Basis of Design For Basic Process Engineering of Omnisulf

71707-02-GWR
Process Engineering Qatargas II LNG

®
OmniSulf
Offenders are liable to the payment of damages. All rights are reserved in the
tion of the contents thereof, are forbidden without express authority by Lurgi.
Copying of this document, and giving it to others and the use or communica-
event of the grant of a patent or the registration of a utility model or design.
BASIS OF DESIGN
for
BASIC PROCESS ENGINEERING

of
OmniSulf®
OWNER
ExxonMobil/Qatar Petroleum
OWNER PROJ.NO. OWNER DOCUMENT NO REV.
CONTRACTOR
Chiyoda Corporation
CONTR. PROJ.NO. CONTRACTOR DOCUMENT NO REV.
Jue 17.10.03 DRTO BE

Name Date Name Name Date Status Basic Engineering
Prepared, revised Checked Approved Remark, kind of revision
Q.L. DL-No. DCC
Project Name Project No. Document No. Sheet / of Revision

Qatargas II LNG 71707-02 00010 1 / 36 2
Derived from GFA 0373E
Issue: Rev. 0 , May 31, 2001 Sheet 1 of 36
Table of Contents
Section Page
1 INTRODUCTION 4
2 PROCESS 5
2.1 PROCESS DESCRIPTION 5
2.2 BLOCK FLOW DIAGRAM 7
3 BATTERY LIMITS 8
3.1 DEFINITION OF BATTERY LIMITS 8
3.2 BATTERY LIMIT CONDITIONS OF PROCESS STREAMS 9
4 DESIGN PARAMETERS 10
4.1 UNIT CAPACITY AND FEED GAS CONDITION AND COMPOSITION 10
4.2 PRODUCT SPECIFICATION 13
4.3 SULPHUR RECOVERY 14
4.4 TURN DOWN 15
4.5 UTILITIES 16
4.6 METEOROGICAL DATA 20
4.7 ADDITIONAL DESIGN INFORMATION 21
5 Engineering documents 24
6 Numbering 25
6.1 UNIT NUMBERING 25
6.2 EQUIPMENT NUMBERING 26
6.3 PROCESS STREAM NUMBERING 27
6.4 NUMBERING OF PIPING 27
6.5 INSTRUMENT TAG NUMBER 32
6.6 ELECTRICAL IDENTIFICATION 34
7 UNITS OF MEASUREMENT 35

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EDP Ident. No. QGII_BasisofDesign_R2.doc Derived from GFA 0373E
Index of Relevant Documents
No. Title Summary of Revisions
QG II/2000/PR/TS/NA/003 Supplement Requirement for Lurgi/BASF Scope of C4

Work
QG II/20/02/PR/TS/NA/001 Technical Requirement for Acid Gas Removal Unit 02 C6
QG II/24/09/PR/DP/NA/001 Technical Requirement for Sulphur Recovery Unit C5
QG II/20/09/PR/TS/NA/001 Technical Specification for Design & Fabrication of C1
Sulfur Recover Units
QG II/20/00/PE/PC/NA/301 Document Numbering Procedure D1
QG II/20/00/PE/PC/NA/303 Equipment / Line / Instrument Numbering Procedure C2
QGII/20/00/ME/TS/NA/603 Technical Specification For Design & Fabrication of
Refractory Lining of Sulfur Recovery Unit

Qatargas II LNG 71707-02 00010 3 / 36 2
1 INTRODUCTION
The client, Exxon Mobile / Qatar Petroleum, wishes to establish an LNG facility on the Persian Gulf
coast, in Ras – Laffan City. The LNG plant will receive, process and store LNG in one train.
The feed gas must be treated in the gas treating facilities to remove all CO2 to prevent freezing in the
downstream liquefaction plant and remove Sulphur components in order to meet LNG product
specifications.
The purpose of this document is to summarize the technical specification and requirements to be used
®
by Lurgi Öl Gas Chemie GmbH in preparing the Basic Process Engineering for the OmniSulf process.
Lurgi will consider Chiyoda’s following project procedures and/or project specifications to extent as it is
necessary and relevant for the scope of Lurgi’s supply:
QG II/20/02/PR/TS/NA/001 Technical Requirement for Acid Gas Removal and Dehydration Unit 02 / 03
QG II/24/09/PR/DP/NA/001 Technical Requirement for Sulphur Recovery Unit
QG II/20/09/PR/TS/NA/001 Technical Specification for Design & Fabrication of Sulfur Recover Units
QG II/20/00/PE/PC/NA/301 Document Numbering Procedure
QG II/20/00/PE/PC/NA/303 Equipment / Line / Instrument Numbering Procedure
QGII/20/00/ME/TS/NA/603 Technical Specification For Design & Fabrication of Refractory Lining of
Sulfur Recovery Unit

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2 PROCESS
®
The OmniSulf process is configured to treat all the feed gas in one gas processing train, in the following
called UNIT. The UNIT consists of a Acid Gas Removal Unit (AGR), a Claus Unit (CLS), a Tail Gas
Treating Unit (TGT), an Incineration Unit (INC) and a Degassing process (Hold).
Feed gas from the offshore facilities in the Persian Gulf is received in the Slug Catcher and preheated,
®
depressurised and metered prior to be processed in the OmniSulf process.
Treated gas, free of CO2, Sulphur components and water, enters the Liquefaction Unit via a Dehydration
and Mercaptan Removal Unit (DMR), a Mercaptan Recovery Unit (MRU) and a Mercury Removal Unit
for LNG production. DMR, MRU and Mercury Removal downstream the unit are not in the licensor’s
scope of work.
2.1 PROCESS DESCRIPTION

aMDEA Acid Gas Removal - Unit 02 - AGR
The aMDEA PROCESS is implemented for removing acid gas components CO2 , H2S and COS from
the Feed Gas stream from battery limit to the unit 02.
In this process activated MDEA is used as a liquid washing agent, recirculated in a washing loop.
The process uses a MDEA/water solution with a certain amount of activator. This amount of activator
depends on the CO2 partial pressure, the desired gas purity and how much energy is available.
Streams leaving the AGR are Flash Gas to the Incinerator Unit 09, Acid Gas to TGT Unit 09 and Clean
Gas to DMR Unit 03 outside of battery limit.
CLAUS - Unit 09 - CLS

The CLAUS PROCESS recovers Sulphur from gases. For optimum operation, in the CLAUS PROCESS
Lurgi’s Multi-Purpose-Burner is used. Mercaptane Gas from the MRU unit 03 will be burnt completely in
the muffle. Rich Acid Gas from the TGT Unit 09 will be processed in the lances around the burner muffle.
The H2S contained in the Rich Acid Gas is first converted partly to SO2 and will react with this SO2 to
form Sulphur and water. The reaction is further driven towards the production of Sulphur by reaction of
the remaining SO2 and H2S in catalytic converters. Sulphur produced is condensed and separated after
each step. The Sulphur stream will be sent to the Degassing Unit. The Claus Tail Gas will be sent to the
TGT Unit 09.
TAIL GAS TREATMENT and ACID GAS ENRICHMENT - Unit 09 - TGT

The TGT process is used for removal of Sulphur compounds from the Claus Tail Gas coming from the
Claus Unit 09 and includes an Acid Gas Enrichment step (AGE) for the Acid Gas coming from the AGR
Unit 02.
By means of a catalyst all Sulphur compounds contained in the Claus Tail Gas and the AGE Off Gas are
hydrogenated to H2S. After the process water is removed by a quench configuration, the Claus Tail Gas
is routed to a gas washing loop using generic amine solvent.
The gas washing loop consists of two absorbers and one common regeneration section for the amine
solvent.
In the first absorber (TGT Absorber), H2S is removed selectively from the hydrogenated Claus Tail Gas.
The TGT Tail Gas leaving the absorber is sent to the Incinerator Unit 09.
In the second absorber (AGE Absorber) the Acid Gas from the AGR Unit 02 is treated to produce an
AGE Off Gas with a low H2S content, which is routed to the Hydrogenation part of TGT.

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The Rich Solution from the AGE Absorber, which contains the main H2S portion of AGR Acid Gas, and
the Rich Solution from the TGT Absorber are treated in a common regeneration section to produce a
Rich Acid Gas processed in the Claus Unit 09.
INCINERATOR - Unit 09 - INC

In order to convert its residual H2S content to less harmful SO2, the desulphurized TGT Tail Gas coming
from the TGT Unit 09 is incinerated before being sent to atmosphere.
Sulfur Degassing – Unit 09 - DEG

On Hold!

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2.2 BLOCK FLOW DIAGRAM
The PROCESSES belonging to the UNIT are interconnected as depicted in the below Block Flow
Scheme:
Figure 1 Block Flow Scheme

?
Block Flow Diagram
B.L. B.L.
DMR Product Gas

aMDEA? Clean Gas Sweet Gas
Acid Gas Removal Dehydration and Mercury Removal
AGR (Unit 02) Mercaptan Removal HGR (Unit YYY)
DMR (Unit 03)
Off Gas
Raw Gas Condensate Mercaptan Gas Fuel Gas

Mercaptan Recovery
Stabilisation MRU (Unit 03 )
Liquid Hydrocarbons
RSH Liquid Storage
(Unit )
DSO B.L.
Acid Gas Rich Flexsorb / AGE

REGENERATION Sol. Acid Gas Flash Gas End Flash Gas
Tail Gas Treatment (EFG)
(Unit XXX) (Unit 09) Enrichment
(Unit 09)
SO2 Rich Acid Gas Incinerator

AGE Off Gas Rich Solution Off
Liquid Hydr.
Claus LTGT Gas
Sulfur TGT / HYDR Tail Gas TGT / ABS
Sulfur Claus Tail Gas Tail Gas Incineration
Sulfur Degassing Sulfur Production Tail Gas Treatment Tail Gas Treatment
(Unit 09) CLS (Unit 09) Hydrogenation Absorption INC (Unit 09)
TGT(Unit 09) TGT (Unit 09)
Residue Gas
B.L.

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3 BATTERY LIMITS
3.1 DEFINITION OF BATTERY LIMITS

The definition of the location of the UNIT and geographic area of the UNIT will be clearly depicted in the
respective layout plans.
Battery Limit for the Basic Process Engineering package means dealing with all process streams
passing the B.L. of the attached Block Flow Diagrams as well as all internal process streams. All utility
streams are engineered only within the process units. Interconnecting utility streams to be engineered by
the FEED contractor.
The following detailed explanations are for defining battery limits shown on P&Ids:

“Battery Limit” for an incoming process material line (e.g. feed gas, fuel gas, regeneration gas)
shall mean 1 m before first process related control device, or, if applicable, check valve or
spectacle blind.

“Battery Limit” for an outgoing process material line (product gas, fuel gas, off gas, off water) shall
mean 1 m after the last process related control device, or, if applicable, check valve or
spectacle blind.

“Battery Limit” for an incoming cooling water line shall mean 1 m before the flange of the
respective cooling water consumer.

“Battery Limit” for an outgoing cooling water line shall mean 1 m after the flange of the respective
cooling water consumer.

“Battery Limit” for an incoming Boiler Feed water line (steam production) shall mean 1 m before
the control device for the BFW flow rate control device before the steam raising vessel.

“Battery Limit” for an outgoing steam line (steam production) shall mean 1 m after the last steam
pressure control device related to the steam producer.

“Battery Limit” for an outgoing condensate line (condensate production) shall mean 1 m after the
last condensate control device or steam trap related to the condensate producer.

“Battery Limit” for an outgoing blow down condensate line (steam production) shall mean 1 m after
the condensate outlet flange of the respective steam raising vessel.

“Battery limit” for flare connections shall mean directly after the respective safety or control valve.

“Battery Limit” for off gas streams to atmosphere shall be directly at the location where the gas is
vented.(Top of the stack)

“Battery Limit” for control loops interconnecting between UNIT and other processes shall mean
directly at the control device inside the Unit.

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3.2 BATTERY LIMIT CONDITIONS OF PROCESS STREAMS
The Battery Limit conditions of the main feed and product process streams are defined as follows:
Table 1 Main Feed/Product Conditions
Feed Process Stream Product Process Stream

Feed Gas Sweet Gas
from B.L. to AGR unit 02 from AGR unit 02 to B.L.
Temperature °C Pressure bar(a) Temperature °C Pressure bar(a)
Operating Condition 40 68.4 50 > 67.2
1) 1) 1) 1)
Mechanical Design 100 82 76 77 100 82 76 77
Mercaptan Gas
from B.L. to Claus unit 09
Temperature °C Pressure bar(a)
Operating Condition 4549 1.78
Mechanical Design ?82 ?3.5 / F.V.
1)
to be defined / confirmed by client and/or contractor
Battery limit conditions of other product streams
Operating Condition Mechanical Design

Temperature °C Pressure bar(a) Temperature °C Pressure bar(a)
Condensate / ? 2.0 ? ?
Process Water
Sour Condensate / ? 3.0 ? ?
Process Water
Condensate ? ? ? ?
(Hydrocarbons,
Water)
Blow Down 60 3.0 ? ?
Liquid Sulphur 135 5.0 ? ?

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4 DESIGN PARAMETERS
4.1 UNIT CAPACITY AND FEED GAS CONDITION AND COMPOSITION

DESIGN CAPACITY:
The design capacities for the units are as following:
Case H2S content Purpose

BASE DESIGN 2.00 Design case for AGR
SRU DESIGN 1.00 Design for one train Claus, TGT, Incineration,
AGE and Regeneration
LOW ACID GAS 0.46 Rating case for Claus, TGT
FEED GAS:
The UNIT shall be able to handle feed gas with the following compositions and conditions:
Table 2 Raw Gas
Feed Gas to AGR

Case 2% H2S 1%H2S 0.46% H2S
Component Mol % Mol % Mol %

CO2 3.6850 2.8708 2.3091
N2 5.1181 4.2939 3.5776
He 0.0491 0.0513 0.0516
METHANE 80.7819 83.2304 84.7933
ETHANE 4.7946 5.0044 5.1534
PROPANE 1.8874 1.8843 1.9397
I-BUTANE 0.3960 0.3962 0.4275
N-BUTANE 0.6043 0.6037 0.6530
I-PENTANE 0.1813 0.1867 0.1821
N-PENTANE 0.1540 0.1560 0.1489
N-HEXANE 0.0861 0.0875 0.0932
Methyl Cyclopentane 0.0152 0.0152 0.0163
Cyclohexan 0.0118 0.0118 0.0123
N-HEPTANE 0.0600 0.0601 0.0619
Methyl Cyclohexane 0.0150 0.0151 0.0155
N-OCTANE 0.0323 0.0314 0.0317
N-NONANE 0.0131 0.0121 0.0121
N-DECANE 0.0049 0.0042 0.0042
N-C11 0.0015 0.0011 0.0011
N-C12 0.0028 0.0017 0.0017
H 2S 2.0472 1.0253 0.4744

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Feed Gas to AGR
Case 2% H2S 1%H2S 0.46% H2S
Component Mol % Mol % Mol %

COS 0.0021 0.0010 0.0003
C1-SH 0.0102 0.0103 0.0044
C2-SH 0.0192 0.0190 0.0085
C3-SH 0.0026 0.0025 0.0017
C4-SH 0.0006 0.0006 0.0003
C5+-Mercaptane/Thiophene 0.0006 0.0006 0.0002
Benzene 0.0119 0.0120 0.0128
Toluene 0.0072 0.0070 0.0073
Xylene 0.0040 0.0038 0.0038
1) 1) 1)
H 2O
Total 100.0000 100.0000 100.0000
o
Temperature, C 40 40 40
Pressure, bar a 68.4 68.4 68.4
Flow Rate (dry basis), kmol/h 72,799.0 72,682.0 72,259.0
1)
Feed gas is saturated at 68.4 bar a. and 35°C.
Table 3 Mercaptane Gas to Claus
Mercaptane Gas to Claus*

Case 2% H2S 1%H2S 0.46% H2S
Component kmol/h kmol/h kmol/h

CO2 0.00 0.00 0.00
N2 1.97 1.89 0.86
He 0.00 0.00 0.00
METHANE 24.15 23.19 10.56
ETHANE 2.58 2.47 1.13
PROPANE 0.00 0.00 0.00
I-BUTANE 0.00 0.00 0.00
N-BUTANE 0.00 0.00 0.00
I-PENTANE 0.00 0.00 0.00
N-PENTANE 0.00 0.00 0.00
N-HEXANE 0.00 0.00 0.00
Methyl Cyclopentane 0.00 0.00 0.00
Cyclohexan 0.00 0.00 0.00
N-HEPTANE 0.00 0.00 0.00
Methyl Cyclohexane 0.00 0.00 0.00
N-OCTANE 0.00 0.00 0.00
N-NONANE 0.00 0.00 0.00
N-DECANE 0.00 0.00 0.00
N-C11 0.00 0.00 0.00
N-C12 0.00 0.00 0.00

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H 2S 0.00 0.00 0.00
COS 0.00 0.00 0.00
C1-SH 7.45 7.45 3.20

C2-SH 13.96 13.80 6.17
C3-SH 1.90 1.85 1.26
C4-SH 0.46 0.43 0.25
C5+-Mercaptane/Thiophene 0.45 0.41 0.17
Benzene 0.00 0.00 0.00
Toluene 0.00 0.00 0.00
Xylene 0.00 0.00 0.00
H2O (V) 4.15 3.98 1.81
Total (kmol/h) 58.56 56.22 25.60
o
Temperature, C 49.0 49.0 49.0
Pressure, bar a 1.65 1.65 1.65
Flow Rate (wet basis), kmol/h 58.56 56.22 25.60
* The given mercaptan streams and conditions shall be basis of design for SRU. Condition and
composition shall be adjusted by licensor of Dehydration & Mercaptan Removal Unit (Unit 03) later.
Mercaptan stream fluctuation shall be within !"$#%&'(*)

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4.2 PRODUCT SPECIFICATION
SWEET GAS
The purified and conditioned product gas to be send to the DMR unit has the following properties:
Quality:
H2S content (ppm vol) 2.0 (guaranteed value)
CO2 content (ppm vol): 10.0 (guaranteed value)
COS content (ppm vol): 1.0 (guaranteed value)
Methyl Mercaptan content (ppm vol): 75.0 (expected value)
Ethyl Mercaptan content (ppm vol): 140.0 (expected value)
Pressure (bar a.): 67.2

Temperature (°C): 50.0
LIQUID SULPHUR
Quality:
Purity (dry basis): ≥ 99.8 %
1)
H2S: ≤ 10 ppm wt
Ash: ≤ 300 ppm wt.
Organics: ≤ 500 ppm wt.
Color: Bright yellow
1) The H2S content of the liquid sulphur can only be guaranteed with a Degassing unit included in the
package.
INCINERATOR OFF GAS

The off gas from the Sulphur Recovery unit is incinerated and routed via stack to atmosphere.
After incineration, the residual H2S content will be the following:
Quality:
The sulphur compounds (H2S, COS, CS2) in flue gas will be less than 50 mg/Nm³ and CO is less than
3
5000 mg/Nm .

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4.3 SULPHUR RECOVERY

(1) Sulfur recovery rate design
The total sulfur recovery rate shall be based on the feed gas to AGRU plus SO2 feed to SRU (Total
Sulfur Feed). The overall sulfur recovery achieved in SRU shall be >99.0%.
(2) Sulfur recovery guarantee
The total sulfur recovery shall be guaranteed as more than 99.0% of the sulfur contained in the Total
Sulfur Feed. Sulfur recovery shall be calculated using the following equation ;
Percent Sulfur Recovery = 100 (X-Y) / X

Where:
X is Total Sulfur feed
Y is Total Sulfur Flow in Incinerator Flue Gas (Unit 09)
The sulfur recovery guarantee shall be based upon the maximum mercaptan co-absorption by the
Acid Gas Removal Unit (Unit 02) solvent specified by AGR Licensor. The mercaptan (RSH) removed
in Unit 02 will be fed to the AGE and processed to the TGTU Hydrogenation Reactor. Non-converted
mercaptans will be released to Incinerator.
*)
Mercaptan Species Co-Absorption Rate
C1SH 50 %
C2SH 40 %
C3SH 15 %
C4SH 10 %
C5SH+ 10 %
*): Max. expected co-Absorption rate in AGR (Unit 02).
(3) Lurgi shall prepare the plant overall sulfur material balance for all feed gas cases to account for all
the sulfur entering the AGRU. Material balance data for facilities outside of Lurgi scope will be
provided by Chiyoda.

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4.4 TURN DOWN

The overall unit is designed for processing the amount of gas specified in chapter 3.1. For the turn down
this gas capacity is defined as 100%. The turn down ratio of the unit is 40% of the design gas capacity.

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4.5 UTILITIES
Any revision to this document must be mutually agreed upon.
Table 4 Utility Conditions
Operation Design
pressure p [bar g.] / P gauge T
temperature t [°C]
Consumer [barg] [°C]
p t
5)
HHP Steam 62/61 440/430 69 72 & FV 470.0
5) 2)
HP Steam 25.0/25 226/226 28.0 & FV 255.0
5)
MP Steam 10.0/9.5 210/205 12.5 & FV 240.0
5)
LP Steam 4.5/4.1 165/160 7.0 & FV 195.0
6)
Condensate System
HP Condensate 4.1 153 7 & FV 195
MP Condensate 4.1 153 7 & FV 195
LP Condensate 1 120 3.5 & FV 180
BFW System
BFW 28.0 80 120.0 35.0 127 148.0
Demin Water System
Demineralized Water 2.7 amb 8 45
3)
Cooling Water Supply 4.0 Max. 38 10 & FV 55.0
min. 3.0 Min. 18
4) 3)
Cooling Water Return Max. 48 10 & FV 55.0
Service Water 5 amb 15 45
Instrum. Air System 7.5 / amb 10 70
min. 4.5
Nitrogen System 7.3 amb. 10 70
Boil Off Gas (BOG) 29.0 36.5 ~ 35 100
43.5
End Flash Gas (EFG) 5.0 36.5 ~ 10.4 100
43.5
for Incinerator Burner
Residue Gas 65.8 36.5 ~ 76 100
43.5
FV = Full Vacuum
amb = ambient Temperature

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Note
1) to be fixed / confirmed by client and/or FEED contractor
2) HP steam is generated and consumed in SRU only. The condition of HP steam shall be specified by
SRU Licensor.
3) FV for aboveground only
4) Maximum pressure loss 1 bar
5) Blow down shall be routed to B.L at operating temperature of steam producer.
6) Condensate will be saturate to B.L. pressure
Condensate recovery system (piping, pump, cooler(s), vessels) outside Licensor’s scope
BFW
Composition:
1)
Total solids; dissolved: 3 (mg/l)
2)
2 (mg/l)
Silica as SiO2 0.00 (mg/l)
Dissolved oxygen as O2: 0.007 (mg/l)
Physical Properties:
1)
Conductivity: 6 microS/cm
2)
4 microS/cm
0
pH range (at 20 C): 9.0 to 9.5
DEMINERALIZED WATER
Composition:
Total solids; dissolved: 5.0 mg/l
Total alkali and other metals: 0.5 mg/l
Silica as SiO2 0.00 (mg/l)
Physical Properties:
0
pH range (at 20 C): 6.5 to 7.5
Conductivity (at 25 °C): < 0.05 micro S/cm
Note:
1) Condensate Max. Loss Case
2) Normal Operational Case

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BOIL OFF GAS (BOG)
Boil off Gas from B.L.

Composition (Mole %) :
Methane: 90.1607
Ethane: 0.0103
Propane: 0.000
CO2 : 0.000
Nitrogen: 9.829
Helium: 0.000
END FLASH GAS (EFG)
End Flash Gas from B.L.

Methane: 57.8669
Ethane: 0.0102
Propane: 0.0000
CO2 : 0.0000
Nitrogen: 42.1136
Helium: 0.0093
RESIDUE GAS
Residue Gas from B.L.

Methane: 89.0442
Ethane: 5.2440
Propane: 0.0114
CO2 : 0.0010
Nitrogen: 5.6452
Helium: 0.0542

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ELECTRICAL
The main power shall be generated at SITE at 11000V, 3PH, 50Hz with a power factor of 0.8 lagging
using GE Frame 7EA (HOLD) Gas Turbine sets

Table 5 Supply Conditions Electrical Power

Range Voltage Phase Hertz
Motor up to 0.2 kW 240 1 50
> 0.20 & < 149 kW 415 3 50
> 149 kW 6600 3 50
Instrument Power 120 1 50

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4.6 METEOROGICAL DATA
AIR TEMPERATURE (DRY BULB)
Minimum temperature (dry bulb) 4 °C (Winter)

Maximum temperature (dry bulb) 49 °C (Summer)
AIR BAROMETRIC PRESSURE
Average: 1.103 013 bar

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4.7 ADDITIONAL DESIGN INFORMATION
FLARE:
Back pressure of flare system at battery limits: Wet Gas Flare: 6 barg
Acid Gas Flare: 0.1 barg
AIR DATA FOR INLET BLOWER DESIGN
max. Temperature: 49 °C in summer

min. Temperature: 4 °C in winter
Pressure: 1.013 bar a.
Relative humidity 59 % (mean daily – design basis)
80 % (mean daily max. – for information purpose only)
DATA FOR AIR COOLERS DESIGN
Air cooling shall be maximized

An air inlet stream maximum temperature of 43°C to Air Fin Coolers should be selected. The minimum
temperature is 4°C.
PRESSURE REFERENCE
Liquid pressures, given in chapter 4, are referenced to grade.

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DESIGN REQUIREMENTS FOR EQUIPMENT
For design criteria of columns, vessels, heat exchangers, tanks, pumps and compressors refer to
following Doc.-No. by client

QG II/24/09/PR/DP/NA/001 Technical Requirement for Sulphur Recovery Unit
QG II/20/09/PR/TS/NA/001 Technical Specification for Design & Fabrication of Sulfur Recover Units
In the event of a conflict between this specification and any one of the Process Licensor’s sizing/design
criteria Licensor’s criteria shall prevail.
OVERPRESSURE PROTECTION AND RELIEF PHILOSOPHY

For overpressure protection, flare and vent philosophy refer to following Doc.-No. by client
QG II/20/00/PR/DP/NA/001 Overpressure Protection, Flare and Vent Philosophy
In the event of a conflict between this specification and any one of the Process Licensor’s sizing/design
criteria Licensor’s criteria shall prevail.

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FOULING FACTORS
Medium m2 • K
Fouling Factor ( )
W
Process Gases Feed Gas 0.00018
Clean Gas 0.00018
Regeneration Gas 0.00018
Sour Gas 0.00036
Claus/TGT Process Gas 0.00260
Process Liquids Process Water 0.00010

Process Liquids in Plate H. E. 1)
Rich /Lean Amine Solution 0.00036
Liquid Sulphur 0.00026
2)
Utilities HP Steam 0.00010
2)
MP Steam 0.00010
2)
LP Steam 0.00010
2)
Boiler Feed Water 0.00026
2)
Cooling Water 0.00018
2)
Ambient Air for Air Cooling 0.00026
Remarks:
1) Overdesign = 20% (added to clean surface)
2) To be defined / confirmed by Consultant / Client

Qatargas II LNG 71707-02 00010 23 / 36 2
5 Engineering documents
All engineering documents will be issued for one train only.

In general the documents will show:
+
Lurgi symbol
+
Job name: Qatargas II LNG
+
Revision no. (0,1, …. as revision index for Lurgi)
+
Project no. (71707-02-GWR for Lurgi project no.)
+
Lurgi document no.
+
Empty fields for Client and Consultant document no.
For reference for the lay out of documents please refer to this document.
Note:
When the documents for Train-1 are identical and only equipment, piping, instrument numbering are
different, use as a common document with the following note:
TYPICAL FOR
ONE SRU TRAIN

Qatargas II LNG 71707-02 00010 24 / 36 2
6 Numbering
The following numbering procedures refers to the documents:

QG II/20/00/PE/PC/NA/301 Document Numbering Procedure
QG II/20/00/PE/PC/NA/303 Equipment / Line / Instrument Numbering Procedure
6.1 UNIT NUMBERING
The unit numbering will be as follows:
Table 6 Unit Number

Unit-No. Description Abbreviation
09 CLAUS CLS
09 Tail Gas Treatment + Acid Gas Enrichment TGT
09 Sulphur Degassing DEG
09 Incineration INC
02 aMDEA Acid Gas Removal AGR

Qatargas II LNG 71707-02 00010 25 / 36 2
6.2 EQUIPMENT NUMBERING
The equipment numbering will be as follows:
2 4 - E M 0 2 3 3 A
1 2 3 4 5
1: 2 digits – System Code (“24”; for LNG Process Train 4)

2: 2 letters - Equipment Class (Refer to Table 7)
3: 2 digits – Unit Code (“02” for aMDEA, “09” for AGE, SRU, TGT, Degassing)
4: 2 digits – Serial Number (For first SRU train only numbers from 0901…..0929 should be used)
5 1 digits – Sequential Number (“A”, “B” for parallel equipment; “1”, “2” for serial equipment)
Table 7 Equipment Class

Code Description Code Description
A Pond, Basin; Concrete Pit P Pump
B Boiler PD Pump Diesel Engine
C Column PM Pump Motor
D Desuperheater S Filter
E Heat Exchanger T Tank, Pit Silo, Hopper
EM Air Cooled Exchanger Motor V Reactor / Vessel / Drum
F Furnace WE Workshop Equipment
FL Flare X Miscellaneous
G Electrical Generator XC Crane
GD Generator Diesel Engine XH Steel Structure, Shelter
GT Generator Turbine XK Building, Loading Station
H Electrical Heater XM Mixer
K Compressor / Blower XP Portable Equipment
KM Compressor Motor XZ Fire and Safety Equipment
KT Compressor Gas Turbine Y Package Unit
KD Compressor Diesel Engine YH HVAC Equipment for Structure
L Loading Arm YK HVAC Equipment for Building
LB Liquid Burner

Qatargas II LNG 71707-02 00010 26 / 36 2
6.3 PROCESS STREAM NUMBERING
Process streams in the PFD and material balance table will be numbered as follows:
2 4 0 9 1 0 1
1 2 3

2: 2 digits - Unit Code (“02” for aMDEA, “09” for AGE, SRU, TGT, Degassing)
3: 3 digits - Sequential stream number, starting with incoming streams to the PROCESS, followed by
outgoing streams from the process; internal streams of the PROCESS will be then numbered in a
process relevant sequence.
6.4 NUMBERING OF PIPING
C W 2 4 0 0 0 0 1 - 1 0 “( 6 R 3 B S )- 1 ( - 4 0 )( 2 4 )
1 2 3 4 5 6 7 8
1: 2 letters – Line Service Code (Refer to Table 8)

2: 2 digits - System Code (“24”; for LNG Process Train 4)
3: 5 digits - Sequential Line Number (See Below)
4: Max. 2 digits - Line Size (Inch)
5: Max. 7 digits and letters - Line Class (See Below)
6: 1 letter - Insulation Code (Refer to Table 14)
7: Normal operating temperature (to be specified during detail engineering)
8: Insulation thickness (to be specified during detail engineering)
Sequential Line Number
0 0 0 0 1
1 2
1: 2 digits – Unit Code (“02” for aMDEA, “09” for AGE, SRU, TGT, Degassing)
2: 3 digits – Serial Number (001 through 999)

Qatargas II LNG 71707-02 00010 27 / 36 2
Piping Material Service Class
1 P 3 K L C 1
1 2 3 4 5 6
1: 1 digit - ANSI Class Code (Refer to

Table 9)
2: 1 digit - Service (Refer to Table 12)
3: 1 digit - Corrosion Allowance Code (Refer to Table 11)
4: 2 letters - Material Code (Refer to Table 10)
5: 1 or 2 letters - Suffix (Optional), A, B, C, ……(Refer to Table 13)
6: 1 digit - Serial Number (Optional)

Qatargas II LNG 71707-02 00010 28 / 36 2
Table 8 Line Service Code
Description Code Description Code

Air A General Process P

Instrument Air IA Ethane ET
Service Air SA Propane Refrigerant PR
, ,
Nitrogen Refrigerant RF
Drain DR Liquefied Natural Gas LG
Chemical contaminated Water CS Natural Gas Liquid GL
, ,
Oily contaminated Water OW
Sanitary Sewer SY Liquid Blowdown BD
Non contaminated Water NW Dry Liquid Blowdown DB
Caustic Waste Water NS Wet Liquid Blowdown WB
, , , ,
Atmospheric Vent AV
, , , ,
Carbon Dioxide Gas CD Steam Condensate SC

Defrost Gas DG Sour Condensate SU
Fuel Gas FG Vacuum Condensate VC
Liquefied Petroleum Gas LP Process Condensate PC
Natural Gas NG High High Pressure Steam HHS
Nitrogen Gas N High Pressure Steam HS
Oxygen Gas OX Contaminated Condensate CC
Acid Gas AG Medium Pressure Steam MS
, ,
Low Pressure Steam LS
, ,
Amine Solvent SV
Glycol GW
, ,
Boiler Feed Water BW
Chemical CH Tempered Water TW
Caustic Soda NA Cooling Water Return HW
Dry Powder DP Cooling Water Supply CW
Methanol ME Demineralized Water DM
Liquid Sulfur SL Fire Water FW
, ,
Chilled Water Supply CHS
Chilled Water Return CHR
Brine Drain BR
Hot Oil HO Process Water PW
Fuel Oil FO Drinking Water DW
Hydraulic Oil HY Service Water SW
Lube Oil LO Sea Water Return SR
Seal Oil SO Sea Water Supply SS
Waste Water WW
, ,
Acid AC
Sour Gas Flare SF Desalinated Water (Raw Water) RW
Wet Gas Flare RV
, ,
Dry Gas Flare CV
, ,
Catalyst CA

Qatargas II LNG 71707-02 00010 29 / 36 2
Table 9 ANSI Class Code
Code ANSI Class

Blank Utility Service
1 150#
3 300#
6 600#
9 900#
X 1500#
Table 10 Material Code

Code Material
A NACE
B Low Temperature C.S.
JL 304L
JH 304H
KL 316L
M Hastelloy
R Aluminium
W Galvanized C.S
WA Cem. Lined C.S./FRP
Z CPVC
Blank Killed C.S
Table 11 Corrosion Allowance Code

Code Corrosion Allowance
0 0 mm
1 1.2 mm
3 3.0 mm
4 4.0 mm
Table 12 Pipe Service Code

Code Service
A Plant Air , Nitrogen
C Process MDEA, Feed Gas
P General Process
R Low Temp. Process
S Steam
T Steam Traced or Jacketed
W Water
Y Lube & Seal Oil
Z Instrument Air Circuits

Qatargas II LNG 71707-02 00010 30 / 36 2
Table 13 Suffix of Line Class
Code Description
S Stress Relieve
U B31.1
P B31.8 ( Stress Relieve)
B31.8 Slug Catcher ( Stress
Q
Relieved )
Blank Jacketed Piping
Table 14 Insulation Code

Description Code
, ,
Hot Insulation for Heat Conservation 1

Hot Insulation for Personnel Protection 2
Insulation for Sound Control with Heat Conservation 3
Insulation for Sound Control without Heat Conservation 4
Insulation for Heat Conservation with Steam Tracing S
Insulation for Heat Conservation with Electrical Tracing E
Insulation for Heat Conservation with Steam Jacketing J
Notes : For more details see QGII/20/00/SP/TS/NA/001 page 5 of 59
Line numbers shall be assigned

a) from individual equipment item to individual equipment item
b) from line to individual equipment item and vice versa, another number is required for the line
downstream of the equipment
c) from line to line (exceptions: control valve bypasses, block valve warm-up and equalizing
bypasses, safety/relief valve bypasses
d) from unique equipment to the same unique equipment, except level standpipes
e) from line or equipment to atmosphere, funnel, or closed drainage systems
f) A new line number is required when the pipe design condition can vary (e.g. downstream of the
control valve assembly) or when a new piping class is to be specified.
g) Line number shall be held up to the point where the line ends to the header or unit battery limit
block valve. All branches to and from header shall have an individual line number.

Qatargas II LNG 71707-02 00010 31 / 36 2
6.5 INSTRUMENT TAG NUMBER
2 4 D P L L 0 2 0 0 1
1 2 3 4 5 6 7

2: Max. 4 letters - Instrument Functional Code (Refer to Table 17)
3: 2 digits - Unit Number (“02” for aMDEA, “09” for AGE, SRU, TGT, Degassing)
4: 1 letter or 0 – Package number (Refer to Table 15)
5: Max. 2 digits - Sequential Loop Number (Refer to Table 16)
6: 1 letter - Suffix (Optional) for identical Package Units : A, B, C, …..
7: 1 letter or Blank – Suffix for Parallel Elements
Table 15 Package Number

Code Description
0 Not for Package Unit
A to W Package Number
For SRU Unit
st
X 1 1% Block
nd
Y 2 1% Block
rd
Z 3 1% Block
Table 16 Sequential Number Range Assignment for Instrument Tag Number
Unit No Facilities Sequential Number

02 AGR 01 – 99
09 SRU 01 – 99

Qatargas II LNG 71707-02 00010 32 / 36 2
Table 17 Instrument Functional Code
First Letter Succeeding Letters

MEASURED OR MODIFIER READOUT OR OUTPUT FUNCTION MODIFIER

INITIATING PASSIVE
VARIABLE FUNCTION
A ANALYSIS ALARM
B BURNER USER'
S CHOICE USER'
S CHOICE USER'
S CHOICE
CUMBUSTION
C USER’S CHOICE CONTROL
D DENSITY DEVIATION
E VOLTAGE SENSOR
(PRIMARY
ELEMENT)
F FLOW RATE RATIO (FRACTION)
G FIRE & GAS GLASS, VIEWING
DEVICE
H HAND HIGH
I CURRENT INDICATE
(ELECTRICAL)
J POWER SCAN
K TIME, TIME - TIME RATE OF CONTROL STATION
SCHEDULE CHANGE
L LEVEL LIGHT LOW
M USER’S CHOICE MOMENTARY MIDDLE OR
INTERMEDIATE
N USER'
S CHOICE. USER'
S CHOICE USER'
S CHOICE USER'
S CHOICE
O USER'
S CHOICE ORIFICE OPEN
P PRESSURE, POINT (TEST)
VACUUM CONNECTION
Q QUANTITY INTEGRATE, INTEGRATE,
TOTALIZE TOTALIZE
R RADIATION RECORD
S SPEED, SAFETY SWITCH
FREQUENCY
T TEMPERATURE TRANSMIT
U MULTI VARIABLE MULTIFUNCTION MULTIFUNCTION MULTIFUNCTION
V VIBRATION VALVE, DAMPER,
MECHANICAL OR LOUVER
ANALYSIS
W WEIGHT, FORCE WELL
X UNCLASSIFIED X-AXIS UNCLASSIFIED UNCLASSIFIED UNCLASSIFIED
Y EVENT, STATE OR Y-AXIS RELAY, COMPUTE
PRESENCE OR CONVERT
Z POSITION, Z-AXIS TRIP/SHUTDOWN
DIMENSION
pH PH

Qatargas II LNG 71707-02 00010 33 / 36 2
1. The functional identification of an instrument shall consist of letters shown above, and shall include
first letter covering the measured or initiating variable, and one or more succeeding letters covering
the functions of the individual instrument, one or more readout or passive functions, or output
function, or both.
2. Modifying letters may modify either a first-letter or other succeeding letters, as applicable.
3. The sequence of identification letters shall begin with a first-letter. Readout or passive functional
letters shall follow in any sequence and output functional letters shall follow these in any sequence
except that output letter C (control) shall precede output letter V (valve); e.g. HCV, a hand-actuated
control valve. However, modifying letters, if used, shall be interposed so that they are placed
immediately following the letters they modify.
4. Any first-letter, if used in combination with modifying letters D (differential), F (ratio) or Q (integrate or
totalize), or any combination of them shall be construed to represent a new and separate measured
variable and the combination shall be treated as a first letter entity.
6.6 ELECTRICAL IDENTIFICATION
Hold

Qatargas II LNG 71707-02 00010 34 / 36 2
7 UNITS OF MEASUREMENT
Table 18 Units of Measurement

Temperature °C
Pressure bar
Mass Kg
Length mm or m
Mass Flow kg/h
Volumetric Flow, Vapour Standard m³/h at 0°C
Volumetric Flow, Liquid m³/h @ operating conditions
Density, Liquid , actual kg/m³
Density, Vapour kg/m³
Viscosity mPas
Heat Capacity kJ/kgK
Thermal Conductivity W/mK
Surface Tension mN/m
Molecular Mass kg/kmole
2
Fouling coefficient m K/W
Enthalpy kJ/kg
Heat Rate kW or MW

Qatargas II LNG 71707-02 00010 35 / 36 2
Rev. Prepared, revised Checked Approved Remark, kind of revision
LF/PS Name Date Name Name Date Status
0 LF Jue 17.10.03 DrTo Shml 17.10.03 FI First Issue

1 LF Jue 01.12.03 DrTo Shml 01.12.03 1 Revision by Client

2 LF Jue 30.01.04 DrTo Shml 30.01.04 2 Revision and Completion by Client
3
4

Qatargas II LNG 71707-02 00010 36 / 36 2

Basis of Design For Basic Process Engineering of Omnisulf

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71707-02-GWR

Process Engineering Qatargas II LNG

event of the grant of a patent or the registration of a utility model or design.

BASIC PROCESS ENGINEERING

OWNER PROJ.NO. OWNER DOCUMENT NO REV.

CONTR. PROJ.NO. CONTRACTOR DOCUMENT NO REV.

Jue 17.10.03 DRTO BE

Project Name Project No. Document No. Sheet / of Revision

event of the grant of a patent or the registration of a utility model or design.

Project Name Project No. Document No. Sheet / of Revision

event of the grant of a patent or the registration of a utility model or design.

No. Title Summary of Revisions

QG II/2000/PR/TS/NA/003 Supplement Requirement for Lurgi/BASF Scope of C4

Project Name Project No. Document No. Sheet / of Revision

event of the grant of a patent or the registration of a utility model or design.

Project Name Project No. Document No. Sheet / of Revision

event of the grant of a patent or the registration of a utility model or design.

2.1 PROCESS DESCRIPTION

CLAUS - Unit 09 - CLS

TAIL GAS TREATMENT and ACID GAS ENRICHMENT - Unit 09 - TGT

Project Name Project No. Document No. Sheet / of Revision

event of the grant of a patent or the registration of a utility model or design.

INCINERATOR - Unit 09 - INC

Sulfur Degassing – Unit 09 - DEG

Project Name Project No. Document No. Sheet / of Revision

event of the grant of a patent or the registration of a utility model or design.

Figure 1 Block Flow Scheme

DMR Product Gas

Raw Gas Condensate Mercaptan Gas Fuel Gas

Acid Gas Rich Flexsorb / AGE

SO2 Rich Acid Gas Incinerator

Project Name Project No. Document No. Sheet / of Revision

event of the grant of a patent or the registration of a utility model or design.

3.1 DEFINITION OF BATTERY LIMITS

Project Name Project No. Document No. Sheet / of Revision

event of the grant of a patent or the registration of a utility model or design.

Table 1 Main Feed/Product Conditions

Feed Process Stream Product Process Stream

Battery limit conditions of other product streams

Operating Condition Mechanical Design

Project Name Project No. Document No. Sheet / of Revision

event of the grant of a patent or the registration of a utility model or design.

4.1 UNIT CAPACITY AND FEED GAS CONDITION AND COMPOSITION

Case H2S content Purpose

Table 2 Raw Gas

Feed Gas to AGR

Component Mol % Mol % Mol %

Project Name Project No. Document No. Sheet / of Revision

event of the grant of a patent or the registration of a utility model or design.

Component Mol % Mol % Mol %

Table 3 Mercaptane Gas to Claus

Mercaptane Gas to Claus*

Component kmol/h kmol/h kmol/h

Project Name Project No. Document No. Sheet / of Revision

event of the grant of a patent or the registration of a utility model or design.

C1-SH 7.45 7.45 3.20

Project Name Project No. Document No. Sheet / of Revision

event of the grant of a patent or the registration of a utility model or design.

Pressure (bar a.): 67.2

INCINERATOR OFF GAS

Project Name Project No. Document No. Sheet / of Revision

4.3 SULPHUR RECOVERY

(1) Sulfur recovery rate design