IINCH-POUND ]

blIL-A-3316C
20 October 1987
SUPERSEDING
NIL-A-3316B
29 A p r i l 1966
(See6.7)

NILITARY SPECIFICATION

ADHESIVES, FIRE-RESISTANT,
THERNAL INSULATION

T h i s s p e c i f i c a t i o n i s approved f o r u s e by a l l Departments and Agencies

of t h e DepartmentofDefense.

1. SCOPE

1.1 S c o p e T . h i s p e c i f i c a t i o nc o v e r sf i r e - r e s i s t a n at d h e s i v e sf o r
s e c u r i n g c l o t h and t a p e t o c e r t a i n t h e r m a l i n s u l a t i o n s and f o r s e c u r i n g t h e r m a l
insulationstometalsurfaces.

1 . 2 C l a s s i f i c a t i o n . The a d h e s i v e ss h a l lb e of t h ef o l l o w i n gc l a s s e s and
g r a d e s ,a ss p e c i f i e d (see 6 . 2 . 1 ) .

Class 1

Grade A - Pigmented w h i t e .
Grade B - Pigmented r e d ( s e a l e r c o a t i n g t o i d e n t i f y
asbestos-freesystem).

F o rb o n d i n gf i b r o u sg l a s sc l o t ht ou n f a c e df i b r o u sg l a s si n s u l a t i o n .
Forsealingtheedgesof, andbonding f i b r o u s g l a s s t a p e t o t h e
j o i n t s o ff i b r o u sg l a s sb o a r d .
Forbondinglaggingclothtothermalinsulation.

Class 2

Grade A - Pigmented w h i t e .

Forattachingfibrousglassinsulationtometalsurfaces.

B e n e f i c i a l comments (recommendations,additions,deletions)and any p e r t i n e n t

d a t a which may be of use in improving this document should be addressed to:
Commander, NavalSeaSystems Command, SEA 5523, Departmentof t h e Navy,
Washington, DC 20362-5101by u s i n g t h e s e l f - a d d r e s s e d S t a n d a r d i z a t i o n Document
Improvement Proposal (DD Form 1426) appearing a t t h e endof t h i s document

a L O r by letter*
AMSC N/A FSC 8040
DISTRIBUTION STATEMENT A I
Approved f o r p u b l i c r e l e a s e ; d i s t r i.b u t i o n u n l i m i t e d

T H I S DOCUMENT CONTAINS PAGES.

\
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Class 3

Grade A - Pigmented white.

For attaching cork and fibrous glass insulation board to metal

surf aces.

2. APPLICABLE DOCUMENTS

2.1 Government documents.

2.1.1 Specifications and standards. The following specifications and

standards form a part of this specification to the extent specified herein.
Unless otherwise specified, the issues of these documents shall be those
in the issue of the Department of Defense Index of Specifications and
(DoDISS) and the supplement thereto, cited in the solicitation.

SPECIFICATIONS

FEDERAL
PPP-C-96 - Cans, Pletal, 28 Gage and Lighter.
PPP-P-704 - Pails, Metal: (Shipping, Steel, 1 Through 12
.
Ga 1lons)

MILITARY
MIL-1-742 - Insulation Board, Thermal, Fibrous Glass.
MIL-C-20079 - Cloth, Glass; Tape, Textile Glass; and Thread,
Glass.
MIL-1-22023 - Insulation Felt, Thermal and Sound Absorbing Felt,
Fibrous Glass, Flexible.
DOD-E-24607 - Enamel, Interior, Nonflaming (Dry), Chlorinated
Alkyd Resin, Semigloss. (Metric)

STANDARDS

FEDERAL
FED-STD-141 - Paint, Varnish, Lacquer and Related Materials;
Methods of Inspection, Sampling and Testing.
FED-STD-313 - Material Safety Data Sheets Preparation and the
Submission of.
FED-STD-595 - Colors.

MILITARY
MIL-STD-105 - Sampling Procedures and Tables for Inspection b
Attributes.
MIL-STD-129 - Marking for Shipment and Storage.

2.1.2 Other Government publication. The following other Government

publication forms a part of this specification to the extent specified
Unless otherwise specified, the issues shall be those in effect on of the
the solicitation.

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 MIL-A-331bC 80 m 77777Ob 007b872 7 W

NIL-A-3316C

DEPARTMENT OF LABOR
Code of Federal Regulations, Title 29
Part 1910, Occupational Safety and Health Standards

(Application for copies should be addressed

to the Superintendent of Docu
ments, U.S. Government Printing Office, Washington,
DC 20402.)

(Copies of specifications, standards, and publications required by con-

tractors in connection with specific acquisition functions should be obtained
from the contracting activity or as directed by the contracting activity.)

2.2 Other publications. The following documents form a part of this speci-
fication to the extent specified herein. Unless otherwise specified, the issues
4 of the documents which are DoD adopted shall be those listed in the issue of the
DoDISS specified in the solicitation. Unless otherwise specified, the issues of
documents not listed in the DoDISS shall be the issue of the nongovernment docu
ments which is current on the date of the solicitation.

AMERICAN SOCIETY FOR TESTING AND MATERIALS (AST)í)

C 640 - Standard Specification for Corkboard and Cork Pipe
Thermal Insulation.
D 92 - Standard Test Method for Flash and Fire Points by
Cleveland Open Cup. (DoD adopted)
D 217 - Standard Test Methods for Cone Penetration of Lubricating
Grease. (DoD adopted)
D 562 - Standard Test Method for Consistency of Paints Using the
Stormer Viscometer. (DoD adopted)
D 903 - Standard Test Method for Peel or Stripping Strength of
Adhesive Bonds. (DoD adopted)
D 1475 - Standard Test Method for Density of Paint, Varnish,
Lacquer, and Related Products. (DoD adopted)
D 2196 - Standard Test Methods for Rheological Properties Non-
of
Newtonian Materials by Rotational (Brookfield) Visco-
meter. (DoD adopted)
D 2486 - Standard Test Method for Scrub Resistance of Interior
Latex Flat Wall Paints.
D 3951 - Standard Practice for Commercial Packaging.
(DoD adopted)

(Application for copies should be addressed to the American Society for

PA 19103.)
Testing and Materials, 1916 Race Street, Philadelphia,

TECHNICAL ASSOCIATION OF TKE PULP AND PAPER INDUSTRY (TAPPI)

T 803 - Puncture and Stiffness Test of Container Board.
(Application for copies should be addressed
to the Technical Association of
the Pulp and Paper Industry, Technology Park/Atlanta, P.O. Box 105113, Atlanta,
GA 30348.)

UNIFORM CLASSIFICATION COMMITTEE AGENT

Uniform Freight Classification Ratings, Rules and Regulations

a (Application for copies should be addressed to the Uniform Classification

Committee Agent , Tariff Publication Officer, Room 1106, 222 South Riverside
Plaza, Chicago,IL 60606.)

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 NIL-A-3316C

INC., AGENT
NATIONAL WOTOR FREIGHT TRAFFIC ASSOCIATION,
National Motor Freight Classification

(Application for copies should be addressed to the National Motor Freig

Traffic Association, Inc.,ATA TRAFFIC Dept., 2200Mill Road, Alexandria,VA
22314.)

(Nongovernment standards and other publications are normally available

from the organizations which prepare or which distribute the documents. Thes
documents also may be available in or through libraries or other information
services.)

2.3 Order of precedence. In the event of a conflict between the text of

this specification and the references cited herein (except for associated
detail specifications, specification sheets NS
or standards), the text of this
specification shall take precedence. Nothing in this Specification, however,
shall supersede applicable laws and regulations unless a specific exemption
has been obtained.

3. REQUIREMENTS

3.1 Qualification. The adhesives furnished under this specification shall

be products which are authorized by the qualifying activity for listing on
applicable qualified products list at the time set for opening of bids 4.2 (see
and 6.3).

3.2 Material. The adhesives shall be effective for the purpose intended
without heating or the addition of other ingredients. They shall be free of a
ingredients which may adversely affect the serviceability, ahave
deleterious
effect on thermal insulation and fibrous glass cloth, or cause corrosion of
bare steel in the adhesion tests or primed steel in service. Adhesives shall
not contain mercury or mercury compounds and shall be asbestos free. When
specified in the contract or order, a certificate
of compliance shall be
prepared (see 6.2.2).

3.3 Stability.

3.3.1 Storage stability. The adhesives shall meet the requirements

specified herein upon the completion of storage a period
for of 6 months in an
airtight container (see 4.4.2.1).

3.3.2 Freeze-thaw stability. The adhesive shall meet the requirements

specified herein (see4.4.4through 4.4.13) upon returning to room temperature
after subjection toa temperature of 16 degrees Fahrenheit('F) for 16 hours
(see 4.4.2.2).

3.4 Toxicity and irritancy. The material shall haveno adverse effect on
the health of personnel when used for its intended purposes. Questions perti
nent to this effect shall be referred by the contracting activity to the
Medical Command (NAVNEDCOM) who will act as an advisor to the contracting
activity (see 4.1.2).

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3.5 F l a s hp o i n t .

a 3 . 5 . 1 Class 1 a d h e s i v e T
doesnotexhibit a flash point.
. h i sm a t e r i a l i s non-flammableand,assuch,

3 . 5 . 2 C l a s s e s 2 and 3 a d h e s i v e s . The f l a s hp o i n to ft h ea d h e s i v e ss h a l l
behigherthan 80°F ( s e e 4 . 4 . 4 ) .

3.6 Consistency.

3 . 6 . 1 C l a s s 1 a d h e s i v e . The consistencyoftheadhesive a t 80°F, a f t e r

it has been s t i r r e d m o d e r a t e l y by hand, s h a l l be s u i t a b l e f o r b o t h b r u s h and
hand a p p l i c a t i o n t o t h e s u r f a c e o f f a c e d and u n f a c e d f i b r o u s g l a s s i n s u l a t i o n
J boardconforming t o MIL-1-742 and t o t h e s u r f a c e of f i b r o u s g l a s s c l o t h con-
forming t o t y p e I , c l a s s 2 of MIL-C-20079 ( s e e 4 . 4 . 5 . 1 ) . The c o n s i s t e n c y of
theadhesiveshallbenotlessthan 50,000 nor more t h a n 150;OOO c e n t i p o i s e
(cP) u n i t s( s e e 4 . 4 . 5 . 1 ) .

3 . 6 . 2 C l a s s 2 a d h e s i v e . The c o n s i s t e n c y of t h ea d h e s i v es h a l lb en o t
l e s s t h a n 9 0 nor more t h a n 130 Krebs u n i t s ( s e e 4 . 4 . 5 . 2 ) .

3 . 6 . 3 Class 3 a d h e s i v e . The c o n s i s t e n c y of t h ea d h e s i v es h a l lb es u c ha s
t o allow a cone p e n e t r a t i o n a v e r a g e of n o t l e s s t h a n 25 nor more t h a n 35 milli-
meters (mm) ( s e e 4 . 4 . 5 . 3 ) .

3.7 Coverage and f i n i s h e dw e i g h t( c l a s s 1 a d h e s i v eo n l y ) . The coverage

o b t a i n e d from t h e a d h e s i v e i n p r o d u c i n g a s a t i s f a c t o r y c o v e r i n g s h a l l be not
e l e s s t h a n 30 s q u a r ef e e tp e rg a l l o nf o re a c hs p e c i m e n( s e e
f i n i s h e d w e i g h t of t h e c o v e r i n g f o r e a c h s p e c i m e n s h a l l b e n o t
o u n c e sp e rs q u a r ef o o to fa p p l i c a t i o n .
4 . 4 . 6 ) . The
more t h a n 5 . 3 5

3.8 Adhesive s t r e n g t h .

3 . 8 . 1 S t r e n g t hb e f o r ed r y i n g( c l a s s 1 a d h e s i v eo n l y ) . The s t r e n g t h of
the adhesive before drying shall be sufficient to prevent fibrous glass cloth
from peeling awaymore t h a n 1 inch a t any p o i n t from t h e f a c e d and unfaced
s u r f a c e s of v e r t i c a l l y mounted f i b r o u s g l a s s i n s u l a t i o n b o a r d andfrom t h e
lower(faced and u n f a c e d ) s u r f a c e s o f h o r i z o n t a l l y mounted f i b r o u s g l a s s
insulationboard(see 4.4.7.1).

3.8.2 D r y i n gt i m ea n ds t r i p p i n gs t r e n g t h .

3.8.2.1 C l a s s 1 adhesiveonly. The a d h e s i v es h a l ld r yt ot o u c hw i t h i n a

p e r i o d of 48 hours, and s h a l l have an average adhesive strength of not less
t h a n 3 pounds ( s e e 4 . 4 . 7 . 2 . 1 ) .

3.8.2.2 C l a s s e s 2 and 3 a d h e s i v e . Specimens s h a l l haveanadhesive

s t r e n g t h of n o t less t h a n 300 grams ( s e e 4 . 4 . 7 . 2 . 2 ) .

3 . 8 . 3 T e n s i l ea d h e s i v es t r e n g t h( c l a s s 3 a d h e s i v eo n l y ) . The adhesive
s t r e n g t h s h a l l benot less t h a n :

e (a)
(b)
(c)
125 pounds when t e s t e d as s p e c i f i e d i n 4 . 4 . 7 . 3 . 2 .
100 pounds when t e s t e d as s p e c i f i e d i n 4 . 4 . 7 . 3 . 3 .
50 pounds when t e s t e d a s s p e c i f i e d i n 4.4.7.3.4.

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 MIL-A-3316C

The adhesive shall be considered as conforming t o t h e s t r e n g t h r e q u i r e m e n t s when

failure occurs in the cork at
a d h e s i v e ,e x c e p tt h a tf a i l u r ea t
a s t r e n g t h lower t h a n t h a t s p e c i f i e d f o r t h e
less t h a n 50 pounds s h a l l r e s u l t i n a retest O
usingcorkselectedforgreaterstrength.

3.9
Color.

3 . 9 . 1C l a s s 1, grade A a d h e s i v e . The a d h e s i v es h a l lb ew h i t ei nc o l o r
(see 4.4.8).

3.9.2Class 1, grade B adhesive. The a d h e s i v es h a l l match r e dn o , 31158

of FED-STD-595 ( s e e 4 . 4 . 8 ) .

3 . 1 0F l e x i b i l i t y( a l lc l a s s e s ) . The adhesiveshallnotdevelopcracks
deep enough t o expose t h e s u b s t r a t e ( s e e 4 . 4 . 9 ) . Cracksoccurring a t e i t h e r
endand extending not more t h a n 1 / 4 i n c h s h a l l b e d i s r e g a r d e d .

3.11Washability(class 1 adhesiveonly). The adhesiveshallbewashable

to the extent that there shall be no definite break-through or detachment of
t h ea d h e s i v e( s e e4 . 4 . 1 0 ) .

3 . 1 2P a i n t a b i l i t y( c l a s s 1 a d h e s i v eo n l y ) . The a d h e s i v es h a l ln o tc a u s e
discolorationorbleedingthrough enamelconforming t o DOD-E-24607, s h a l l n o t
causecrackingorcrazingoftheenamel, and s h a l l b e c o m p a t i b l e w i t h t h e
enamel ( s e e4 . 4 . 1 1 ) .

3 . 1 3F i r er e s i s t a n c e .

3 . 1 3 . 1V e r t i c a ls p e c i m e nt e s t( a l lc l a s s e s ) .T h e r es h a l lb e no r e s i d u a l
a
flame or continuous burning of any specimen for more t h a n 3 seconds a f t e r t h e
t e s t flame i s e x t i n g u i s h e d ( s e e 4 . 4 . 1 2 . 1 ) .

3 . 1 3 . 2H o r i z o n t a lp a n e lt e s t .

3.13.2.1 Class 1 adhesive. When t h ea d h e s i v e i s t e s t e da ss p e c i f i e di n

4 . 4 . 1 2 . 2 . 1 and 4 . 4 . 1 2 . 2 . 3 , no s u s t a i n e d f l a m i n g s h a l l i s s u e fromany specimen.
Any flamewhichoccurs shallbelimitedtointermittentshortflames from t h e
a r e a d i r e c t l y exposed t o t h e t e s t flames. No flameor glow from t h e specimen
shall reach the angle frame at any p o i n t d u r i n g or a f t e r t h e t e s t p e r i o d .
Flaming s h a l l n o t c o n t i n u e more t h a n 2 minutes a f t e r t h e b u r n e r f l a m e is extin-
guished. A t no time d u r i n g t h e t e s t p e r i o d s h a l l any p i e c e of t h e specimen
h a v i n ga na r e ag r e a t e rt h a n 10 s q u a r e i n c h e s f a l l from t h e specimen.

3 . 1 3 . 2 . 2 Classes 2 and 3 a d h e s i v e s . The a d h e s i v e ss h a l lf l a m eo n l yi n t e r -

m i t t e n t l y when t e s t e d as s p e c i f i e d i n 4 . 4 . 1 2 . 2 . 2 and 4 . 4 . 1 2 . 2 . 3 , and t h e y s h a l l
n o ts m o l d e ra f t e rt h a t t e s t . When t h e i n s u l a t i o n b o a r d is p u l l e d o f f t h e s t e e l
plate, the separation shall occur within the fibrous glass insulation rather than
at the glueline.

3 . 1 4P u n c t u r er e s i s t a n c e( c l a s s 1 o n l y ) . The p u n c t u r er e s i s t a n c eo ft h e
finishedcoveringshallbenot less t h a n 800 inch-ouncesperinchoftear
(see 4.4.13).

O
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NIL-A-3316C

3.15 Workmanship. The a d h e s i v es h a l lb ef r e e from g r i t , lumps and s k i n s

0 ( s4
e e. 4 . 1 4 ) .

3 . 1 6U n i tc o n t a i n e rc o n t e n t . The u n i tc o n t a i n e rs h a l lc o n t a i nn o tl e s s
than the capacity specified in 5.1 (see 4.4.15).

3 . 1 7M a t e r i a ls a f e t yd a t as h e e t . The c o n t r a c t i n ga c t i v i t ys h a l lb ep r o -
v i d e d a m a t e r i a ls a f e t yd a t as h e e t (NSDS) a t t h e t i m e of c o n t r a c t award. The
WSDS i s Form OSHA-20 found i n and p a r t of FED-STD-313. The MSDS s h a l l b e
included with each shipment of the material covered by t h i s s p e c i f i c a t i o n ( s e e 6 . 5 ) .

4. QUALITY ASSURANCE PROVISIONS

*
4 . 1R e s p o n s i b i l i t yf o ri n s p e c t i o n .U n l e s so t h e r w i s es p e c i f i e di nt h e
contractorpurchaseorder,thecontractor i s responsiblefortheperformance
of a l l i n s p e c t i o nr e q u i r e m e n t sa ss p e c i f i e dh e r e i n .E x c e p ta so t h e r w i s es p e c i -
fied in the contract or purchase order, the contractor may u s e h i s own o r any
other facilities suitable for the performanceoftheinspectionrequirements
s p e c i f i e dh e r e i n ,u n l e s sd i s a p p r o v e d by t h e Government. The Government
reservestherighttoperform any of t h e i n s p e c t i o n s s e t f o r t h i n t h e s p e c i f i -
c a t i o n where such inspections are deemed n e c e s s a r y t o a s s u r e s u p p l i e s and
s e r v i c e s conform t o p r e s c r i b e d r e q u i r e m e n t s .

4.1.1Responsibilityforcompliance. A l l items must meet a l l require-

mentsof s e c t i o n s 3 and 5 . The i n s p e c t i o n set f o r t h i n t h i s s p e c i f i c a t i o n
s h a l l become a p a r t o f t h e c o n t r a c t o r ' s o v e r a l l i n s p e c t i o n system o r q u a l i t y
program. The absenceof any i n s p e c t i o nr e q u i r e m e n t si nt h es p e c i f i c a t i o ns h a l l
n o tr e l i e v et h ec o n t r a c t o r of t h er e s p o n s i b i l i t y of a s s u r i n gt h a t a l l p r o d u c t s
orsuppliessubmittedtothe Government f o r a c c e p t a n c e comply w i t h a l l r e q u i r e -
mentsof t h ec o n t r a c t . Sampling i n q u a l i t y conformancedoesnotauthorize
submissionof known d e f e c t i v e m a t e r i a l , e i t h e r i n d i c a t e d o r a c t u a l , n o r d o e s it
commit t h e Government t o a c c e p t a n c e of d e f e c t i v e m a t e r i a l .

4 . 1 . 2T o x i c o l o g i c a lf o r m u l a t i o n . The manufacturerofthe compound s h a l l

d i s c l o s e t h e f o r m u l a t i o n of h i s p r o d u c t t o t h e Commander NavalMedical Command
(MEDCOM-02) Washington, DC 20372 f o ra p p r o v a l( s e e3 . 4 ) . The d i s c l o s u r eo f
p r o p r i e t a r y i n f o r m a t i o n , which w i l l b e h e l d i n c o n f i d e n c e by t h e NavalMedical
Command, s h a l l i n c l u d e t h e name, formula, and approximatepercentage by weight
and volume o f e a c h i n g r e d i e n t i n t h e p r o d u c t ; t h e r e s u l t s o f any t o x i c o l o g i c a l
t e s t i n g of t h e p r o d u c t ; and s u c h o t h e r i n f o r m a t i o n a s may be needed t o permit
an accurate appraisal of any t o x i c i t y problem a s s o c i a t e d w i t h t h e h a n d l i n g ,
s t o r a g e ,a p p l i c a t i o n ,u s e ,d i s p o s a l ,o r combustionof t h em a t e r i a l .

4 . 2Q u a l i f i c a t i o n t e s t s . Q u a l i f i c a t i o nt e s t ss h a l lb ec o n d u c t e da t a
l a b o r a t o r ys a t i s f a c t o r yt ot h e NavalSeaSystems Command (NAVSEA). Qualifica-
t i o n tests s h a l l c o n s i s t of t h e t e s t s s p e c i f i e d i n 4 . 4 . 2 t h r o u g h 4 . 4 . 1 4 .

4 . 3Q u a l i t y conformance i n s p e c t i o n .

4 . 3 . 1I n s p e c t i o np r o c e d u r e s . Each l o t of a d h e s i v eo f f e r e df o ra c c e p t a n c e
s h a l l r e c e i v e a q u a l i t y conformance i n s p e c t i o n , which s h a l l c o n s i s t of t h e
examinations and t e s t s s p e c i f i e d i n t a b l e I . P r e - c o n d i t i o n i n gs h a l lb ea s
specified in 4.4.2.2, and t e s t c o n d i t i o n s s h a l l b e a s s p e c i f i e d i n 4 . 4 . 3 o r as
0 specified int h ae p p l i c a b l tee spt a r a g r a p h .

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4.3.2 Sampling.

4 . 3 . 2 . 1L o t . For t h ep u r p o s eo ft h es a m p l i n gp l a n ,a ni n s p e c t i o nl o t
shallconsistofalladhesiveprocessedin one b a t c h and o f f e r e d f o r d e l i v e r y
a t one time.

4 . 3 . 2 . 2S a m p l i n gf o rq u a l i t y of a d h e s i v e .S a m p l i n g ,e x c e p tf o rt h e
examinationof filledcontainers,shallconsist of t h r e e 1 - q u a r t s a m p l e u n i t s
from eachbatchtaken from t h e p o u r i n g s t a t i o n of thebatch-mixingtank. The
t a n ks h a l lb ea d e q u a t e l ys t i r r e d . To o b t a i na s s u r a n c eo fa d e q u a t es t i r r i n g ,
the1-quartcontainersshallbetakenasfollows:

No, 1 - A s emptyingof t h e t a n k b e g i n s .
No. 2 - As t h e t a n k i s h a l f empty.
No. 3 - A s t h e t a n k i s n e a r l y empty.

The t e s t s t o beperformed i n t h e s e 1 - q u a r t sample u n i t s s h a l l b e a s s p e c i f i e d

i n t a b l e I . Shouldany1-quartsampleunit f a i l i n any t e s t , the b a t c h s h a l l
be rejected.

4 . 3 . 2 . 3S a m p l i n gf o re x a m i n a t i o no ff i l l e dc o n t a i n e r s . A random s e l e c -
t i o n of f i l l e d c o n t a i n e r s s h a l l b e i n s p e c t e d i n a c c o r d a n c e w i t h MIL-STD-105
withanInspectionLevelof I w i t h an AQL of 2.5.Examination t o b ea ss p e c i -
fied in 4.4.15.

4 . 3 . 2 . 3 . 1R e j e c t e dl o t sf o re x a m i n a t i o n . A l o t which i s s u b m i t t e df o r
examinationafterbeingrejectedforfailure t o meet one o r more of t h e r e q u i r e -
ments s p e c i f i e d i n 3 . 1 6 o r 5 . 3 , o r a lot s u b m i t t e d i n p l a c e of a r e j e c t e d l o t ,
shall be given a tightenedinspectiontodetermineconformancewiththerequire-
mentswhich t h e o r i g i n a l l o t f a i l e d t o meet. Any l o t r e j e c t e d i n a c c o r d a n c e
withthesamplingplan may n e v e r t h e l e s s b e a c c e p t e d by examinationof all unit
containersinthelot andremovalof all defectives.

4 .T4e s t s .

4 . 4 . 1 Weight p e rg a l l o n . A no. 2 o n e - q u a r tc o n t a i n e rs h a l lb et h o r o u g h l y
mixed. The weightpergallon of i t s c o n t e n t ss h a l lb ed e t e r m i n e di na c c o r d a n c e
w i t h ASTM D 1475 f o r u s e i n t h e c a l c u l a t i o n s p e c i f i e d i n 4 . 4 . 1 5 .

4 . 4 .S2t a b i l i t y .

4 . 4 . 2 . 1S t o r a g es t a b i l i t y . The a d h e s i v es h a l lb es t o r e df o r a p e r i o d of
6 months i n an a i r t i g h t c o n t a i n e r . A t t h e endof t h i sp e r i o d ,t h ea d h e s i v e
shallbeinspected as s p e c i f i e d i n 4 . 4 . 2 t h r o u g h 4 . 4 . 1 4 .

4 . 4 . 2 . 2F r e e z e - t h a ws t a b i l i t y .P r i o rt ot h ep e r f o r m a n c e of any i n s p e c t i o n s
specifiedin4.4.4through4.4.14,thethree1-quartcontainersofthesample
shall be subjected to a t e m p e r a t u r e of 16 & 2'F f o r a period of 16 h o u r s , s h a l l
then be allowed to return to room t e m p e r a t u r e , and s h a l l b e mixed thoroughly a t
low s p e e d j u s t p r i o r t o p e r f o r m a n c e of t h e r e m a i n i n g - t e s t s andexaminations.

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4.4.3Temperature and humidity.Drying,curing,conditioning, and t e s t i n g

duringtheinspectionsspecifiedin4.4.4through4.4.12shallbeconductedat
a room temperatureof 80-f 10°F and a t a r e l a t i v e h u m i d i t y of 50 f 20 p e r c e n t .

4 . 4 . 4F l a s hp o i n t . The f l a s hp o i n to fc l a s s e s 2 and 3 a d h e s i v es h a l lb e
determinedinaccordancewith ASTM D 9 2 . Throughout t h e t e s t t h e a d h e s i v e s h a l l
be s t i r r e d s u f f i c i e n t l y t o p r e v e n t skimming o r s u r f a c e s e g r e g a t i o n .

4.4.5
Consistency.

4 . 4 . 5 . 1C l a s s 1 adhesive. The c o n s i s t e n c yo ft h ea d h e s i v es h a l lb e
determined through the use of a Brookfield viscometer in accordance with ASTM D
2196. The v i s c o m e t e rs h a l lb es u p p l i e dw i t h a h e l i p a t ha t t a c h m e n t and T-bar
s p i n d l e s( s i z e s A t h r u F) o r d i s c t y p e s p i n d l e s . The adhesivesampleshallbe
p e n e t r a t e dw i t ht h es p i n d l et o1 / 4i n c h . The v i s c o m e t e rs h a l lt h e nb et u r n e d
on t o a speedof2.5revolutionsperminute(r/min) t o allowthespindleto
r o t a t e . The h e l i p a t ha t t a c h m e n ts h a l lt h e nb et u r n e d on and d i a lr e a d i n g so f
e a c hr e v o l u t i o nt h r o u g ht h e downward and upward s t r o k e s s h a l l berecorded. The
h e l i p a t h s h a l l t h e n be turned off and t h e s p i n d l e s p e e d i n c r e a s e d t o 5 r/min t o
a l l o wt h es p i n d l et or o t a t e . The h e l i p a t ha t t a c h m e n ts h a l lb et u r n e d on a g a i n
and d i a l r e a d i n g s o f e a c h r e v o l u t i o n t h r o u g h t h e downward and upward s t r o k e s
s h a l l a g a i n b er e c o r d e d .D i a lr e a d i n g ss h a l lb em u l t i p l i e d by t h e a p p r o p r i a t e
f a c t o rt oo b t a i nt h ev i s c o s i t yr e a d i n g si n cP. A minimum of 10 v i s c o s i t y
readings shall then be averaged to obtain the adhesive viscosity.

4 . 4 . 5 . 2 Class 2 a d h e s i v e . The c o n s i s t e n c yo ft h ea d h e s i v es h a l lb ed e t e r -
mined in accordance with ASTPl D 562.

4 . 4 . 5 . 3C l a s s 3 adhesive.

4.4.5.3.1Apparatus. The a p p a r a t u su s e ds h a l lb ea sS p e c i f i e di n
ASTW D 2 1 7 , e x c e p t t h a t t h e t o t a l w e i g h t of t h e coneandrod s h a l l be 75 grams.

4.4.5.3.2Procedure. The opencup p o r t i o no ft h eg r e a s e - w o r k e rs h a l lb e

c o m p l e t e l yf i l l e dw i t ht h ew e l l - m i x e ds a m p l ea t a temperature of 77 & 1°F. A
straightedgeshallbe drawn a c r o s s t h e s u r f a c e o f t h e sample t o remove any
e x c e s sm a t e r i a l and t o p r e s e n t a smooth s u r f a c e . The a p p a r a t u ss h a l lb e
l e v e l e d and t h e p l u n g e r l o w e r e d u n t i l t h e t i p o f t h e p e n e t r o m e t e r cone j u s t
t o u c h e st h es u r f a c e of thesample. The s e a l s h a l l t h e n beadjusted so t h a t t h e
scale actuating device is in contact with the top of t h e r o d h o l d i n g t h e
penetrometercone and t h es c a l er e a d i n gr e c o r d e d . The p l u n g e rs h a l lb er e l e a s e d
suddenly and k e p t r e l e a s e d f o r 5 seconds. The s c a l e - a c t u a t i n gd e v i c es h a l lb e
moved u n t i l i t i s a g a i n i n c o n t a c t w i t h t h e t o p o f t h e r o d h o l d i n g t h e p e n e t r o -
metercone,and t h es c a l er e a d i n gr e c o r d e d . The p e n e t r a t i o n i s t h e d i f f e r e n c e
between t h e two r e a d i n g s .F i v e t e s t s s h a l l b e made and theaveragerecorded.
Tests s h a l l b e p e r f o r m e d w i t h s u f f i c i e n t r a p i d i t y t o g u a r d a g a i n s t n o n - u n i -
f o r m i t yd u et oe v a p o r a t i o no r skimming. The sample s h a l l besmoothed over
before each test.

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4 . 4 . 6 Coverage and f i n i s h( c l a s s 1 a d h e s i v eo n l y ) . A prime o ru n d e r l y i n g

a c o a to fa d h e s i v es h a l lb ea p p l i e d t o thefacingof
f i b r o u sg l a s si n s u l a t i o nb o a r d ,c o n f o r m i n gt ot y p e
f o o tp i e c eo ff i b r o u sc l o t hc o n f o r m i n gt ot y p e
a l-squarefootsectionof
I ofNIL-1-742. A l-square
I , c l a s s 2 of NIL-C-20079 s h a l l
thenbeimmediatelysuperimposed upon t h e primed s u r f a c e ofeachboardand
hand-troweledsmooth,eliminatingairpockets. An o v e r l y i n go rf i n i s hc o a to f
a d h e s i v es h a l lt h e nb eb r u s h e do v e rt h ec o t t o nc l o t h . Each specimen s h a l l b e
weighed b e f o r e and a f t e r a p p l i c a t i o n of t h ea d h e s i v e . The volume of t h e
adhesivecoatineachspecimenshallbecalculated by d i v i d i n g t h e d i f f e r e n c e
i n weight before and a f t e r a p p l i c a t i o n of t h e a d h e s i v e by t h e d e n s i t y o f t h e
a d h e s i v e . The a r e a of t h e c o a t e d s u r f a c e of t h e specimen s h a l l t h e n b e d i v i d e d
by t h a t volume t o o b t a i n t h e c o v e r a g e i n s q u a r e f e e t p e r g a l l o n .

4.4.7 Adhesive s t r e n g t h .

4 . 4 . 7 . 1S t r e n g t hb e f o r ed r y i n g( c l a s s 1 a d h e s i v eo n l y ) . A l - s q u a r ef o o t
s e c t i o n of t y p e I f i b r o u s g l a s s i n s u l a t i o n b o a r d and a l - s q u a r e f o o t s e c t i o n of
t y p e I I f i b r o u sg l a s si n s u l a t i o nb o a r d ,b o t hc o n f o r m i n gt o EIIL-1-742, s h a l l e a c h
b e mounted i n a v e r t i c a l p o s i t i o n . Two s e c t i o n s o f i n s u l a t i o n b o a r d i d e n t i c a l
t o t h e v e r t i c a l l y mounted b o a r d s s h a l l b e mounted i n a h o r i z o n t a l p o s i t i o n , so
t h a tt h ef a c i n go ft h et y p e I board i s down. A p r i m eo ru n d e r l y i n gc o a to f
adhesive shall then be applied at the same c o v e r a g e u s e d i n 4 . 4 . 6 t o o n e s i d e
of e a c h o f t h e v e r t i c a l l y mounted boardsand t o t h e lower s i d e ofeachof the
h o r i z o n t a l l y mounted b o a r d s . The a d h e s i v es h a l lb ea l l o w e dt o set f o r a p e r i o d
ending 5 m i n u t e sa f t e rt h ea p p l i c a t i o n of t h ea d h e s i v e was s t a r t e d . A f t e r t h e
endof t h a t p e r i o d and p r i o r t o t h e c o m p l e t i o n of an a d d i t i o n a l 5 - m i n u t e p e r i o d ,
a l - s q u a r ef o o tp i e c e of f i b r o u s g l a s s c l o t h conforming t o t y p e I , c l a s s 2 of
a MIL-C-20079 s h a l l besuperimposed upon t h e primed s u r f a c e of t h e specimenand
hand-troweledsmooth,eliminatingairpockets, andan o v e r l y i n g o r f i n i s h c o a t
o ft h ea d h e s i v es h a l lb eb r u s h e do v e rt h ef i b r o u sg l a s sc l o t h ,a tt h e same
coverageusedin4.4.6, and t h e f i b r o u s g l a s s c l o t h s h a l l bepeeledback 1 inch
fromeachof two o p p o s i t es i d e so ft h es p e c i m e n . A t t h e end of t h a t a d d i t i o n a l
5-minuteperiodthefibrousglassclothshallbeallowedtostandwithoutthe
a i d of s h o r i n g , p i n n i n g , o r o t h e r m e c h a n i c a l d e v i c e s and s h a l l beexamined for
s e p a r a t i o n from t h e i n s u l a t i o n b o a r d .

4.4.7.2Dryingtime and s t r i p p i n gs t r e n g t h .

4 . 4 . 7 . 2 . 1C l a s s 1 a d h e s i v e . The f a c i n g of a l - s q u a r ef o o ts e c t i o no f
t y p e I fibrousglassinsulationboardconformingto MIL-1-742 s h a l l b e c l e a n e d
w i t hs o l v e n t s( f o re x a m p l e , a m i x t u r eo fe q u a lp a r t so fx y l o l , MEK and a l c o h o l )
t o remove p o s s i b l ec o n t a m i n a n t s . The board,while s t i l l w e t ,s h a l lb e wiped
with a c l e a n , d r y c l o t h i n o r d e r t o a s s u r e removalof thecontaminants(drying
s h a l lt h e nb et h o r o u g h ) . A 12- by 6 - i n c h a r e a of t h e f a c i n g of t h e b o a r d s h a l l
b ec o a t e dw i t ht h ea d h e s i v et o anapproximatethicknessof1/32inch,leaving a
12- by 6 - i n c ha r e au n c o a t e d .A f t e rt h ea d h e s i v eh a sd r i e df o r 5 minutes, a
l-squarefootpiece of f i b r o u s g l a s s c l o t h conforming t o t y p e I , c l a s s 2 of
MIL-C-20079 s h a l l b e superimposedon t h e f a c i n g o f t h e b o a r d , and p r e s s e d and
t r o w e l e ds u f f i c i e n t l yt oe x t r u d et h ea d h e s i v et h r o u g ht h ei n t e r s t i c e s . The
adheredhalfoftheclothshallthenbegiven a f i n i s h c o a t i n g , which s h a l l be
s c r a p e do f f down t o t h e f a b r i c i n o r d e r t o remove excessadhesive. The
adhesive shall be inspected for drying to touch at the endof 48 h o u r s a f t e r
a p p l i c a t i o n . The a d h e s i v es h a l lb ev i s u a l l yi n s p e c t e df o rd r y n e s s .I ft h e
a adhesive i s n o td r y , an a d d i t i o n a l 1 2 h o u r sd r y i n gt i m es h a l lb ea l l o w e d . The

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 f a c i n g of t h e i n s u l a t i o n b o a r d s h a l l t h e n b e c a r e f u l l y s l i c e d away from t h e
f i b r o u sg l a s sf e l t . The bonded assemblyof t h ef i b r o u sg l a s sf a c i n g and
fibrousglassclothshallthen becuttoprovidefivestrips 2 incheswideand
12 incheslong. A s t r i p - a d h e s i o n t e s t ofeach s t r i ps h a l lb e conducted i n
accordancewith ASTM D 903. The f a c i n g of c e r t a i nb a t c h e so ff i b r o u sg l a s s
i n s u l a t i o n b o a r d may r e q u i r e a d d i t i o n a l t r e a t m e n t p r i o r t o t h e a p p l i c a t i o n of
theadhesiveinordertoachieve a t e s t ofadhesivestrength;thistreatment
shall be accomplished by priming with a t h i n brushed-on coat of a small portion
o ft h ea d h e s i v ew h i c hh a sb e e nt h i n n e ds u f f i c i e n t l yf o rt h i sp u r p o s e .T h i s
c o a t s h a l l be d r i e d f o r 72 h o u r s .

4 . 4 . 7 . 2 . 2C l a s s e s 2 and 3 a d h e s i v e s .S i xb a r e1 6 - g a u g ec o l d - r o l l e ds t e e l
p l a t e s , 5 by 10 i n c h e s , s h a l l b e c l e a n e d w i t h t h e s o l v e n t s p r a y o f method
2011.2of FED-STD-141, and s h a l l b e c o a t e d w i t h a d h e s i v e t o a p p r o x i m a t e l y 1 / 3 2 -
i n c h t h i c k n e s s andallowed t o s e t u n t i l t a c k y , b u t n o t l o n g e r t h a n 14 minutes.
S i x 3 - by 12-inchpiecesof bonded f i b r o u s g l a s s i n s u l a t i o n c o n f o r m i n g t o
MIL-1-22023 s h a l l t h e n b e a p p l i e d t o t h e c o a t e d s t e e l p l a t e s andallowed t o d r y
f o r 24 h o u r s . T h r e e o f t h e s e s p e c i m e n s s h a l l t h e n b e a g e d a t a temperatureof
194 k 5'F f o r 24 hours.Within 6 t o 24 h o u r s a f t e r removal from t h e oven, a l l
s i x specimens s h a l l be supported in a horizontal position with the bonded
f i b r o u s g l a s s s i d e down and a 300-gram w e i g h t a t t a c h e d t o t h e f r e e endof t h e
i n s u l a t i o n andsuspended f o r a p e r i o d of 10 m i n u t e s .I ff a i l u r eo c c u r si nt h e
g l a s s i n s u l a t i o n a r e t e s t s h a l l b e made w i t h s p e c i m e n s o f i n s u l a t i o n s e l e c t e d
for higher strength.

4 . 4 . 7 . 3T e n s i l ea d h e s i v es t r e n g t h( c l a s s 3 a d h e s i v eo n l y ) .

4 . 4 . 7 . 3 . 1P r e p a r a t i o n of s p e c i m e n s .E i g h t e e ns t e e ld i s k s , 4 i n c h e si n
diameter by 1 / 2 i n c h t h i c k , s h a l l b e d r i l l e d and t a p p e d i n t h e c e n t e r t o r e c e i v e
a 1 / 2 - i n c hb o l t . The t a p p e d h o l e s s h a l l n o t b e d r i l l e d e n t i r e l y t h r o u g h t h e
d i s k s . Each b o l t s h a l l b e d r i l l e d c r o s s w i s e a t t h e o u t e r end t o r e c e i v e a s t e e l
pinforattachingtothetesting machine. (The p i n a t oneend s h a l l be i n a
p l a n e 90 degrees t o t h e p l a n e of t h e p i n a t t h e o t h e r e n d , t o p r o v i d e freedom i n
b o t hp l a n e s . ) The a d h e s i v e s h a l l b e a p p l i e d t o t h e s u r f a c e o f t h e s t e e l d i s k s a t
anapproximatethickness of 1/16inch andallowed t o s e t f o r 5 minutes. The
coated steel d i s k s s h a l l t h e n b e a p p l i e d t o t h e two s i d e s of 1 - i n c h t h i c k by
4-inchdiameterpieces of corkinsulationboard,conformingto ASTM C 640, i n
such a manner t h a t t h e c o r k s h a l l besandwichedbetween t h e s t e e l d i s k s . Both
f a c e so ft h ec o r ks h a l l ,i fn e c e s s a r y ,h a v eb e e nf i r s ts a n d e d smooth, f l a t and
p a r a l l e l , and t h ed u s t removed. The ninespecimensthuspreparedshallbe
allowed t o d r y f o r 72 hoursunder a loadof 2 pounds p e r s q u a r e i n c h ( l b / i n 2 ) .

4 . 4 . 7 . 3 . 2P r o c e d u r e .T h r e eo ft h es p e c i m e n ss h a l lb ep u l l e dt or u p t u r ei n
a pendulum t y p e machine a t a normal r a t e of 2 i n c h e s p e r m i n u t e o r i n a load-cell
t y p e machine a t a r a t e of from 0 . 1t o0 . 2i n c hp e rm i n u t e , The r e s u l t s s h a l l b e
averaged.Afterremovalofthecork,the bonded s u r f a c e of t h e s t e e l s h a l l b e
examined f o r c o r r o s i o n .

4 . 4 . 7 . 3 . 3S a l tw a t e rt e s tp r o c e d u r e . .T h r e e of t h e specimens s h a l l besub-
merged i n s a l t w a t e r (5 p e r c e n t NaC1) f o r 2 h o u r s . Upon r e m o v a l ,t h e ys h a l l
immediatelybetestedasspecifiedin4.4.7.3.2.

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4 . 4 . 7 . 3 . 4 Oven t e s t p r o c e d u r e . The remainingthreespecimensshallbe

0 h e a t e di n an oven
specifiedin4.4.7.3.2,shallbe
a t 200 k 10°F f o r 2 h o u r s . The t e s tf o re a c hs p e c i m e n ,a s
completedwithin 3 minutes a f t e r removal from
t h e oven. Thebonded s u r f a c e of t h e s t e e l s h a l l beexamined f o rc o r r o s i o n .

4 . 4 . 8C o l o r( c l a s s 1 a d h e s i v e ) . The s p e c i m e n sp r e p a r e df o rt h et e s t s
specified in 4.4.7.1 shall be examined t o d e t e r m i n e t h e c o l o r o f t h e a d h e s i v e
when d r i e d . The a d h e s i v ec o l o rs h a l l meet t h er e q u i r e m e n t so f3 . 9 .

4 . 4 .F9l e x i b i l i t y .

4 . 4 . 9 . 1C l a s s 1 a d h e s i v e .F o rc l a s s 1 a d h e s i v e ,t h es p e c i m e ns h a l l be
preparedasspecifiedin4.4.7.2.1usingtheadheredhalfonly.

4 . 4 . 9 . 2C l a s s e s 2 and 3 a d h e s i v e s .F o rc l a s s e s 2 and 3 a d h e s i v e s ,t h e
specimens s h a l l b e p r e p a r e d on t i n p l a t e i n a c c o r d a n c e w i t h method 2012.2of
- FED-STD-141. A s i n g l ef i l mo fa d h e s i v e0 . 0 2 & 0 . 0 0 2i n c ht h i c ks h a l lt h e nb e
a p p l i e d t o the. t i n p l a t e p a n e l i n a c c o r d a n c e w i t h method2161 o r 2162 of
FED-STD-141.

4 . 4 . 9 . 3P r o c e d u r e . The coatedspecimen s h a l lb ea i rd r i e df o r 24 hours

and t h e n baked f o r 75 minutes a t 217 k 4OF i n a c i r c u l a t i n g a i r o v e n . The
coatedspecimen s h a l l t h e n b e c o n d i t i o n e d f o r 1 - 1 / 2 t o 2 hours a t 73 k 2OF a t a
r e l a t i v e h u m i d i t y of50 It: 5 p e r c e n t . The f l e x i b i l i t y t e s t s h a l lt h e nb ec o n -
ducted with the coated specimen using a 1.4-inch diameter mandrel in accordance
w i t h method 6221of FED-STD-141, e x c e p t t h a t t h e m a g n i f i c a t i o n and s p e c i a l
illumination specified therein for the examination of the coated specimen will
n obt er e q u i r e d . The a d h e s i v ef i l ms h a l b
le examined f o cr r a c k sd e e p enough t o
expose the substrate.

4 . 4 . 1 0W a s h a b i l i t y( c l a s s 1 a d h e s i v eo n l y ) . The a p p a r a t u s t o beusedfor
thewashabilitytestforclass 1 a d h e s i v e ss h a l lb ea sf o l l o w s :

(a) A w a s h a b i l i t y machine w i t hc o u n t e r and brushconforming t o

ASTM D 2486.
(b) A g l a s sp a n e l , 6 by 18 inches,conforming t o method 2021of
FED-STD-141.
(c) A f i l ma p p l i c a t o r ,w i t h a 0.020inchclearance,conformingto
method 2162 of FED-STD-141.
(d) A b a r of "Bon-Ami", o re q u a lt y p ea b r a s i v es o a p .
(e) Sample o fm a t e r i a lt ob et e s t e d .

4 . 4 . 1 0 . 1P r o c e d u r e . The g l a s sp a n e ls h a l lb ep r e p a r e d as s p e c i f i e di n
method 2021of FED-STD-141. A f i l m of m a t e r i a l , t o b e t e s t e d , s h a l l b e drawn
down u s i n g t h e 0 . 0 2 0 - i n c h f i l m a p p l i c a t o r . The f i l m s h a l l b e drawn down t h e
e n t i r e l e n g t h of t h e g l a s s p a n e l on t h e ground s i d e . The draw-down s h a l l be
3 . 5 i n c h e so r more i n w i d t h . The p a n e ls h a l lb ea l l o w e dt od r yf o r 6 days a t
. room temperature(approximately 75 f 5'F). The g l a s sp a n e ls h a l l beplaced on
t h e t a b l e of t h ew a s h a b i l i t ym a c h i n e . The b r u s hs h a l lb es o a k e di nw a t e rf o r
30 minutes. The b r u s hs h a l lb er u b b e dv i g o r o u s l yo v e rt h eb a ro f "Bon-Ami", o r
e q u a lt y p es o a pu n t i lt h eb r i s t l e sa r et h o r o u g h l ys a t u r a t e dw i t hs o a p . The
brush shall be placed into the machine r e c e p t a c l e and s h a l l b e a l i g n e d on t h e
coatedglasspanel so that the brush stroke is entirely within the coated area.
During t h et e s t ,t h ew a t e rs h a l l b ep e r m i t t e dt od r o po rr u ni n t ot h ep a t h of

13

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 thebrushattherateofabout 12 d r o p s p e r m i n u t e , o r j u s t s u f f i c i e n t t o k e e p
t h ep a n e lw e t . The machine s h a l l be s t a r t e d and r u nf o r 1000 d o u b l es t r o k e s .
The p a n e l s h a l l b e washed a t once i n w a t e r a t m o d e r a t e t e m p e r a t u r e , and O
inspectedforfilmwithinthemiddle 6 inchesofbrushtravelfordefinitebreaks,
wear o r detachmentof t h e f i l m down t o t h e g l a s s . A few s m a l lp i n p o i n ta r e a s
shall be disregarded.

4 . 4 . 1 1P a i n t a b i l i t y( c l a s s 1 a d h e s i v eo n l y ) . The a d h e s i v es h a l lb ea p p l i e d
tothefibrousglassclothfacing of a 12- by 12-inchspecimenoffibrousglass
insulationboardconforming t o t y p e I of MIL-1-742 andallowed t o s e t f o r 10
minutes. A s t r i p of f i b r o u sg l a s st a p ec o n f o r m i n gt ot y p e I I , c l a s s 1 of
MIL-C-20079, s h a l lt h e nb ea p p l i e dt ot h ea d h e s i v e - c o a t e ds p e c i m e n . Then a c o a t
ofadhesiveshallbeappliedoverthetape. The specimen s h a l l b e a l l o w e d t o a i r
d r yf o r 24 h o u r s . A c o a t of p a i n t conforming t o DOD-E-24607 s h a l l b ea p p l i e dt o , -
thefaceofthe specimen and allowed t o a i r d r y f o r 24 h o u r s , a f t e r which a second
coatof enamel s h a l l beapplied. The specimen s h a l l b e i n s p e c t e d a f t e r 24 and
48 h o u r s f o r s i g n s of b l e e d i n g and f o r d i s c o l o r a t i o n , c r a c k i n g o r c r a z i n g of t h e
paint.

4 . 4 . 1 2F i r er e s i s t a n c e .

4 . 4 . 1 2 . 1V e r t i c a l specimen t e s t . Three s t r i p s o ff i b r o u sg l a s st a p e , 6
incheslong and 2 incheswide,conforming t o t y p e I I , c l a s s I of NIL-C-20079
s h a l l becoated on b o t h s i d e s - w i t h t h e a d h e s i v e , t h e n drawn through two p o l i s h e d
metalrods(1/2- t o 1 - i n c hd i a m e t e r ) . The b a r s s h a l l be p a r a l l e l s o t h a t t h e
t a p e w i t h c o a t i n g on b o t h s i d e s when d r i e d s h a l l h a v e an o v e r a l l t h i c k n e s s o f
0.013inch. The c o a t e d s t r i p s s h a l l b e a i r - d r i e d f o r 24 hours and thenplaced
i n a f o r c e d - d r a f t oven f o r 20 hours a t 212 t o 221°F.Thesespecimens shall
then be removed from t h e ovenand, a f t e r n o t less than 1/4 hour, nor more t h a n
1/2 hour,eachinturnshallbesuspendedvertically from a clamp t h a t c o v e r s
t h eu p p e r1 / 2i n c h of t h e s t r i p , i n a d r a f t - f r e el o c a t i o n . A Meker b u r n e r ,
having a 30-mm d i a m e t e r g r i d , and s u p p l i e d w i t h n a t u r a l g a s of 1100 k 100
B r i t i s ht h e r m a lu n i t s( B t u )p e rc u b i cf o o t ,s h a l lh a v e i t s flameadjusted s o
t h a t i t s outerzone i s 1 - 1 / 2 incheshigh and i t s l i g h t b l u e i n n e r zone i s 1/16
i n c hh i g h . The temperatureoftheflameshallbemeasuredusing a type R o r S
thermocouple a t a p o i n t 1 - 1 / 4 k 1/32inches above t h e c e n t e r o f t h e g r i d and
s h a l l b e between 1300 and 1900'F. Flame adjustmentshallbeperformedin a
darkened area and s h a l l u t i l i z e a b l a c k o b j e c t b e h i n d t h e f l a m e i n o r d e r t o
enhanceobservation of t h e f l a m e h e i g h t . The b u r n e r s h a l l t h e n b e p l a c e d
d i r e c t l y below t h e specimen i n a p o s i t i o n s u c h t h a t i t s g r i d i s 1 i n c h below t h e
middleoftheloweredgeofthespecimen.After 5 s e c o n d s ,t h eb u r n e rs h a l lb e
e x t i n g u i s h e d and t h e l e n g t h o f t i m e t h a t t h e c o a t i n g c o n t i n u e s t o b u r n a f t e r t h e
e x t i n c t i o ns h a l lb en o t e d . The r e s u l t s o f t h e t h r e e specimens s h a l l beaveraged.

I 4 . 4 . 1 2 . 2H o r i z o n t a lp a n e l

4 . 4 . 1 2 . 2 . 1P r e p a r a t i o n
test.

ofspecimen,class 1 a d h e s i v e . The a d h e s i v es h a l l
beappliedtothefacing of a 30- by 30-by 1-inchspecimenoftype I fibrousglass
i n s u l a t i o n b o a r d and t o one s i d e of a 30- by 30- by 1 - i n c h specimen of t y p e I I
fibrousglassinsulationboardconformingto MIL-1-742 (thesespecimens may be
made upfrom more t h a n one p i e c e ) . Then a 30- by 3 0 - i n c h p i e c e o f f i b r o u s g l a s s
c l o t h conforming t o t y p e I , c l a s s 2 of MIL-C-ZOO79 s h a l l b e superimposedon t h e
primedsurfaceofeachofthespecimens andhandtroweledsmooth,eliminating and
removing a i rp o c k e t s ,u n t i lt h ea d h e s i v ee x t r u d e st h r o u g ht h ei n t e r s t i c e so ft h e

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 MIL-A-3316C

c l o t h . An o v e r l y i n g o r f i n i s h c o a t ofadhesiveshallthenbebrushedoverthe
c l o t h . A 36-by36- by 1 / 1 6 - i n c hs t e e lp l a t e ,s t i f f e n e da g a i n s ts a g g i n g ,s h a l l
be bonded t ot h eo p p o s i t es i d eo fe a c hs p e c i m e n . Then eachspecimen s h a l l be
dried to constant weight at a temperature recommendedby t h e a d h e s i v e manufac-
t u r e r a.s b e i n g n o n - i n j u r i o u s t o t h e p a r t i c u l a r a d h e s i v e u n d e r t e s t .

4 . 4 . 1 2 . 2 . 2P r e p a r a t i o no fs p e c i m e n ,c l a s s e s 2 and 3 a d h e s i v e s . The adhesive

s h a l l beappliedtotheunfacedsides and t o t h e edgesof two f i b r o u s g l a s s
i n s u l a t i o nb o a r d sc o n f o r m i n gt ot y p e I of MIL-1-742 andmeasuring 15 by30by 1
incheach. The two boardsshallthenbesecured by t h e a d h e s i v e t o a 36-by
36- by 1 / 1 6 - i n c h s t e e l p l a t e , s t i f f e n e d a g a i n s t s a g g i n g , so thattheboardsare
b u t t e d t o g e t h e r t o form a 30-squareinchspecimen,centered on t h e s t e e l p l a t e .
A p i e c eo fg l a s st a p e , 30 incheslong and 2 incheswide,conforming to type II,
W c l a s s 1 of MIL-C-20079, s h a l lb ea p p l i e do v e rt h e seam where t h e two boards
a r ej o i n e d ,b e i n g bonded t o t h e b o a r df a c i n g sw i t hc l a s s 1 a d h e s i v e . The s p e c i -
men s h a l lb ea l l o w e dt od r yf o r 24 h o u r s . Two c o a t so f enamelconforming to
DOD-E-24607 s h a l l b e b r u s h e d o v e r t h e g l a s s c l o t h f a c i n g of thespecimen,each
coatbeingallowedtodryfor 24 h o u r s .

4 . 4 . 1 2 . 2 . 3 Test procedure. Each specimen s h a l l be t e s t e ds e p a r a t e l y , i n

a room which i s f r e e from a i r c u r r e n t s . The specimen s h a l l b e p l a c e d i n a
horizontal position with the insulation downward and w i t h t h e s t e e l p l a t e s u p -
p o r t e d on t h e f l a t s u r f a c e by a 2 - by 2 - by 1 / 2 - i n c h s t e e l angleframehaving a
30-by 30-inchclearopening. A g a s - a i r b u r n e r of3/4- t o7 / 8 - i n c hd i a m e t e rs h a l l
beplacedverticallywith i t s t o p 24 inches below t h e c e n t e r o f t h e lower s u r -
faceofthespecimen. A thermocouple made of 1 / 8 - i n c hw i r e s andformed into a
3-inchhorizontalcoilshallbeplaced 1 i n c h below t h e c e n t e r o f t h e lower
0 s u r f a c e of t h e specimen. The w i r e ss h a l lb eb a r ef o r
from t h e j u n c t i o n . The t e s t s h a l l b e c o n d u c t e d
a d i s t a n c e of 2 inches
by d i r e c t i n g a flame from t h e
burneragainstthecenter of t h e lower s u r f a c e of t h e specimen f o r a p e r i o d of
40 m i n u t e s .D u r i n gt h et e s t ,t h et e m p e r a t u r e of t h et h e r m o c o u p l es h a l lb er e a d
and recorded a ti n t e r v a l sn o te x c e e d i n g 2 minutes. The f l a m es h a l lb er e g u l a t e d
togivetemperatureindicationsconformingtothetime-temperaturecurve shown
on f i g u r e 1. The flame s h a l l c o n t a c t t h e s p e c i m e nd u r i n gt h ee n t i r et e s tp e r i o d ;
anexception may be made f o r t h e f i r s t 5 minutes, i f r e q u i r e d f o r p r o p e r temp-
e r a t u r er e g u l a t i o n . A t no t i m e d u r i n g t h e t e s t s h a l l t h e f l a m e from t h eb u r n e r
contactthespecimenat any p o i n t which i s more t h a n 6 i n c h e s from t h e c e n t e r of
t h e specimen. The areaunderthetime-temperaturecurveobtained from t h e thermo-
couplereadingsshallbewithin 5 p e r c e n t of t h e a r e a u n d e r t h e c u r v e on f i g u r e 1.
During t h e 40-minute t e s t p e r i o d , t h e e x t e n t and d u r a t i o n o f f l a m i n g s h a l l b e
noted. A t t h e end of t h et e s tp e r i o d ,t h ef l a m es h a l lb ee x t i n g u i s h e d . The
specimen s h a l l t h e n b e examined t o d e t e r m i n e t h e f u r t h e r e x t e n t and d u r a t i o n of
flaming, andglowing o rs m o l d e r i n g .A f t e rt h e t e s t of e i t h e r t h e c l a s s 2 or
the class 3 adhesive, the insulation board shall be pulled off the steel plate,
and t h e s t e e l p l a t e s h a l l b e examined t o d e t e r m i n e w h e t h e r s e p a r a t i o n o c c u r r e d
within the insulation board or between t h e i n s u l a t i o n b o a r d and t h e s t e e l p l a t e .

4 . 4 . 1 3P u n c t u r er e s i s t a n c e .P u n c t u r er e s i s t a n c es h a l lb ed e t e r m i n e di n
accordancewith TAPP1 T 8 0 3 , e x c e p t t h e t e s t s p e c i m e n s h a l l b e p l a c e d , w i t h t h e
f i n i s h e dc o v e r i n gs u r f a c e down, between t h e clamping p l a t e s . B e f o r e e a c h t e s t
i s made, t h e l o o s e s l e e v e s h a l l b e p l a c e d a g a i n s t t h e b a s e of t h e p u n c t u r e p o i n t
and t h e p o i n t e r s e t a b o u t 1 inchabovetheexpectedreading. The pendulum s h a l l

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MIL-A-33LbC A O W 9999906 009b905 3 W ~~

MIL-A-3316C

be raised to the horizontal position and r e l e a s e d by p u s h i n g t h e l a t c h h a n d l e t o

the left. The r e a d i n g s h a l l b e n o t e d on t h e p r o p e r s c a l e a f t e r t h e pendulum has
completed i t s swing.

’. 1
’14 Workmanship. The a d h e s i v ei ne a c h of t h e1 - q u a r t sample u n i t s
S p L i f i e a 1,. A b l e I and 4 . 3 . 2 s h a l l b e examined f o r t h e p r e s e n c e of g r i t ,
lumps and s k i n s .

4 . 4 . 1 5U n i tc o n t a i n e rc o n t e n t . The u n i tc o n t a i n e rs h a l l beweighedand
t h i s n e t weight s h a l l be divided by t h e w e i g h t p e r g a l l o n of t h e m a t e r i a l , as
determinedin4.4.1, t o obtainthevolumetriccontent of t h e c o n t a i n e r .

4 . 5I n s p e c t i o n ofpackaging. Sample packagesandpacks,and t h ei n s p e c t i o n

of the preservation-packaging, packing andmarking f o r shipment and s t o r a g e s h a l l
beinaccordancewiththerequirementsofsection5 and t h e documents s p e c i f i e d
therein.

5. PACKAGING

(The p a c k a g i n g r e q u i r e m e n t s s p e c i f i e d h e r e i n a p p l y o n l y f o r d i r e c t Govern-
ment acquis it i o n . )

5.1
Packaging,
Packaging
shall be l e v e l A o r C , a s s p e c i f i e d ( s e e 6 . 2 . 1 ) .

5 . 1 . 1 Level A . The a d h e s i v es h a l l b ef u r n i s h e di n1 - g a l l o nc a n so r
5 - g a l l o np a i l s ,a ss p e c i f i e d( s e e6 . 2 . 1 )

5.1.1.1One-galloncans.One-galloncansshall conform t ot y p e V , c l a s s 2
of PPP-C-96. The cans s h a l l b e roundand s h a l l haveplan B e x t e r i o r c o a t i n g .

5 . 1 . 1 . 2F i v e - g a l l o np a i l s .F i v e - g a l l o np a i l ss h a l l conform t o t y p e I I ,
c l a s s 3of PPP-P-704.

5 . 1 . 2 Level C . The a d h e s i v es h a l lb e packaged t oa f f o r da d e q u a t ep r o t e c -

t i o n a g a i n s t d e t e r i o r a t i o n and damage during shipment from t h e s u p p l y s o u r c e t o
t h ef i r s tr e c e i v i n ga c t i v i t y ,f o r immediate use.Packaging may conform t o t h e
c o n t r a c t o r ’ s normal r e t a i l p r o c e d u r e when such meets the requirements of t h i s
level.

5 . 2P a c k i n g .P a c k i n gs h a l lb el e v e l A , B , C , o r commercial,asspecified
(see6.2.1).

5.2.1 Level A .

5.2.1.1One-galloncans. The 1 - g a l l o nc a n ss h a l lb e packed inaccordance

with the overseas shipment requirements of t h e a p p e n d i x t o PPP-C-96.

5 . 2 . 1 . 2F i v e - g a l l o np a i l s . The 5 - g a l l o np a i l sr e q u i r e no packing.

5.2.2Level B.

5.2.2.1One-galloncans. The 1-galloncansshallbepackedinaccordance

with the domestic shipment requirements of the appendix t o PPP-C-96.

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EíIL-A-3316C

5.2.2.2 Five-gallon pails. The 5-gallon pails require no packing.

O 5.2.3 Level C. Adhesives packaged as specified (see6.2.1) shall be packed

in containers acceptable to the common carrier which will ensure safe delivery
at the destinationin a satisfactory condition at the lowest applicable rate.
Containers or method of shipment shall comply with Uniform Freight or National
Motor Freight Classification rules or regulations or other carrier rules and
regulations as applicable to the mode of transportation.

5.2.4 Commercial. When specified (see 6.2.1), commercial packing shall

be in accordance with ASTMD 3951.
5.3 Narking. In addition to any marking required by the contract or order
* (see 6.2.1), interior and exterior containers and palletized or containerized
loads shall be marked in accordance NIL-STD-129
with and the requirements of the
Code of Federal Regulations, Title29, Part 1910 when applicable. Interior and
exterior containers shall both be marked with the date of manufacture.

5.3.1 Special marking. All classes and grades containers shall include
the following marking:

"DOES NOT CONTAIN MERCURY OR MERCURY COMPOUNDS

ASBESTOS FREE
DO NOTADD WATER OR ANY THINNING AGENTS"

In addition, class1 grade B containers shall also include the following:

USEWITH ASBESTOS FREE THERMAL INSULATION

O 6. NOTES
"FOR ONLY"

6.1 Intended use. The adhesives covered by this specification are intended
for use in securing cloth and tape to thermal insulations and for securing
thermal insulations to metal surfaces.

6.2 Ordering data.

6.2.1 Acquisition requirements. Acquisition documents should specify the

following:

(a) Title, number, and date of this specification.

(b) Class and grade of adhesive required (see1.2).
(c) Levels of packaging and packing required (see 5.1, 5.2 and 5.2.3).
(d) Capacity of interior container required (5.1.1).
(e) When palletized or containerized loads are required (see 5.2.4).
(f) When special marking is required (see
5.3).

6.2.2 Data requirements. When this specification is used in an acquisi-

tion and data are required to be delivered, the data requirements identified
below shall be developed as specified an approved
by Data Item Description
(DD Form 1664) and delivered in accordance with the.approved Contract Data
Requirements List (CDRL), incorporated into the contract. When the provisions
of DoDFAR Supplement, Part 27, Sub-Part 27.475-1 (DD Form 1423) are invoked
0 and the DD Form 1423 is not used, the data specified below shall be delivered by

17

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 MIL-A-3316C

the contractor in accordance with the contract or purchase order requirements.

Deliverable data required by this specification are cited in the following
paragraph.

Paragraphno.DatarequirementtitleApplicable DID no.Option

compliance
Certificate
of
3.2 DI-E-2121 -"-

(Data item descriptions related to this specification, and identified in

section 6 will be approved and listed as such in5010.12-L.,
DoD AMSDL.
Copies of data item descriptions required by the contractors in connection with
specific acquisition functions should be obtained fromNaval
the Publications
and Forms Center or as directed by the contracting officer.)

3, 4 , or
6.2.2 and any task in sections
6.2.2.1 The data requirements of
5 of this specification required to be performed to meet a data requirement may
be waived by the contracting/acquisition activity upon certification by the
offeror that identical data were submitted by the offeror and by the
accepted
Government under a previous contract for identical item acquired to this specifi-
cation. This does not apply to specific data which may be required for each
contract regardlessof whether an identical item has been supplied previously
(for example, test reports).

6.3 Qualification. With respect to products requiring qualification, awards

will be made only for products which are, at the time set for opening of bids,
qualified for inclusion in Qualified Products List QPL-3316 whether or not such
products have actually beenso listed by that date.The attention of thecon-
tractors is called to these requirements, and manufacturers are urged to arrange
to have the products that they propose to offer to the Federal Government tested
for qualification in order that they may be eligible to be awarded contracts or
purchase orders for the products covered by this specification.The activity
responsible for the Qualified Products List is the Naval Sea Systems Command,
SEA 5523, Department of the Navy, Washington, DG 20362-5101 and information
pertaining to qualification of products may be obtained from that activity.
Application for qualification tests shall be made in accordance with "Provisions
Governing Qualification SD-6" (see 6.3.1).

6.3.1 Copies of "Provisions Governing Qualification SD-6" may be obtained

upon application to Commanding Officer, Naval PublicationsForms
and
Center,
PA 19120.
5801 Tabor Avenue, Philadelphia,

6 . 4 Cross-reference of classifications. The classes of this specifi-

cation corresponding to the types of the previous issues are as follows:

MIL-C-3316
MIL-A-3316A
MIL-A-3316C
and
NIL-A-3316B

Class 1 Type 1 ""

Class 1 Type II Type II

Class 2 Type III Type III
Class 3 ""
Type 1

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 HIL-A-3316C 80 9777706 0076708 7

MIL-A-3316C

6 . 5 M a t e r i a ls a f e t yd a t as h e e t s .C o n t r a c t i n go f f i c e r s will i d e n t i f yt h o s e
activitiesrequiringcopies ofcomple'ted N a t e r i a lS a f e t yD a t aS h e e t s (MSDS)
preparedinaccordancewith FED-STD-313.The p e r t i n e n t Government m a i l i n g
a d d r e s s e sf o rs u b m i s s i o no fd a t aa r el i s t e di na p p e n d i x B of FED-STD-313. I n
order to obtain the MSDS, FAR c l a u s e 5 2 . 2 2 3 - 3 must be i n t h e c o n t r a c t .

6.6 S u b j e c t term (keyword) listing.

Bonding
F i b r o u sg l a s sc l o t h
. F i b r o u sg l a s si n s u l a t i o n

6 . 7 Changes from p r e v i o u si s s u e .A s t e r i s k sa r en o tu s e di nt h i sr e v i s i o n
t o i d e n t i f y changeswithrespecttothepreviousissue due t o t h e e x t e n s i v e n e s s
of the changes.

Custodians: Preparing activity:

Army MR - Navy SH -
Navy SH - (Project 8040-0462)

User a c t i v i t i e s :
Navy - AS, OS, YD, CG

19

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 NIL-A-3316C

SH 131921
FIGURE 1. Time temperaturecurve.

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 )5EEüÑq
MIL-A-3316C
AMENDMENT 2
23 August 1990
SUPERSEDING
INT. AMENDMENT 1
14 June 1988

MILITARY SPECIFICATION

ADHESIVES, FIRE-RESISTANT,
THERMAL INSULATION

This amendment forms a partof MIL-A-3316C, dated 20 October 1987,and is

approved for use by all Departments and Agenciesof the Departmentof Defense.
PAGE 4

3.4, second sentence: Delete "(see 4.1.2)" and substitute '(see 4.4.15)".
PAGE 5

3.5.1, first sentence: Delete and substitute: "The flash point of the
adhesive shall be higher than llO'F (see 4.4.4)."

PAGE 7

3.16: Delete '(see 4.4.15)" and substitute "(see 4.4.16)".

3.17: Delete and substitute:

"3.17 Material safetv data sheet (MSDS). The contracting activity shall be
provided a material safety &ta sheet at thetime of contract award. The MSDS
shall be provided in accordance withthe requirements of FED-Sm-313 and 29 CFR
1910.1200, Hazard Communication Standard. When FED-STD-313 is at variance with
the CFR, 29 CFR 1910.1200 shall takeprecedence. FED-STD-313 shall be modified
and supplemented accordingly. The MSDS shallbe included with each shipment of
the material covered by this specification (see6.5)."

4.1.2: Delete.

4.2, second sentence: Delete '4.4.14" and substitute '4.4.15'.

AMSC N/A FSC 8040

DISTRIBUTION STATEMENT 4 Approved for publicrelease; distribution unlimited,

1 of 3

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 MIL-A-3361C
AHENDMENT 2

PAGE 8

Table I,Flash point, under Inspection procedures for Adhesive class 1

column, add: "4-4.4' and Unit container content, under Inspection procedures for
adhesive class 1, 2, and 3 columns, delete"4.4.15" and add '4.4.16".
PAGE 9

4.3.2.3, second sentence: Delete "4.4.15" and substitute '4.4.16".

4.4.1, second sentence: Delete "4.4.15" and substitute "4.4.16".

PAGE 10

4.4.4, first sentence: Add "1," after "classes'.

PAGE 16

4.4.15: Renumber to '4,4.16".

Add newparagraph 4.4.15:

"4.4.15 Toxicoloeical formulation. To determine conformance to the

requirements of 3.4, the manufacturer of the compound shall disclose the
formulation of his product to the Commander, Naval Medical Command (MEDCOM-02)
Washington, DC 20372 for approval. The disclosure of proprietary information,
which will be held confidence
in bythe Naval Medical Command, shall include the
name, formula, and approximate percentageby weight, and volume of each
ingredient in the product; the results of any toxicological testing of the
product; and such other information as may be needed to permitan accurate
appraisal of any toxicity problem associated with the handling, storage,
application, use, disposal, or combustion of the material."

PAGE 18
* 6.2.2.1: Delete.

PAGE 19 .
6.5: Delete and substitute:

"6.5 Material safety data sheet (MSDSL. Contracting officers shall

identify those activities requiring copies of MSDSs. Additional required Govern-
ment information is contained in FED-STD-313. In order to obtain the MSDS,FAR
clause 52.223-3 mustbe in the contract."

2
,
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 MIL-A-3361C
AMENDMENT 2

The margins of this amendment are marked with an asterisk to indicate where
changes (additions, modifications, corrections, deletions) from the previous
amendment were made. This was done asa convenience only and the Government
assumes no liability whatsoever for any inaccuraciesin these notations. Bidders
k and contractors are cautioned to evaluate the requirements of this.document base
on the entire content irrespective of the marginal notations and relationship to
the last previous amendment.

Custodians:
Army
Navy
-- SH
MR
Preparing activfty:
Navy - SH
(Project 8040-0499)

-
User activities:
Navy .AS, OS, YD, CG

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