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International Journal of Mineral Processing 136 (2015) 2–6

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International Journal of Mineral Processing


journal homepage: www.elsevier.com/locate/ijminpro

Size specific energy (SSE)—Energy required to generate minus 75


micron material
Grant R. Ballantyne a,b,⁎, Wolfgang Peukert c, Malcolm S. Powell a,b
a
The University of Queensland, Sustainable Minerals Institute, Julius Kruttschnitt Mineral Research Centre, 40 Isles Road, Indooroopilly, Brisbane, QLD 4068, Australia
b
CRC ORE: Optimised Resource Extraction, The University of Queensland, Level 7, Sir James Foots Building, St Lucia, QLD 4072, Australia
c
Institute of Particle Technology, Friedrich-Alexander University Erlangen-Nuremberg, Cauerstrasse 4, D-91058 Erlangen, Germany

a r t i c l e i n f o a b s t r a c t

Article history: This paper explores the relationship between energy and the generation of minus 75 micron material. Rittinger's
Received 13 December 2013 law of comminution states that the energy input is proportional to the generation of new surface area. An accu-
Received in revised form 27 August 2014 rate and consistent measurement of surface area, applicable across multiple size ranges, is required to apply this
Accepted 24 September 2014
practically. The amount of new −75 μm material generated has previously been proposed as a proxy for surface
Available online 2 October 2014
area. This has been demonstrated to some extent on a range of different laboratory equipment, but not in a man-
Keywords:
ner suited to equipment-independent ore characterisation. To this end the JK Rotary Breakage Tester (JKRBT) and
Comminution Schönert breakage device have been used to measure the progressive production of fines from cumulative single
Energy impacts starting with 37.5 mm particles down to 250 μm. As per expectation, the generation of −75 μm material
Efficiency was found to be proportional to the specific energy, but there was a secondary influence of size. A model was de-
Benchmarking veloped to describe the breakage and it was found that the standard t10 relationship could be used to effectively
calculate the size specific energy. Measuring the intrinsic competence of an ore in this way can then be used to
assess the energy efficiency of full-scale mills in relation to a lab scale test. It is envisaged that this relationship
also has the potential to be used in the design of new comminution circuits. The methodology and the results
from its application are presented for discussion and review.
© 2014 Elsevier B.V. All rights reserved.

1. Introduction probability of internal flaws and weaknesses (Napier-Munn et al.,


2005; Wang and Forssberg, 2007).
The relationship between energy and size reduction is of primary This paper proposes the use of the energy required to produce new
importance in the field of comminution. Rittinger (1867) was credited − 75 μm material (hereafter referred to as size specific energy or SSE
as proposing that the work done in crushing is proportional to the after (Powell et al., 2003–2010)) as a simplified measure across a
area of new surface produced. Just 18 years later, Kick (1885) proposed broader range of particle sizes. Hukki (1979) first introduced this
that for a homogeneous rock, the work input is proportional to the method to characterise the efficiency of closed grinding circuits. Later,
reduction in particle. Bond (1952) proposed the third theory, a compro- Levin (1992) argued that the energy required to generate −75 μm ma-
mise between the two earlier relationships, originally thought to infer terial could be used as a competence measurement, providing similar
proportionality with the length of new crack formation. Walker results to the Bond work index. More recently, Hilden and Suthers
(1937) and later Hukki (1961) found that these three laws may not be (2010) found the linear relationship between energy and per cent
mutually exclusive and are each applicable within a specific size −75 μm to hold true over a wide range of machines, from crushing to
range. Tavares and King (1998) proved experimentally that Kick's as- ball milling (see Fig. 1). Musa and Morrison (2009) found that typically
sumption is valid at large sizes where the surface energy is negligible 70 to 80% of the surface area of mill product existed below 75 μm. The
compared to the internal energy required for breakage. The results of 75 μm proxy has no intrinsic value. For circuits producing a much finer
Griffith (1921) have more recently been used to relate the increase in (or coarser) product, a finer (or coarser) proxy size may be more appro-
energy required to break smaller particles with the reduction in the priate. They also found that the total surface area measured from coarse
to fine was well enough limited at the fine end to justify the original
Rittinger hypothesis that comminution energy generates new surface
area—albeit not very efficiently. Therefore, the theory behind size specific
⁎ Corresponding author at: The University of Queensland, Sustainable Minerals
Institute, Julius Kruttschnitt Mineral Research Centre, 40 Isles Road, Indooroopilly,
energy may be related to the original Rittinger hypothesis.
Brisbane, QLD 4068, Australia. Tel.: +61 7 3365 5839; fax: +61 7 3365 5999. Currently, the standard method for calculating comminution unit
E-mail address: g.ballantyne@uq.edu.au (G.R. Ballantyne). energy efficiency is the ratio of operating work index and the Bond

http://dx.doi.org/10.1016/j.minpro.2014.09.010
0301-7516/© 2014 Elsevier B.V. All rights reserved.
G.R. Ballantyne et al. / International Journal of Mineral Processing 136 (2015) 2–6 3

100%
2. Method
90%
Fines generated (%-75µm)

80% The relationship between input energy and generation of −75 μm


y = 0.0228x + 0.3312
70% material was tested using controlled single particle impacts. Two
60% Australian copper–gold ores were tested and the feed particle sizes
y = 0.054x
50% started at 37.5 mm and reduced to 250 μm over successive steps of
40% y = 0.0407x breakage. The JKRBT was used for breaking particles larger than
30%
4.75 mm with accurate input energies (Shi et al., 2006). Breakage of
smaller particle sizes was achieved with the Schönert breakage device
20% Hilden and Suthers (2010)
at Erlangen Institute of Particle Technology (Vogel and Peukert, 2005).
10% Levin (1992) This equipment is able to break particles in the size range 4.75 mm to
0%
0 5 10 15 20 25 30
250 μm within a vacuum of 20 mbar, thus reducing errors associated
with air-drag on the particles. Both machines utilise a spinning internal
Specific energy (kWh/t)
rotor to propel the particles outward, impacting with a stationary anvil
Fig. 1. Published size specific energy data.
ring (Fig. 3).
The specific kinetic energy (kWh/t) of the particle before impact was
determined by half the velocity of the particle squared. Theoretically,
work index. This gives an indication of the efficiency of the milling cir- when the particle exits the rotor, its tangential and radial velocity com-
cuit in relation to the Bond (1952) standard crush, rod and ball mill cir- ponents equal the tip speed. However, in practice the transfer of energy
cuit. Observed and predicted specific energy calculations are displayed is not 100% efficient. For the JKRBT, these calibration factors have been
in Fig. 2. The styles of the data points correspond to different databases. established through high-speed video analysis (Shi et al., 2006). Dis-
Filled data points were collated from the database published by crete element modelling (DEM) was used to calculate the factors for
Ballantyne and Powell (2014) and the unfilled data points were pub- the Schönert breakage device. Analysis of the DEM simulations allowed
lished in Morrell (2004). Sixty percent of the mines analysed had overall the velocity efficiency to be calculated for a range of particle sizes using
circuit efficiencies between 50 and 65%. These low efficiency values in- the following equation (Weerasekara, 2013):
dicated that there was great potential across the industry to improve ef-
ficiency of comminution equipment. However, when the efficiencies of Velocity efficiencyð%Þ ¼ 84:08−0:89  particle sizeðmmÞ ð1Þ
the autogenous and semi-autogenous grinding (AG/SAG) circuits and
the ball mill circuits were calculated a more complex underlying rela- The breakage testwork procedure started with 90 particles between
tionship was found. It is widely known that by calculating the energy ef- 37.5 and 26.5 mm and progressively comminuted these down through
ficiency using the Bond equation, AG/SAG circuits appear significantly root-2 size intervals to 100% passing 250 μm (Fig. 4). The methodology
less efficient. A number of researchers have attempted to account for was repeated for energy levels between 0.4 and 3.5 kWh/t. Due to the
this with a range of correction factors (Barratt and Allan, 1986; small diameter of the rotor, the maximum input energy for the Schönert
Rowland, 1988) and alternative power factors (Hukki, 1961; Morrell, breakage device was 0.8 kWh/t. Care was taken to minimise sample
2004). The underlying reason for the discrepancy is that the Bond equa- losses that can occur during this type of testwork. This justified the
tion requires parallel feed and product size distributions in log/log assumption that all the material lost during the experiment was dust
space. AG/SAG mills do not fit this assumption because they tend to pro- below 75 μm in size. On average this added 1.55% to the −75 μm figures.
duce a large amount of fines without reducing the sieve size that 80% of
the material passes (P80) significantly. Using the size specific energy to 3. Results
calculate the energy efficiency is more effective than the Bond equation
because it is related to the generation of fines, not the reduction in the Previous work has shown linear relationships between cumulative
top size. However, a standard test procedure is required for this to be comminution energy consumption and material generated below
achieved (Musa and Morrison, 2009). The operating work index and 75 μm (Hilden and Suthers, 2010; Hukki, 1979; Levin, 1992; Musa and
size specific energy were found to be linearly related in the database Morrison, 2009). The results from this investigation have found
published by Ballantyne et al. (2012). This linear relationship suggests that the generation of − 75 μm is dependent on more than simply
similarity in the measurement of rock competence between the two the input energy. The results for one of the two samples (Ore 1) are
methods. However, this may have been a result of the similar circuits
across the sampled mines, because this would not be so if the gradient
of the size distributions in log–log space changed.

40

35

30
Observed kWh/t

Combined
25

20
AG/SAG
15

10 Ball

0
0 5 10 15 20 25
Bond predicted kWh/t

Fig. 2. Comminution energy efficiency calculated using ratio between operating and Bond Fig. 3. Rotor/anvil configuration for both JKRBT and Schönert breakage device (Tavares,
work indices (unfilled data points from Morrell (2004)). 2007).
4 G.R. Ballantyne et al. / International Journal of Mineral Processing 136 (2015) 2–6

25% Ore 2
y = 0.09x

Cumulative generation of-75 µm


20%

15% Ore 1
y = 0.04x

10%

5%

0%
0 1 2 3 4
Cumulative specific energy (kWh/t)

Fig. 6. Combined progressive generation of −75 μm.

mines corresponding to ore 1 and 2 being 74% and 43% efficient


respectively.
The cumulative generation of − 75 μm material displayed a slight
non-linear relationship. To investigate this deeper, the results were
Fig. 4. Simplified testwork workflow. The Schönert breakage device replaced the JKRBT
below 4.75 mm. analysed independently for each feed particle size. This technique re-
vealed that the generation of −75 μm material increased with decreas-
ing particle size. The cause of this trend is that the marker size of 75 μm
displayed in Fig. 5. The sample was split into three and progressively corresponds to a smaller reduction ratio when the feed particle size is
comminuted in the JKRBT at 1, 2 and 3 kWh/t. The generation of reduced. Therefore, since the breakage function was found to be consis-
−75 μm material appeared relatively linear within each of these energy tent, smaller particles resulted in larger production of −75 μm material.
levels. The gradient of the relationship is consistent at different energy This phenomenon was explored further through the development of a
levels, but the y-intercept was strongly dependent on variability of the model to describe the breakage.
initial breakage event. Normalising the generation of − 75 μm after
the initial breakage event produced a linear relationship passing 4. Model development
through the origin. However, this analysis simply proved the similarity
of the gradients at different energy levels. A model was developed to describe the results generated through
When the breakage was extended to finer sizes using the Schönert the experimental programme. The model was based on the breakage
breakage device, the relationship visibly deviated from linearity. As (appearance) function developed by Narayanan and Whiten (1988)
the smaller particles were broken, the generation of −75 μm material and the modified Weibull (1939) distribution model developed by
for the same energy input increased. Vogel and Peukert (2005) and later modified by Shi and Kojovic
The results for the second ore are displayed together with the first (2007). Musa (2010) developed a similar technique to analyse the effi-
sample in Fig. 6. Ore 2 was less competent than ore 1, producing signif- ciency of breakage within crushers and mills. The degree of breakage
icantly more −75 μm material at the same input energy levels. The size was characterised using the t10 parameter which is defined as the per-
specific energy (SSE) for the sample is the inverse of the gradient of a centage of material passing through a screen size one tenth the size of
trendline forced to pass through the origin. For ore 1 and 2 the values the initial geometric mean particle size. The Shi and Kojovic (2007)
are 24.9 and 11.1 kWh/t−75 μm respectively. The scatter in the data re- model (Eq. (2)) was used to reduce the t10 data from different input
sults from a combination of ore variability, particle size effects and the energies and initial particle sizes to one master curve (Fig. 7).
relationship between impact velocity and specific energy. The SSE
values corresponded well with historical survey results from the two
mines. A comparison of the theoretical minimum energy measured
through single particle breakage and mine site SSE resulted in the t10 ¼ Mð1‐exp ½‐ f mat : x :ðEcs ‐E min ÞÞ ð2Þ

15% 70%
Cumulative generation of -75 µm

60%

50%
10%
40%
t10

30%

5% 20%

10%

0%
0% 0 0.2 0.4 0.6 0.8 1 1.2 1.4
0 1 2 3 4 Ecs.Fmat.x
Cumulative specific energy (kWh/t)
Fig. 7. Master curve showing the degree of breakage (t10) at different energy levels and
Fig. 5. Ore-type 1: progressive generation of −75 μm. initial particle sizes for ore 1.
G.R. Ballantyne et al. / International Journal of Mineral Processing 136 (2015) 2–6 5

100% 45

Size specific energy (kWh/t-75µm)


90% 40
t 1.2
80% 35
t2
tn (% passing)

70%
30 Ore 1
60%
t4 25
50%
t 10 20
40% t 25
15
30%
t 75 Ore 2
10
20%
t 150 5
10%
0% 0
0% 10% 20% 30% 40% 50% 60% 70% 0.1 1 10 100

Breakage Index, t10 (%) Initial particle size (mm)

Fig. 10. Relationship between initial particle size and size specific energy for both Ore 1
Fig. 8. Breakage (appearance) function for ore 1 in the form of the t-family of curves.
and 2. Error bars represent the standard deviation around the mean and the line is the
predicted size specific energy from the model.

where M represents the maximum t10 for a material subject to breakage,


fmat (1/kWh m) is the material breakage property, x (m) is the initial t-values. The accuracy of the interpolation function was improved by
particle size, Ecs (kWh) is the mass-specific impact energy, and Emin taking the log of the particle size. The goodness of fit for this model
(kWh) is the threshold energy. over the range of tests completed within this experimental campaign
Plotting of the degree of breakage (t10) parameter against the other is displayed in Fig. 9. The top and bottom end of the size distribution
reduction ratio parameters (t-family) provides the basis for determin- was predicted more accurately than the intermediate sizes. This is evi-
ing the whole size distribution from the t10 parameter (Narayanan dent in the wider scatter that is observable between the 30 and 70%
and Whiten, 1988). The results for ore 1 are displayed in Fig. 8. To enable passing figures.
a more accurate prediction of the progeny over a wide range of t10, t1.2 The model was tested to its limits by the predicting the size specific
and t150 values were added to the classic analysis. The t1.2 corresponds energy and its variability with initial particle size (Fig. 10). As alluded to
to the probability of breakage parameter as described by the proportion earlier, the %−75 μm corresponds to a larger t-value for coarser initial
of material that falls through the screen below in a root two sieve series. particle sizes. Therefore, since self-similar breakage is assumed in this
This technique provides a method for linking the results from low model, the size specific energy is smaller for finer initial particle sizes.
energy collisions where breakage probability is the dominant descriptor This trend matches the experimental data well across the wide range
and high energy impacts where t10 becomes dominant. A spline func- of initial particles sizes and energy levels. There is a sharp increase in
tion is fitted through five chosen points that cover the whole range the modelled SSE at the extreme coarse end of the distribution. In this
of t10 values. Using this technique, the whole t-family of curves can be range, 75 μm corresponds to large t-values and, the model under-
described by a 5 × 7 matrix. This analysis technique is able to effectively predicts the amount of −75 μm material generated.
describe the breakage progeny when self-similar breakage is apparent—
as evident in this case. 5. Discussion
Combining these t-family modelling techniques provides a robust
methodology for determining the progeny from single particle impact The SSE consumption is a useful metric for the determination of the
tests over a wide range of input energies and initial particle sizes. Dou- practical comminution energy efficiency. Thermodynamic milling
ble parabolic interpolation functions were used to calculate the t-values efficiencies are typically calculated as below 2%, a value so low as to
from the experimental size distributions, the t-values that corresponded be useless (Fuerstenau and Abouzeid, 2002). Determining the practical
to the fitted t10, and the per cent passing screen sizes between the given minimum SSE from single particle impact breakage will result in a much
more realistic and achievable efficiency benchmark. This can also be
100% measured easily by sampling at different points around the comminu-
R² = 0.992
tion circuit to troubleshoot where the inefficiencies enter the system.
The SSE calculation has a key advantage over the use of t10—it can be
80% found for single particle breakage as well as size distributions. Com-
pared to Bond's use of P80 it is more closely related to the surface area
production than top size reduction and doesn't rely on the assumption
% passing (observed)

of parallel feed and product size distributions.


60%
The SSE decreases with particle size—a result opposed to the tradi-
tional t10 approach. This highlights an inherent limitation in the calcula-
tion because the t10 changes with feed size, whereas the 75 μm marker
40% does not. A factor related to the tn of the marker size may help reduce
this effect, but may also affect the applicability of the results.

20% 6. Conclusion

Single particles from 37.5 mm to 250 μm were broken using impact


breakage—a wider range than previously attempted. This was achieved
0%
0% 10% 20% 30% 40% 50% 60% 70% 80% 90% 100% by combining coarse particle breakage data from the JKRBT with fine
% passing (predicted) particle breakage using the Schönert breakage device. A linear relation-
ship was observed between specific breakage energy and generation of
Fig. 9. Correlation between predicted and observed progeny size distributions obtained for −75 μm material for two ores comminuted via single particle impact.
ore 1. The inverse gradient of this relationship is the SSE (kWh/t− 75 μm)
6 G.R. Ballantyne et al. / International Journal of Mineral Processing 136 (2015) 2–6

which is a measure of the competence of an ore. This can be used as a Hilden, M., Suthers, S., 2010. Comparing energy efficiency of multi-pass high pressure
grinding roll (HPGR) circuits. International Mineral Processing Congress (IMPC),
benchmark and to provide a simple method for assessing the practical Brisbane, Australia.
comminution energy efficiency of full scale grinding circuits. It can be Hukki, R.T., 1961. Proposal for a solomonic settlement between the theories of von
used to assess energy efficiency of existing circuits, benchmark opera- Rittinger, Kick and Bond. AIME Trans. (mining) 220, 403–408.
Hukki, R.T., 1979. Fundamentals of the closed grinding circuit. Eng. Min. J. 180, 102–109.
tions internationally, measure productivity improvements and assess Kick, F., 1885. Das Gesetz des proportionalen Widerstands und seine Anwendug. In:
performance of individual equipment. Leipzig, F. (Ed.).
A simple model relating the t10 to input energy, feed size and the Levin, J., 1992. Indicators of grindability and grinding efficiency. J. South. Afr. Inst. Min.
Metall. 92, 283–290.
resulting t-family of curves was developed to validate the results. Morrell, S., 2004. An alternative energy–size relationship to that proposed by Bond for the
Using this model, the size specific energy was calculated proving that design and optimisation of grinding circuits. Int. J. Miner. Process. 74, 133–141.
the size specific energy is not independent from classical t10 analysis. Musa, F., 2010. Development of Methods to Assess the Efficiency of Comminution Devices
and Operations. Julius Kruttschnitt Mineral Research Centre. The University of
Using this analysis technique, it is also possible to assess the breakage
Queensland.
probability functions that were also previously thought of as indepen- Musa, F., Morrison, R., 2009. A more sustainable approach to assessing comminution
dent variables. efficiency. Miner. Eng. 22, 593–601.
Napier-Munn, T., Morrell, S., Morrison, R., Kojovic, T., 2005. Mineral Comminution
Circuits—Their Operation and Optimisation. Julius Kruttschnitt Mineral Research
Acknowledgements Centre, Brisbane.
Narayanan, S.S., Whiten, W.J., 1988. Determination of comminution characteristics from
single particle breakage tests and its application to ball mill scale-up. Trans. Inst.
The authors would like to acknowledge the support of CRC ORE, Min. Metall. Sect. C: Mineral Proc. Extraction Metall.) 97, C115–C124.
20090048 established and supported by the Australian Government's Powell, M., Morrison, R., Djordjevic, N., Hilden, M., Cleary, P., Owen, P., Govender, I.,
Cooperative Research Centres Program and all their sponsors who pro- Weerasekara, N., Michaux, S., Kojovic, T., Pokrajcic, Z., Musa, F., Sinnott, M., Mainza,
A., Bbosa, L., 2003–2010. Eco-efficient liberation: outcomes and benefits. In: Powell,
vided financial assistance for this research. We thank the research group M. (Ed.), Centre for Sustainable Resource Processing (CSRP).
at the Institute of Particle Technology at Erlangen University for their Rittinger, P.R., 1867. Lehrbuch der Aufbereitungskunde. Ernst and Korn, Berlin.
hospitality and the use of the Schönert breakage device. We thank Rowland, C.A., 1988. Diameter factors affecting ball mill scale-up. Int. J. Miner. Process. 22,
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JKTech management for their permission to access its database. Nirmal Shi, F., Kojovic, T., 2007. Validation of a model for impact breakage incorporating particle
W contributed DEM simulations for this work size effect. Int. J. Miner. Process. 82, 156–163.
Shi, F., Kojovic, T., Larbi-Bram, S., Manlapig, E., 2006. Development of a new breakage
characterisation device. JKMRC, AMIRA P9N, 5th technical report.
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