Ministry of Defence

Defence Standard 80-81

Issue 3 Publication Date 25 April 2003

Anti-Seize Compound, Molybdenum

Disulfide
NATO Code: S-722
Joint Service Designation: ZX-38

Reprinted 9 January 2006

to incorporate Amendment 2
DEF STAN 80-81 Issue 3

Contents

Foreword ..........................................................................................................................................................iii
Introduction......................................................................................................................................................iv
1 Scope ....................................................................................................................................................1
2 Warning.................................................................................................................................................1
3 Normative References .........................................................................................................................1
4 Materials................................................................................................................................................2
5 Product Conformity Certification (PCC) ............................................................................................2
6 Keeping Qualities.................................................................................................................................2
7 Containers And Marking Of Containers ............................................................................................3
8 Testing ..................................................................................................................................................3

Tables

Table 1 Test Requirements ..........................................................................................................................3

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 DEF STAN 80-81 Issue 3

Foreword
AMENDMENT RECORD

Amd No Date Text Affected Signature and Date

1 29/8/05 Editorial amendment to the pagination

2 9/01/06 Ref. to Antioxidant limits Para 4.2 & 4.3, SPM3

Standard formatted to the Template V2.

REVISION NOTE

This standard is raised to Issue 3 to update its content.

HISTORICAL RECORD

This standard supersedes the following:

DTD 5617 dated March 1974

Def Stan 80-81/1 dated 16 May 1980
Def Stan 80-81/2 dated 16 April 1993

a) This standard provides requirements for one grade of Anti-seize Compound, Molybdenum Disulfide, for
Ministry of Defence use..

b) This standard has been produced on behalf of the Defence Fuels and Lubricants Committee (DF&LC)
by the Aviation Propulsion Fuels and Lubricants Advisory Group (APFLAG).

c) This standard has been agreed by the authorities concerned with its use and is intended to be used
whenever relevant in all future designs, contracts, orders etc. and whenever practicable by amendment
to those already in existence. If any difficulty arises which prevents application of the Defence Standard,
UK Defence Standardization (DStan) shall be informed so that a remedy may be sought.

d) Any enquiries regarding this standard in relation to an invitation to tender or a contract in which it is
incorporated are to be addressed to the responsible technical or supervising authority named in the
invitation to tender or contract.

e) Compliance with this Defence Standard shall not in itself relieve any person from any legal obligations
imposed upon them.

f) This standard has been devised solely for the use of the Ministry of Defence (MOD) and its contractors
in the execution of contracts for the MOD. To the extent permitted by law, the MOD hereby excludes all
liability whatsoever and howsoever arising (including, but without limitation, liability resulting from
negligence) for any loss or damage however caused when the standard is used for any other purpose.

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DEF STAN 80-81 Issue 3

Introduction

iv
 DEF STAN 80-81 Issue 3

Standards for Defence - Anti-Seize Compound, Molybdenum

Disulfide - NATO Code: S-722,
Joint Services Designation: ZX-38

1 Scope
This Defence Standard specifies the requirements for one grade of anti-seize compound intended for use up
to 250°C. This product should not be used as an engineering lubricant. This product should not be used on
titanium or titanium alloys.

2 Warning
The Ministry of Defence (MOD), like its contractors, is subject to both United Kingdom and European laws
regarding Health and Safety at Work. All Defence Standards either directly or indirectly invoke the use of
processes and procedures that could be injurious to health if adequate precautions are not taken. Defence
Standards or their use in no way absolves users from complying with statutory and legal requirements
relating to Health and Safety at Work.

3 Normative References

3.1 The publications shown below are referred to in the text of this standard. Publications are grouped and
listed in alpha-numeric order.

Def Stan 05-50:

Part 38 Methods for Testing Fuels, Lubricants and Associated Products:
Molybdenum Disulphide Content of Lubricants
Def Stan 05-52:
Part 1 Markings for the Identification of Fuels, Lubricants and Associated Products:
Containers Holding 216.5 Litres or Less
IP 50 Determination of Cone Penetration of Lubricating Grease
IP 112 Determination of Corrosiveness to Copper of Lubricating Grease – Copper Strip Method
IP 154 Corrosiveness to Copper – Copper Strip Test
IP 367 Determination and Application of Precision Data in Relation to Methods of Test
IP 396 Determination of Dropping Point of Lubricating Grease – Automatic Apparatus Method

3.2 Reference in this Standard to any normative references means in any Invitation to Tender or contract
the edition and all amendments current at the date of such tender or contract unless a specific edition is
indicated.

3.3 In consideration of clause 3.2 above, users shall be fully aware of the issue and amendment status of
all normative references, particularly when forming part of an Invitation to Tender or contract. Responsibility
for the correct application of standards rests with users.

3.4 DStan can advise regarding where normative references documents are obtained from. Requests for
such information can be made to the DStan Helpdesk. How to contact the helpdesk is shown on the outside
rear cover of Def Stans.

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DEF STAN 80-81 Issue 3

4 Materials

4.1 The anti-seize compound, molybdenum disulfide, ZX-38 shall be manufactured from a mineral oil and
a suitable gelling agent and not less than 50 percent by mass of molybdenum disulfide. The Molybdenum
disulfide shall be of Technical Fine Grade with a particle size of 0.65 to 0.75 micrometers and of minimum
98% purity.

4.2 The use of the additives 2,6-di-tert-butylphenol and 2,6-di-tert-butyl-4-methylphenol is not permitted
and the incidental presence of these materials is limited in total to 50mg/l of the finished product.

4.3 The Ministry of Defence reserves the right to require that the material and any components used be
subjected to toxicological and physiological tests to ascertain their suitability for use.

“NOTE: Products supplied to this standard may be used on HM Submarines and shall be subject to a
Material Toxicity Hazard Review. Details for obtaining the Material Toxicity Hazard Review are available from
the Technical Authority.”

5 Product Conformity Certification (PCC)

5.1 Product Conformity Certification (PCC) procedure applies to product supplied for MoD use against this
Standard.

5.2 Before any product can be considered as complying with this Standard, the manufacturer must
demonstrate to the Technical Authority that the product meets all the requirements of this Standard. At this
time, a declaration in confidence of the formulation, including identification and source of all components, is
required.

5.3 The Technical Authority will then assign a unique identification reference to this product, which
becomes a Technically Acceptable Product. The Technical Authority will maintain a list of Technically
Acceptable Products in a Technically Acceptable Products List (TAPL). Only those products that are listed
on the TAPL may be stated as complying with the requirements of this specification.

5.4 Once accepted as a Technically Acceptable Product, no change in formulation of the product so
referenced shall be made without prior notification to the Technical Authority. The supplier shall also certify
that the reformulated product continues to meet the requirements of this Standard and provide evidence to
that effect.

5.4.1 Once such certification and evidence has been received, the reformulated product will be assigned a
new discrete identification number and will be added to the TAPL.

5.5 When supplying product to the Ministry of Defence, the supplier shall certify that the product delivered
fully complies with the requirements of this Standard.

5.6 Testing of the finished product shall be in accordance with Table 1. The Technical Authority reserves
the right to require additional evidence that the product or components are compliant at any stage of the
manufacturing process.

5.7 If any sample taken from the consignment were found not to comply with the requirements of this
standard, the whole consignment may be rejected.

6 Keeping Qualities
The product, when suitably stored in its original sealed containers, shall retain the properties described in
this Standard for a period, from the date of filling, of not less than 12 months in temperate climates and not
less than 6 months in tropical climates.

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 DEF STAN 80-81 Issue 3

7 Containers And Marking Of Containers

7.1 The product shall be supplied in sound, clean and dry containers, suitable for the product and in
accordance with the requirements of the contract or order.

7.2 Coatings and paint finishes shall comply with the requirements of the contract or order. Markings shall
be in accordance with the requirements of Def Stan 05-52 (Part 1). The product identification shall be
specified in the contract or order.

7.3 It shall be the responsibility of the contractor to comply with any legal requirements for the marking of
containers.

8 Testing

8.1 Test results for the product shall not exceed the maximum nor be less than the minimum values set
out in Table 1.

8.2 Methods quoted in the table are referee methods and shall be used in cases of dispute. Alternative,
technically equivalent standard methods may be used by agreement of the Technical Authority.

8.3 The IP 367 procedure, which covers the use of precision data, shall be used for the interpretation of
test results.

Table 1 Test Requirements

Test Property Units Limits Method

1 Appearance Homogeneous, free Visual examination
from visible
impurities

2 Cone Penetration:
Worked 0.1 mm 200 to 300 IP 50

3 Dropping Point °C Min 140 IP 396

4 Molybdenum Disulphide % m/m Min 50 Def Stan 05-50

Content Part 38

5 Corrosiveness to Copper: IP 112

Test temperature 100 °C
Condition of Copper Strip No etching or pitting for 24 hours

Copper Strip Rating Max 1b Rating as per IP 154

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 ©Crown Copyright 2005

Copying Only as Agreed with DStan

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The DStan file reference relating to work on this standard is .D/DSTAN/80/81

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