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.6
or" J
(GPa)
E
/
/
/
B/
.3
G
CD
.2
.1
| i i i I $
100 s time
Fig. 1. C o m p r e s s i o n test o f an hourglass-shaped a l u m i n u m alloy 6061 s p e c i m e n . In a d d i t i o n t o t h e static loading
at a strain rate o f 1 × 10 -4 s-1 t h e s p e c i m e n is in r e s o n a n c e w i t h a d o u b l e r e s o n a t o r at b o t h ends, t h e r e b y subject-
ing it t o cyclic loading at 20 kHz. When the d y n a m i c loading is s w i t c h e d on at B, the m e a n stress m e a s u r e d
e x t e r n a l l y o n a load cell d r o p s t o C. A f t e r cessation o f i n s o n a t i o n at D the s p e c i m e n follows an elastic line t o E,
w h e r e it reaches the static s t r e s s - s t r a i n curve. A t F t h e e x p e r i m e n t is r e p e a t e d .
the specimen again follows an elastic line until location structure and thereby the plastic
it reaches at E the stress-strain curve that it flow properties, (c) merely consists in heating
would have followed in a purely static test the specimen or (d) in wire drawing is tri-
(shown as a broken line). At F the ultrasound bological and involves the sliding of the metal
is superimposed again, the stress level drops to against the horn. With the appreciable interest
300 MPa (point G), which lies above C exactly in ultrasonic testing that has arisen during the
the same a m o u n t that F lies above B. At H last few years, it might be expected that the
the ultrasound is again discontinued, the application of ultrasonic techniques to manu-
specimen follows an elastic line and, after facturing, especially to metal forming [2] or
having reached the static stress-strain curve at compaction processes [4], would attract in-
J, continues along it. It should be noted that terest as well. In order to assess potential
the mean stress level is reduced by approxi- application a better understanding of the
mately 40% from B to C and from F to G. physical principles involved is required first.
The question remains as to whether the ob- Quantitative investigations of the effect so
served effect (a) is trivial and consists merely far have been impeded by the fact that it is
in repeated unloading of the specimen, (b) is extremely difficult, even almost impossible,
a genuine fatigue effect that changes the dis- to determine the stress level inside the speci-
199
2. LOW A N D M E D I U M F R E Q U E N C I E S
o"
[ l--
[GPa)
.3
I '
100 s Time
1 2 3 4 5 6 Strain (%) ~ 9
(b)
Fig. 4. (a) Stress-time curve for an aluminum alloy 6061 specimen subjected to sinusoidal loading blocks of
N = 50 cycles at the indicated frequencies and amplitudes. After each loading block the elastic line is resumed.
(b) Stress-strain curve for the same specimen and the same test, The large plastic strains accumulated during the
first quarter-cycle of each loading should be noted.
m a x i m u m stress (9max reached during dynamic As can be seen more clearly in Fig. 4(b)
deformation follows the purely static stress- than in Fig. 4(a), oma~ is not reached im-
time curve, although it exceeds it slightly by mediately during the first few cycles of each
an a m o u n t equal to areas -- Ostatic (where loading block, but rather after a strain of
(/static is the static stress). During the block approximately 1% has been accumulated. This
loadings the stress follows 6 + Ao where ~ + transient of a few cycles starts, in fact, at the
Ao OmaX and 0 -- Ao = Omin (~ is the mean
= stress level that had been reached previously
stress and omin the minimum stress). After at the static strain rate e0. The results of tests
each block loading, a new elastic line starts at on rapidly solidified and compacted powder
and is followed up to the previously reached aluminum alloys 7090 and 7091 are shown in
stress level, at which the static curve is re- Fig. 5. The results are similar to those for
sumed. During the last loading block the aluminum alloy 6061.
specimen actually went into compression,
which could not be fully recorded.
The stress-strain curve of Fig. 4(b) shows
that the cycles within each loading block fol- 2.2. Medium frequencies
low elastic lines. The onsets of the dynamic The strain rate program of eqn. (2) was also
blocks are marked as before. Unlike the situa- run at frequencies v of 10 and 50 Hz but, be-
tion in the time-based chart, the remarkably cause of the decreased machine response at
large strain accumulated during the first cycle those frequencies, at slightly smaller ampli-
of each block is indicated by bars and is tudes. At these speeds the pen recorders could
clearly visible. The strain accumulated during only follow the mean stress and not the actual
the tension phase of the first few cycles corre- stress any more. The actual stress was mea-
sponds to the chosen amplitude A. During the sured on an oscilloscope. The behaviors of
unloading of the first few cycles the specimen both aluminum alloy and the rapidly solidi-
relaxes elastically to the previously reached fied powder aluminum alloys 7090 and 7091
static strains. are the same as at low frequencies.
0-~ "8
(GPa) !
.6
.4 /
tl) t~) t3) t~) t3) [07 t#) to) t';)
|/ /
I .. ..... I
1
I
2
|
3
i
4
I
5
I
6 7
I ~ i
S t r a i n (%)
i
10
111
Fig. 5. S t r e s s - s t r a i n curve for static plus s u p e r i m p o s e d d y n a m i c loading in sinusoidal blocks. As for Fig. 4(b) but
for rapidly solidified p o w d e r a l u m i n u m alloy 7090 and 7091.
202
1 2 3
Or
/m 7091
(GPa)
1 2 3 4 1 2 A
.4
6061
A 1 2 3 1 3 1 2 4 1 3 1 2 4
.1
1 2 3 4 5 Strain (%) 8 9
Fig. 6. Stress-strain curve for aluminum alloy 6061 and rapidly solidified powder aluminum alloys 7090 and
7091. The static strain rate is 1 × 10-4 S-I; ultrasonic strain oscillations of the indicated amplitudes in arbitrary
units are superimposed. The clip-on strain gauge can follow only the accumulating static strain; the load cell can
follow only the mean static stress.
n=4.3 x 1621/233
.05
.04 6061
d c~/o
.03
.02
.Ol
(a) I I I I I I I
10 10s 108 104 106 106 101
~ I l I I I I I
In(l+2 u #A/~o)
10
Ego
10~
10a
104
106
106
20 kHz \
( b ) lo ~
Fig. 8. L o g a r i t h m i c s t r e s s i n c r e a s e d u r i n g d y n a m i c s i n u s o i d a l l o a d i n g w i t h a m p l i t u d e A a n d f r e q u e n c y v s u p e r -
i m p o s e d o n a s t a t i c t e s t w i t h a s t r a i n r a t e e0 ( t h e s t r a i n r a t e s e n s i t i v i t y n o b t a i n e d f o r a l u m i n u m a l l o y is 1 / 2 3 0 ;
it s h o u l d be n o t e d t h a t t h e u l t r a s o n i c t e s t s lead t o s t r a i n r a t e s w h i c h are l a r g e r b y a f a c t o r o f 1 0 0 0 ) ; ( b ) t h e
d e c r e a s e in t h e m e a n s t r e s s : I, v = 0.5 Hz a n d p = 1 H z ; I , p = 10 H z a n d v = 50 Hz. T h i s f i g u r e a l l o w s t h e s t r e s s
i n c r e a s e s w h i c h are u n m e a s u r a b l e at t h o s e f r e q u e n c i e s t o be d e d u c e d f r o m t h e u l t r a s o n i c a l l y m e a s u r a b l e d e c r e a s e
in t h e m e a n stress.
205
.05 - -~ O + Ostatic - -
nOstatie nOstatie
d (Y/cY
.04
47rPnOstatic 2
As, on the left-hand side, 5o < Ostatic - -
.03 rt=3.9 x 10"--31/256 and, on the right-hand side, r / 2 -- 1
/
e x p ( 5 o / n O s t a t i c ) w e therefore have
7090,7091 /
.02
60 - - n l n { 2 ( O s t a t i c - - O)} + n
1 (9)
(/static n\E~o/
For any material the elastic modulus E, the
.01 static strain rate go and the strain rate sensi-
tivity n can be obtained in quasi-static tests.
//
If the stress ostatic before ultrasonic loading
i
and the mean stress level 0 with simultaneous
1'0 ,08 ultrasonic and static loading are measured,
ln(l* 2n'v~/~-.o} eqn. (9) provides the possibility of computing
Fig. 9. S a m e as f o r Fig. 8, b u t f o r r a p i d l y s o l i d i f i e d the stress level go + Ostatie t h a t is actually
and compacted aluminum alloys 7090 and 7091. reached.
Essentially the decrease in the externally
observable mean stress during ultrasonic at-
tenuation indicates only the elastic relaxation
Ed° ~I 4Au 1 of the specimen during the unloading cycles.
2((/m~ -- 5) = [~ + ~oo" (5) The reason for the stress decrease is the irre-
versibflity of plastic deformation: an increase
Figure 8(b) shows the required plot, where in the strain rate slightly increases the stress,
for convenience we used In(1 + 2~rAu/do) in- but the following decrease fully relaxes the
stead of In(1 + 4Av/go) on the abscissa. This specimen elastically to a much lower stress. On
corresponds to a shift of the curve by In(u/2) average, therefore, the stress appears to be
to the left. It can be seen that eqn. (5) is in- lower.
deed obeyed.
Equation (9), together with Fig. 8, allows
us to find the m a x i m u m stress developed
3. 3. Overshoot of ultrasonic frequencies during the ultrasonic test of Fig. 1. There the
For low frequencies, both the mean stress
stress decrease (/static - - ~ equals 0.4(/static.
level O and the overshoot
Moreover, (/static = 500 MPa = E/140 on the
(/max -- ~ : 5 0 -~- Ostatic - - ~ (6) assumption that E = 70 GPa. For a basic
strain rate eo of 1 × 10 -4 s-1 and an ultrasonic
are experimentally accessible. At ultrasonic
frequency v of 2 × 104 Hz, 8((/static - - O)P]
frequencies, only 5 can be measured, but the
Ei0 = 4 × 106 corresponding to a relative
actual stress and strain situation within the
stress increase do/(/of 0.07. It is concluded
elastic-plastic specimen is not k n o w n and
that during this test a m a x i m u m stress Oma,
therefore the strain amplitude A is also not
of approximately 1.07(/static was reached, in
known. Under the assumption t h a t there is
spite of the fact that only the low mean stress
no frequency dependence of the effects in-
of 0 . 6 O s t a t i c W a s observable.
volved, combination of eqns. (5) and (6) gives
for the ultrasonic tests, had no appreciable vibrations at elevated temperatures where
effect on the shape of the stress-strain curve. remarkable changes in the deformation re-
At room temperature for both aluminum sistance during powder compaction were
alloy and the rapidly solidified powder alumi- reported.
num alloys there is little hardening in any case (5) The above analysis has been carried out
and any recovery would be hardly noticeable. only for aluminum alloys. Experiments with
However, a kind of superdynamic recovery other materials, especially those with a differ-
during superimposed ultrasonic loadings at ent lattice structure, appear to be necessary.
higher temperatures, where normal dynamic
recovery becomes noticeable, could be en-
visaged. Dynamic recovery consists of the
softening of the dislocation movement. Ob- ACKNOWLEDGMENTS
viously, dislocation movement is increased
markedly by the ultrasonic fatigue super- H. O. K. Kirchner and W. K. Kromp are
imposed on the static tests. Whatever the pro- grateful for support by the Max Kade Foun-
cesses effecting dynamic recovery are, dation. The project was financed by the
whether they are pipe or volume diffusion, Defense Advanced Research Projects Agency.
they should be just as effective in response to
the additional cyclic dislocation movement.
In contradistinction to dynamic recovery pro-
duced by unidirectional deformation, this REFERENCES
effect might be called superdynamic recovery
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perature regions where dynamic recovery is Zink-Einkristallen unter Ultraschalleinwirkung,
Naturwissenschaften, 42 (1955) 556.
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