here τmax and τres are peak and residual shear strengths,
principle unload – reload cycles should be performed to respectively (see also Figure 1). Hajiabdolmajid and
identify the transition. Kaiser [3] suggested a strain dependent brittleness
parameter
εel εpl ε p −ε p
τmax B6 = f c
εp c
(6)
measured from the failure envelope at zero normal All these definitions require laboratory tests with rock
stress. cores. B7 may however be estimated from log data, if an
appropriate correlation between rock strength and log
Other brittleness parameters were based on impact and parameters can be found. Based on experiments with
indentation tests. Although the various techniques gave North Sea shales, Horsrud found the following empirical
widely different numbers, the data presented by Hucka relationship between unconfined strength and P-wave
and Das showed mutual consistency when the brittleness velocity [6]:
indices of two different rocks were compared [1].
C0 [ MPa ] = 0.77v P [km / s ]2.93 (10)
Rickman et al. [7] argue that the brittleness concept An essential question for practical use of brittleness is to
should combine Poisson’s ratio, which they claim reflect identify a representative definition for the field situation
the rock’s ability to fail, and Young’s modulus, which in question. This is a difficult question, but through
represents its ability to maintain a fracture. They suggest controlled laboratory experiments and numerical
an empirically based brittleness index, which increases simulations one may investigate the role of brittleness
with increasing Young’s modulus and decreases with and obtain practical guidelines.
decreasing Poisson’s ratio. They used the dynamic
Poisson’s ratio derived from P- and S-wave log data, and
3. BRITTLENESS FROM LABORATORY
used an empirical correlation to obtain a value for the
static Young’s modulus [7]. Their brittleness index may DATA
be written 3.1 Effect of confining pressure
1 Edyn [ Mpsi ] (0.8 − φ ) − 1 ν dyn − 0.4
=B8 ( + ) ⋅100 As stated in the Introduction, rocks are commonly found
2 8 −1 0.15 − 0.4 (11)
to be brittle at low confining pressures, with a transition
to ductile behavior as the confinement is increased. In
The dynamic Young’s modulus (Edyn) and Poisson’s order to quantify this in terms of brittleness parameters
defined in the previous Section, we have digested stress
ratio (νdyn) are well-known functions of P- and S-wave
vs. strain curves from a selection of Consolidated
velocities (or slownesses, when derived from log data)
Undrained (CU) triaxial tests performed in our
[8, 9]. The way B7 and B8 are defined, they do not
laboratory. The tested shales were mainly from the
normalize to 1 (or 100%) in case of perfect brittleness.
overburden above North Sea petroleum reservoirs. The
It is quite clear that the brittleness parameters B1 – B8 clay contents and the porosities of these shales (see
defined above will give different values for a given rock, Table 1) are typical for drilling problem wells, but are
in line with the observations of Hacka and Das [1]. We higher than for common commercial gas shales. For
do not know to what extent they will show equal trends example, Barnett shale has porosities in the range 3–
amongst different rocks, and the availability of data 10% and clay contents around 20-25%, while Woodford
limits the possibilities to answer this question in full. For shale has 15-25% porosity and 20– 40% clay [10]. We
instance, definitions B1 and B2 in principle require that a believe, however, that the methodology used and the
core sample is loaded and unloaded prior to failure, results shown are of relevance also for gas shale
which is very rarely (if ever) done in otherwise time- applications, and hope to be able to extend this analysis
consuming shale tests. Definitions B3 and B4 require to such cores.
multiple core tests, which also is a limiting factor.
Definitions B5 and B6 require characterization of post- Table 1: Geological age, depth, porosity (from water
failure behavior, which depends on stiffness and control content) and clay content (from XRD analysis) for the
of the loading machine. Using servo-controlled shales used in the current study.
hydraulic load frames operating in strain rate control,
reliable data may be obtained, but may not be Shale Age Depth Porosity Clay
comparable to similar data obtained in another [m] [%] content [%]
laboratory. Definition B8 and to some extent B7 are H Tertiary 1900 28-46 30-85
attractive because they can be derived from log data and S Cretaceous 2200 21 47
W Tertiary 2160 28 44
do not require core testing. However, these parameters
F Upper Jurassic 2630 10 75
need to be considered at best to be indirect indicators of
Q Tertiary 1870 34 56
brittleness. P Cretaceous - 19-26 40-60
Fundamentally, brittleness is stress dependent, with a The effect of confining pressure is demonstrated in
transition from brittle to ductile behavior occurring at Figure 2 and Figure 3, where B1 and B5, respectively,
sufficiently high stress. This means that tests at several are plotted vs. confining stress for 3 different shales. “H”
confining pressures are necessary for a complete denotes a Tertiary shale from ~1900 m depth that shows
characterization. Also, shale is anisotropic, often with a significant heterogeneity, with porosity ranging from 28
pronounced plane of weakness. Thus, brittleness is also to 46 %, and clay content varying from 30 to 85 %. “S”
likely to be directionally dependent. Below we will Shale is from the Cretaceous at approximately 2200 m
include these aspects when evaluating brittleness from depth, and has 21 % porosity and 47 % clay (no
internal data collected throughout 25 years of shale smectite). “W” Shale is Tertiary from 2160 m depth and
testing. has 28 % porosity and 44 % clay.
1 some cases no stress drop occurred after the peak stress
had been reached.
0,8
Brittleness Index B1 [-]
0
that B8 increases with stress. This does not imply that B8
0 5 10 15 may not be used to distinguish between brittleness of
Effective Confining Stress [MPa] different shales under in the same stress field. Notice
that the value of B8 across the Barnett shale varies
Figure 3: Brittleness index B5 vs. effective confining stress between 20 and 55 [7]; i.e. Barnett shale is as expected a
at failure from triaxial tests with 3 different North Sea lot more brittle than the clay rich F shale studied here.
shales, named H, S and W shale (see Table 1). Unfortunately reliable S-wave data were not available in
the old test data analysed here, so a wider comparison
B1 was obtained by analysis of the behavior during between field and shale core data could not be performed
undrained loading. No unloading was performed. The at this stage.
stress - strain curves were fitted to a function mimicking
the curve shapes seen in triaxial tests, with B1 as a fitting 20
parameter [11]. This means that the data are essentially
Brittleness Index B8 [%]
30
commonly used additive to drilling fluids, and as can be 25
seen from the Figure, a main effect is to enhance 20 Drained test
plasticity (for further analysis, see [12]). B1 was reduced 15 Undrained test
to 0.2, while B5 was almost unaffected and remained 10
close to 0.2. Physically, the effect of KCl is largely 5
caused by ionic exchange, with an associated shrinkage 0
of the shale framework, allowing for larger strain prior 0 5 10 15 20 25 30 35 40
Axial strain [millistrain]
to failure.
Figure 6: Triaxial phase of undrained and drained triaxial
test on Pierre outcrop shale drilled perpendicular to
bedding.
4. IMPACT OF BRITTLENESS ON BOREHOLE
One complicating factor here is anisotropy. Shales are STABILITY
always anisotropic, because of alignment of clay
minerals and lamination on the grain scale. Using the In the presence of a borehole, differential stresses
formalism of anisotropic elasticity, the drained response increase in the vicinity of the borehole wall. For a linear
can be derived from the undrained response according to elastic material, these stresses are at their maximum at
the borehole wall. If the mud weight is too low to
an effective stress ∆σ z =∆σ z − S ∆p f , where the
*
support the borehole, shear failure may be induced at the
coefficient S depends on Biot’s α and on the elastic borehole wall, potentially leading to borehole collapse.
anisotropy. S may be estimated from the undrained data, However, since shales are generally plastic, i.e. lacking
provided the pore pressure response is measured, and some amount of brittleness, the stresses at the borehole
that the drained stiffness is constant throughout a wall will to various degrees be shielded near the
significant part of the loading. Figure 7 shows this borehole wall. This may in its turn significantly increase
inversion from data on Pierre Shale loaded normal to the stability of the borehole, potentially having profound
bedding. The upper curve is the measured differential influence on the applied mud weight, and whether a well
stress vs. differential strain curve, while the lower curve is drillable or not.
is the computed drained response. It is intriguing that the A number of poro-elasto-plastic models exist, taking into
drained curve appears to show almost perfect brittleness. account the effect of plasticity to various degrees. Such
Similar results have been obtained from other shale tests models typically require numerous input parameters,
as well. If generally valid, this implies that the pore making them cumbersome to use in practice due to
pressure response is a major source of undrained plastic limited amounts of consistent input data. We have made
behavior. a borehole stability model for shales, which takes into
account plasticity in a sufficiently simplified manner to
allow for more easy calibration of the model [13]. In
addition to input of conventional elastic and rock
strength parameters, dedicated borehole geometry
(hollow cylinder) laboratory tests are performed on
shales in our rock mechanical laboratory to specifically
calibrate for plasticity effects. In cases where laboratory
data are absent, plasticity parameters are estimated from
in-house models generated from available laboratory
data on a number of shales.
To illustrate the effect of plasticity on borehole stability,
Figure 8 shows the predicted stable mud weight
window (MWW) for a vertical well penetrating a field
shale when plasticity is excluded. The minimum
required mud weight to assure borehole stability is 1.61
s.g. (about 32.5 MPa at the given depth) soon after
drilling when an oil based mud is employed. Figure 9
shows the corresponding widened, stable MWW when
plasticity as determined from laboratory hollow cylinder
tests is included. In this case, the minimum required mud
weight is 1.51 s.g. (about 30.4 MPa). In case of a
horizontal well, the stable MWW will narrow
significantly in a normal stress regime, in particular
when plasticity is excluded. This is illustrated in Figure
10 and Figure 11 for the same field shale. Without
plasticity, the stable MWW has almost vanished, and the
lower limit (1.89 s.g.) even exceeds the minimum
horizontal stress, potentially fracturing the well. Thus,
the horizontal well may be difficult to drill in practice if
Figure 7: Stress-strain curves from an undrained uniaxial judged from the linear elastic model only. On the other
compression test on Pierre Shale. Upper curve: Measured hand, when plasticity is included, Figure 11 shows that
differential stress versus differential strain. Lower curve: the stable MWW is wider, and with the lower stable mud
Estimated axial stress versus axial strain if the test were
run under drained conditions.
weight (1.80 s.g.), now being less than the minimum
horizontal stress.