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SUPPLEMENT TO THE WELDING JOURNAL, JUNE 1999
Sponsored by the American Welding Society and the Welding Research Council
Flat microtensile specimens were found suitable for determining the mechanical
properties of similar and dissimilar laser beamweld joints
ABSTRACT. Laser beam (LB) welding is sile specimens, the mechanical proper- ily weldable by this process. A series of
increasingly being used in welding of ties were examined by microhardness studies describing the successful use of
structural steels. The thermal cycles as- survey and conventional transverse and laser beam (LB) welding to different steels
sociated with laser beam welding are round tensile specimens. The results of in various industrial applications can be
generally much faster than those in- the microtensile specimens were com- found in the literature (Refs. 1–9). How-
volved in conventional arc welding pared with standard round tensile speci- ever, the chemical composition (particu-
processes, leading to a rather small weld mens, and this clearly showed the suit- larly C, P and S contents as well as car-
zone, that usually exhibits a high hard- ability of the microtensile specimen bon equivalent) of the structural steels
ness for C-Mn structural steels due to the technique for such joints. The crack tip significantly influences the laser weld-
formation of martensite. It is rather diffi- opening displacement (CTOD) tests were ability of these materials. In modern
cult to determine the tensile properties of also performed to determine the fracture structural steels, the carbon content is
a laser weld joint area due to the small toughness of the LB welds using three- significantly reduced and the strength is
size of the fusion zone. Complete infor- point bend specimens. The effect of attained by alloying elements and/or
mation on the tensile and fracture tough- strength heterogeneity (mismatching) thermal processing during rolling. These
ness properties of the fusion zone is es- across the weld joint and at the vicinity fine-grained steels are particularly suit-
sential for prequalification and a of the crack tip on the CTOD fracture able for the low-heat-input laser welding
complete understanding of the joint per- toughness values was also discussed. process to avoid the development of a
formance in service, as well as for con- coarse-grained microstructure in the
ducting the defect assessment procedure Introduction HAZ region. However, the low heat input
for such weld joints. Therefore, an ex- and high cooling rate (high welding
perimental investigation on the mechan- Steel is a good absorber of the light speed) typical of this process promote the
ical properties of laser welded joints wave lengths produced by CO2 and formation of hard and brittle microstruc-
using flat microtensile specimens (0.5 Nd:YAG lasers and many steels are read- tures (i.e., martensite) within the narrow
mm thick, 2 mm wide) was carried out to weld and HAZ regions of steels subjected
establish a testing procedure to deter- to solid-state phase transformations.
mine the tensile properties of the weld Since the hardness values reached in
metal and heat-affected zone (HAZ) of KEY WORDS these regions are usually well above
the laser beam welds. those specified in standards and codes of
In the present work, two similar joints, Laser Beam Welding conventional arc welds, expensive and
namely, ferritic-ferritic and austenitic- LBW time-consuming qualification proce-
austenitic and one dissimilar ferritic- CO2 Laser dures may be required for some compo-
austenitic joint were produced with a Fracture Toughness nents (Ref. 10). It has been reported (Ref.
CO2 laser using 6-mm-thick steel plates. Flat Microtensile 11) that the use of the IIW formula for car-
In addition to the testing of flat microten- Hardness Test bon equivalent (Ceq) is not adequate to as-
sess the hardening effect in the fusion
G. ÇAM and M. KOÇAK are with GKSS Re-
Crack Tip Opening
zone of the laser welds of C-Mn steels.
search Center, Institute of Materials Research, C-Mn Steel
The weld formation and quality of LB
Geesthacht, Germany. S. ERIM and Ç. YENI HAZ
steel weldments are usually associated
are with Dokuz Eylül University, Mechanical
Engineering Dept., Izmir, Turkey. with three aspects: porosity, solidifica-
Fig. 1 — Three-point bend specimen geometry for fracture toughness Fig. 2 — Schematic showing the extraction and loading of the flat mi-
testing. crotensile specimens.
RESEARCH/DEVELOPMENT/RESEARCH/DEVELOPMENT/RESEARCH/DEVELOPMENT/RESEARCH/DEVELOPMENT
base metal will subsequently prevent the and they were tested at both room tem-
brittle fracture initiation in the laser beam perature and –40°C (–40°F). CTOD mea-
weld zone, which contains a martensitic surements using the GKSS developed d5
microstructure and hence high hardness. clip gauges (Refs. 14, 22) were con-
The fracture toughness testing procedure ducted on SENB specimens, which al-
for LBW joints should take this very nat- lowed a direct measurement of the crack
ural phenomenon into account and tip opening displacement for each spec-
hence should not take any artificial mea- imen.
sure (by producing larger weld zone or Standard flat transverse-tensile speci-
extensive side-grooving) to force the frac- mens were extracted from the welded
ture process to remain within the weld
plates. Weld reinforcement was ma-
zone. This may be achieved in laboratory
scale specimens, but fracture behavior of
LBW joints will follow its own natural
course during the service.
In the present study, an emphasis has
also been given to the establishment of
the flat microtensile specimen testing
procedure and hence the determination
of the tensile property gradient existing in
the LB fusion zone. The flat microtensile
specimen technique was originally de-
veloped for property determination of
HAZ for conventional multipass weld
joints (Ref. 19). Successful applications
of this technique for thick-section similar
and dissimilar electron beam welds (Ref.
12) and for the strength determination of
diffusion welded joints (Refs. 20, 21)
were also carried out at the GKSS re-
search center. This study is an extension
of these experimental activities and
specifically addresses the development
and refinement of the testing procedure
for laser beam steel welds, and hence,
similar and dissimilar laser beam weld
joints between ferritic and austenitic
steels produced by CO2 laser using 6-mm
thick plates were systematically investi-
gated. Fig. 4 — Hardness profiles of the joints. A — Schematic illustration of the micro-hardness mea-
surement procedure; B — similar ferritic; C — similar austenitic; D — dissimilar joints.
Experimental Procedure
Fig. 6 — Stress-strain curves of the flat microtensile specimens ex- Fig. 7 — Mechanical property variations across the joints (0 represents the weld
tracted from: A — Similar ferritic; B — similar austenitic; C — dis- center): A — Similar ferritic; B — similar austenitic; C — dissimilar joints.
similar joints.
chined before testing. Sets of flat mi- loading was introduced using four high- Results and Discussion
crotensile specimens were also extracted strength round pins at the shoulders of
by spark erosion cutting from base met- the specimens — Fig. 2. All tensile tests Microstructural Observations
als, HAZs and weld metals of all the were carried out at room temperature
joints studied as schematically shown in using a displacement rate of 0.5 mm/min Microstructural examinations of the
Fig. 2. The flat microtensile specimen in a screw-driven universal testing ma- joints investigated showed that the weld
preparation was conducted mainly in chine. After testing, the broken half of the regions of similar ferritic and dissimilar
joints contained bainite and martensite.
two stages: 1) extraction of a pre-shaped flat microtensile specimens were
Figure 3 shows macrosections of the
block with laser weld in the middle, 2) mounted for microstructural verification
joints. Similar ferritic joints displayed a
cutting out specimens from etched pre- of the specimen location. The fracture weld metal structure consisting of bainite
shaped block using a spark erosion cut- surfaces of selected bend and tensile and martensite, whereas similar
ting technique (with 0.1-mm diameter specimens were also examined by scan- austenitic welds exhibited an austenite-
Cu wire) parallel to the weld. Due to the ning electron microscopy for presence of dendritic (cellular) structure with no evi-
small size of the microtensile specimens, porosity. dence of martensitic formation as ex-
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rite/pearlite structure and pearlite disso- containing ferritic
lution at the base metal sides. A dissimi- steel always failed in
lar joint, on the other hand, showed an the lower strength fer-
inhomogeneous weld metal microstruc- ritic base metal. The
ture containing a mixture of ferrite and stress-strain curves
austenite solidification structures in vary- obtained from flat
ing degrees due to an incomplete mixture transverse tensile
of the molten metals of both sides in the specimens show
weld pool during solidification. As re- some differences
ported earlier for dissimilar LB joints be- compared to the
tween St37 and austenitic steels (Refs. 2, round tensile speci-
4), some solidification cracks parallel to
mens due to the pres-
the dendritic growth were observed in
ence of LB weld re-
the weld zone of the dissimilar joints,
gion at the middle of
which indicates that sufficient thermal
the specimens. The
stresses were developed in these weld-
ments to separate the grain boundaries in stress-strain curve ob-
the cellular structure during solidifica- tained from the flat
tion, which was coarser than that in the transverse tensile
weld metal of similar austenitic joints. specimens of the dis-
The microstructural aspects of these similar joint lies be-
joints were discussed in more detail in an tween those of the
earlier publication (Ref. 4). similar joints of the
constituent steels, as
Hardness expected — Fig. 5.
Evidently, these tests,
In order to determine the hardness particularly for ferritic
profiles, extensive microhardness mea- joints where a high
surements were conducted at three posi- hardness profile ex-
tions (top, middle and root), Fig. 4A. The ists, do not give any
microhardness results exhibited no sig- information on the
local mechanical Fig. 8 — Comparison of the stress-strain curves of base metals obtained
nificant difference between these posi-
properties of the weld by testing standard round and flat microtensile specimens: A — Fer-
tions for all the weld joints studied, Fig.
region. ritic; B — austenitic steel.
4, implying that no significant gradient in
mechanical properties of laser welds
along the plate thickness direction is pre-
sent. Similar ferritic steel joints displayed
a high hardness profile in the weld region
while austenitic welds showed almost
no change in hardness across the joint.
Similar St37 joints exhibited a peak
hardness value of about 330 HV, whereas
similar austenitic joints displayed a hard-
ness value of about 210 HV in the weld
region — Figs. 4B and 4C, respectively.
This is expected due to the lack of bainite
and/or martensite formation in the weld
regions of austenitic joints. Dissimilar
joints displayed a hardness peak of about
380–400 HV within the weld metal —
Fig. 4D, which is slightly higher than that
of similar ferritic weld metal.
Tensile Properties
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standardized CTOD or J) of mis-matched
laser weld specimens is very hard to
overcome due to the high strength mis-
match within a very small region at the
vicinity of the crack tip. It is not a simple
task to distinguish the contributions from
both the base metal (lower strength) and
the narrow LB weld (highly over-
matched) at the vicinity of the crack tip
to the remotely measured crack mouth
opening displacement (CMOD) and load
line displacement (VLL) usually used in
standardized CTOD and J estimates.
A local and direct measurement tech-
nique (d5 technique) was developed at
GKSS Research Center as a measure of
the CTOD for determining the fracture
toughness and the crack growth resis-
tance. It consists of measuring the rela-
tive displacement of two gauge points di-
rectly at the crack tip using special
displacement gauges. The resulting
CTOD is called d5 because the gauge
length over which the CTOD is deter- tremely high overmatch-
mined amounts to 5 mm. The advantage ing of the fusion zone
of this measurement concept is that the (about 310%, Table 2) —
d5 type CTOD can be easily measured on Fig. 11. The very high
any configuration with a surface break- CTOD values for similar
ing crack; no calibration functions are re- ferritic laser weld joints
quired. Another appealing aspect of the are obviously not repre-
d5 technique is that since it is measured senting the intrinsic
locally as a displacement at the location toughness properties of
of interest, it does not have to be inferred the weld zone, which
from remotely measured quantities, like showed very high hard-
the J integral or the standardized CTOD. ness values and predom-
This is of particular importance when the inantly bainitic/marten-
specimen is mechanically inhomoge- sitic microstructure. If
neous, as is the case for highly mis- the maximum load
matched strength in narrow laser welds. CTOD values (dm) are re-
The CTOD values of the laser weld joints ported (as standard
on the SENB specimens have, therefore, CTOD procedure re-
been measured in terms of the CTOD (d5) quires) the toughness
technique. level of laser welds will
For each weld condition, three deeply therefore be overesti-
notched (a/W = 0.5) three-point bend mated. This is due to the
specimens were tested at room tempera- effect of lower strength
ture (RT) and –40°C, and they all exhib- base metal present near
ited fully ductile fracture behavior. Fer- the vicinity of the crack
ritic base metal displayed similar CTOD tip (laser weld width
values at both testing temperatures, indi- being approximately 2
cating that –40°C lies at the upper shelf mm), which relaxes the
of ductile-brittle transition for this ferritic stress state at the fatigue
steel grade, whereas austenitic base crack tip in the middle of
metal exhibited slightly lower CTOD val- the laser weld. The ap-
ues at –40°C, indicating sensitivity of plied deformation prin-
toughness to testing temperature — Figs. cipally goes to the lower
9 and 10. strength base metal part
Similar ferritic joints displayed higher of the specimen, and
CTOD values than the base metal at RT, hence, the critical frac-
which can be attributed to the extensive ture stress for a possible Fig. 12 — Crack propagation in dissimilar joint along the weld
brittle fracture at the zone (small arrows indicating solidification cracks). Note crack
crack tip branching and crack path devi-
path deviation into lower strength ferritic base metal.
ation into the softer base metal due to ex- crack tip cannot be
CTOD values at RT (Fig. a slight crack path deviation into the base
9) due to asymmetric metal (overmatching of the fusion zone is
plastic zone develop- about 110%, Table 2) in the austenitic
ment, which comes from similar joints. The crack propagates
the strength mismatch along the weld region parallel to the weld
between ferritic and at both testing temperatures (Fig. 13) il-
austenitic steel base met- lustrating that these specimens do not
als (M = 0.76, Table 1). contain strength mismatch between the
Figure 12 shows the dis- laser weld zone and the austenitic base
similar joint crack tip metal as hardness results indicated. In the
that displays a one-sided dissimilar ferritic-austenitic joints, the
deformation, and hence, crack path deviates clearly into the lower
crack growth towards strength ferritic steel side and propagates
lower strength ferritic within the ferritic steel at both testing
steel (the mismatch be- temperatures as illustrated in Fig. 12. On
tween the ferritic base the other hand, an excessive crack tip
metal and fusion zone is branching in the similar ferritic joints was
about 230%, Table 2). It observed, and the cracks always devi-
is interesting to note that ated into the softer base metal due to ex-
the presence of small so- tensive plastic zone development within
lidification cracks lying the base metal at both testing tempera-
perpendicular to the tures — Fig. 11.
crack direction in the The fracture behavior of all these
weld zone of dissimilar specimens can be explained with the
joints (Fig. 12) did not help of strength mismatch information,
show any detrimental ef- hardness profiles and the microstructures
fect on the fracture developed in the weld regions. Obvi-
toughness values, al- ously, the ferritic base metal is the weak-
though dissimilar joints est constituent (in terms of tensile
exhibited slightly lower strength) in similar ferritic joints and in
CTOD values than simi- dissimilar joints into which the crack de-
lar joints. This can be viates. This crack path deviation into the
due to the fact that ex- lower strength base metal, which is
tensive plastic deforma- schematically shown in Fig. 14, during
tion developed at the standard three-point bend tests with the
Fig. 13 — Crack propagation in a similar austenitic joint. There is lower strength ferritic notch in the overmatched narrow laser
no distinct crack path deviation but the crack propagates in the steel side of the speci- weld zone leads to an experimental dif-
base metal along the weld zone. men (shielding effect of ficulty in determining the intrinsic frac-
the overmatched weld ture toughness properties of thin section
zone). C-Mn steel laser welds.
Conclusions
RESEARCH/DEVELOPMENT/RESEARCH/DEVELOPMENT/RESEARCH/DEVELOPMENT/RESEARCH/DEVELOPMENT
joints displayed significantly higher robots in the automotive industry. 5th Euro-
strength values (M = ~3.1) and markedly pean Conference on Laser Treatment of Mate- 13. Koçak, M. and Schwalbe, K.-H. 1994.
rials, ECLAT’94, pp. 151–164, Bremen, Ger- Fracture of weld joints: mismatch effect.
lower strain values than the base metal
many. Neuentwicklungen im Konstruktiven Inge-
specimens, due to the presence of bai-
2. Yeni, Ç., Erim, S., Çam, G., and Koçak, nieurbau, pp. 137–155, Ed. H. Saal and Ö.
nite/martensite in the weld zone. The all- Bucak, Univ. of Karlsruhe, Germany.
M. 1996. Microstructural features and fracture
HAZ specimens also exhibited higher 14. Schwalbe, K.-H., and Koçak, M. 1992.
behaviour of laser welded similar and dissim-
strength values and lower strain values Fracture mechanics of weldments-properties
ilar steel joints. Int. Welding Technology ’96
than those of the base metal. Symposium, pp. 235–247, Istanbul, Turkey, and applications to components. 3rd Int. Conf.
4) Similar austenitic joints exhibited Gedik Education Foundation. on Trends in Welding Research, pp. 479–494,
no significant property variation across 3. Çam, G., Riekehr, S., and Koçak, M. Gatlinburgh, Tenn.
the weld zone as indicated by a hardness 1997. Determination of mechanical proper- 15. Koçak, M., Es-Souni, M., Chen, L., and
profile. The microtensile specimens ex- ties of laser welded steel joints with microten- Schwalbe, K.-H. 1989. Microstructure and
tracted from the weld zone of the dis- sile specimens. The ASM International Euro- weld metal matching effects on heat affected
similar joint exhibited high strength and pean Conference on Welding and Joining zone toughness. 8th Int. Conf. OMAE-ASME,
low strain values. The all-HAZ speci- Science and Technology, pp. 63–79, Madrid, pp. 623–633, The Hague, Netherlands.
mens extracted from the HAZ at the fer- Spain, ASM International, IIW Doc. SC X-F- 16. Kirk, M. T., and Doods, R. H. 1992. The
ritic side also displayed higher strength 055-97. influence of weld strength mis-match on crack
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and Koçak, M. 1998. Investigation into prop- imens. University of Illinois Report, UILU-
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5) CTOD fracture toughness testing
steel joints. Journal of Science and Technology 17. Cao, H. C. and Evans, A. G. 1994. An
does not provide “intrinsic toughness
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strength base metal side (mismatch). 6. Kristensen, J. K., and Borgreen, K. 1994. ification, process monitoring, NDT and adap-
6) The CTOD values obtained for sim- Mechanical properties and microstructures of tive welding control. Int. Conf. on Explotation
ilar and dissimilar joints demostrate the laser welded constructional steels. 5th Euro- of Laser Processing in Shipyards and Structural
toughness trends, which can be ex- pean Conference on Laser Treatment of Mate- Steelworks, Glasgow, U.K.
plained with strength mismatch and mi- rials, ECLAT’94, pp. 226–239, Bremen, Ger- 19. Klausnitzer, E. 1976. Entwicklung
crostructure aspects. many. eines Verfahrens zur Entnahme und Prüfung
7) Finally, an application of the flat 7. Sun, Z., and Moisio, T. 1994. Effect of von Mikro-Flachzugproben aus der WEZ von
microtensile specimen technique to laser processing parameters on laser welded dis- Schweißverbindungen. Materialprüfung 18(
welded joints was demonstrated. By similar joints. Welding Journal 73(4): 63-s to 11): 411–416
using this technique, it is possible to de- 70-s. 20. Çam, G., Bohm, K.-H., Müllauer, J.,
termine the local mechanical properties 8. Strychor, R., Moon, D. W., and Met- and Koçak, M. 1996. The fracture behavior of
zbower, E. A. 1984. Microstructure of ASTM diffusion-bonded duplex gamma TiAl. JOM,
of the joints, which can be correlated to
A-36 steel laser beam weldments. JOM, pp. pp. 66–68.
the respective microstructure and hard-
59–61 21. Çam, G., Müllauer, J., and Koçak, M.
ness. 1997. Diffusion bonding of two-phase g-TiAl
9. Metzbower, E. A. 1990. Laser beam
welding: thermal profiles and HAZ hardness. alloys with duplex microstructure. Journal of
Acknowledgments Welding Journal 69(7): 272-s to 278-s. Science and Technology of Welding and Join-
10. Dilthey, U., Dobner, M., Ghandehari, ing 2(5): 213–219.
This work is a part of the German- A., Lüder, F., and Träger, G. 1996. Entwick- 22. Koçak, M., and Denys, R. 1994. CTOD
Turkish joint project financed by Interna- lung, Stand und Perspektiven der Strahltech- and wide plate testing of welds with particu-
tional Bureau, KFA-Jülich and Türkiye nik, pp. 1–14, Konferenz Strahltechnik, Halle, lar emphasis on mis-match welded joints.
Bilimsel Teknik Arastirma Kurumu Germany. 10th European Conf. on Fracture, ECF 10,
(TÜBITAK), Turkey. The authors would 11. Kalla, G., Funk, M., et al. 1993. Heavy Structural Integrity, Experiments, Models, Ap-
like to thank both organizations for their section laser beam welding of fine-grained plications, pp. 97–120, Edited by K.-H.
financial support. They also would like to structural steels. LASER Technology and Ap- Schwalbe and C. Berger, Engineering Materi-
thank Mr. S. Riekehr and Mr. H. Mackel plications, pp. 319, H. Kohler (ed.), Vulkan- als Advisory Services (EMAS) Ltd.
for their technical assistance in testing. Verlag, Essen, Germany.