UNCERTAINTY BUDGET

Contribution
Distribution
Uncertainty

Uncertainty

Uncertainty
Probability

Coefficient
Sensitivity
Sources of

Standard
Estimate

Limit
Verification
Parameters
Repeatability 17.00 NA Type A 5.38 1.00 5.38
Reproducibility 3.09 NA Type A 0.98 1.00 0.98
Environment 3.00 Type A 1.22 1.00 1.22
Sample
Sample Weight 0.10 Type B 0.06 1.00 0.06

Titration of
Ammonia
Burette 0.00 Type B 0.00 1.00 0.00
Pipette / Measuring Cylinder 0.004 Type B 0.00 1.00 0.00
Purity of HCl 0.50 Type B 0.29 1.00 0.29
Normality of
HCL
Purity of sodium bicarbonate 0.50 Type B 0.29 1.00 0.29
Volume of titrant 0.004 Type B 0.00 1.00 0.00
Temperature of titrant 3.00 Type B 1.73 1.00 1.73

Uncertainty 5.8
Raw Data
Repeatability

Casein Repeatability

Pinto Anjum Sridevi Arun Ganesh Rashmi Lolashree Spoorthi

Trial
1 94 95 93 98 98 98 95 93
2 97 98 96 93 97 98 96 95
3 93 96 98 95 96 95 95 94
4 96 95 96 97 97 98 93 97
5 93 94 98 93 96 97 97 97
6 97 98 93 98 98 98 95 93
7 93 96 94 95 94 97 95 96
8 97 93 95 95 97 94 97 98
9 94 94 95 97 96 96 95 97
10 93 98 94 93 94 95 97 98

Mean 94.7 95.7 95.2 95.4 96.3 96.6 95.5 95.8

Std DeV 1.82 1.82 1.81 2.018 1.41 1.5 1.2 1.9
Degrees
of 10 10 10 10 10 10 10 10
freedom

The Average of the Standard deviation is 1.7, this is multiplied with degree of freedom to get the pooled data 17
 Raw Data
Reproducibility
Casein Reproducibility

Pinto Anjum Sridevi Arun Ganesh Rashmi Lolashree Spoorthi

Trial
1 94 95 93 98 98 98 95 93
2 97 98 96 93 97 98 96 95
3 93 96 98 95 96 95 95 94
4 96 95 96 97 97 98 93 97
5 93 94 98 93 96 97 97 97
6 97 98 93 98 98 98 95 93
7 93 96 94 95 94 97 95 96
8 97 93 95 95 97 94 97 98
9 94 94 95 97 96 96 95 97
10 93 98 94 93 94 95 97 98
Mean 94.7 95.7 95.2 95.4 96.3 96.6 95.5 95.8
Std DeV 1.82 1.82 1.81 2.01 1.41 1.50 1.2 1.9
Degrees of
10 10 10 10 10 10 10 10
freedom

Reproducibility is calculated by the Square root of sum of mean / sum of degrees of freedom