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Optical Materials
journal homepage: www.elsevier.com/locate/optmat
a r t i c l e i n f o a b s t r a c t
Article history: We propose a simple hollow-core circular lattice photonic crystal fiber (PCF) based surface plasmon
Received 23 October 2017 resonance (SPR) refractive index sensor. The sensing performance is investigated by using the finite
Received in revised form element method (FEM). Silver is used as the plasmonic material for this design, which is placed on the
23 December 2017
outer surface of the PCF to facilitate the fabrication. The proposed sensor shows a maximum wavelength
Accepted 25 December 2017
sensitivity of 4200 nm/RIU with a sensor resolution of 2.38 105 RIU. Besides, a maximum amplitude
sensitivity of 300 RIU1 and a resolution of 3.33 105 RIU is reported for an analyte refractive index of
1.37. Moreover, the effect of varying structural parameters on the sensing performance such as pitch, air
Keywords:
Surface plasmon resonance
hole diameter and silver layer thickness are also discussed thoroughly. Sensitivity analysis of the pro-
Photonic crystal fiber posed sensor is performed in order to investigate the impact on loss depth and amplitude sensitivity.
Refractive index sensor Thanks to high sensitivity and linearity characteristics, the proposed sensor can be potentially employed
Sensitivity in practical bio-sensing and chemical sensing applications.
Resolution © 2017 Published by Elsevier B.V.
1. Introduction air hole dimension, and number of air hole rings, it is possible to
operate the PCF sensor at the optimum condition. In contrast to
Over the last three decades, surface plasmon resonance (SPR) conventional optical sensors, PCF-based SPR sensors permit better
phenomenon has been highlighted as a powerful optical detection control of the evanescent field by varying the structural parame-
technique due to its highly sensitive behavior, and capability for ters. Moreover, the size of the PCF SPR sensors is small, making
label-free sensing [1,2]. SPR sensors have revealed impressive them suitable for nanosensors and remote sensing applications
progress in bio-sensing applications including biological analytes [19].
detection, medical diagnosis, bio-imagining, antibody-antigen Over the last few years, several PCF SPR sensors have been
interaction, organic chemical sensing, water testing, and environ- explored in order to improve the sensitivity, detection accuracy and
mental safety [3e7]. Due to ongoing development of SPR technol- dynamic range of detection. PCF SPR sensors are classified into two
ogy, it has been also employed in optoelectronic devices such as categories. First, internally metal-coated PCF sensors where plas-
film thickness monitoring [8,9], optical tunable filters [10,11], SPR monic material is selectively deposited inside the PCF and liquid
imaging [12,13], and optical modulators [14,15]. Additionally, SPR analyte is selectively infiltrated into the air hole(s). Second, exter-
technology permits integration of nanoelectronic and nano- nally metal-coated PCF sensors where plasmonic materials are
photonic components with the aim of obtaining ultra-compact deposited on the outer surface of the PCF. Very recently, a diamond
optoelectronic devices [16,17]. ring fiber (DRF) based SPR sensor has been proposed [20] showing
Recently, photonic crystal fiber (PCF) based SPR sensors have maximum wavelength sensitivity of 6000 nm/RIU and sensing
been extensively studied due to their unusual and appealing optical resolution of 1.67 105 RIU in the sensing range between 1.33 and
characteristics over the conventional optical fibers [18]. Due to 1.39. The open-ring channel-based sensor proposed by Liu et al.
controllable birefringence and confinement loss, PCF SPR sensors [21] can be used to detect low refractive index (RI) analyte between
have shown an improved performance in bio-sensing applications. 1.23 and 1.29. The proposed design shows average wavelength
For instance, by changing the structural parameters such as pitch, sensitivity of 5500 nm/RIU and maximum amplitude sensitivity of
333.8 RIU1.
Based on internal metal coating, few potential PCF SPR sensors
have been reported in Refs. [22e25]. In practice, deposition of
* Corresponding author.
E-mail addresses: rojy.ruet12@gmail.com (M.R. Momota), ruetrabu@gmail.com metal on several air holes while maintaining uniform thickness is
(Md.R. Hasan). unfeasible from the fabrication point of view. Moreover, selective
https://doi.org/10.1016/j.optmat.2017.12.049
0925-3467/© 2017 Published by Elsevier B.V.
288 M.R. Momota, Md.R. Hasan / Optical Materials 76 (2018) 287e294
infiltration of air holes with analyte is complex and time to investigate how sensing performance varies due to fluctuations
consuming. It potentially limits widespread applications in prac- of the fiber design parameters.
tical sensing applications. Recently, nanowire-based PCF SPR sen-
sors have been reported in order to eliminate the issues of selective
infiltration [26,27]. Very recently, a hollow-core silver nanowire- 2. Structural design and plasmonic materials
based PCF SPR sensor [28] has been proposed having large detec-
tion range from 1.33 to 1.50. The proposed sensor shows maximum Cross-section view of the proposed circular lattice PCF sensor is
wavelength sensitivity of 1800 nm/RIU when analyte index is var- shown in Fig. 1. There are two air-hole rings with four missing air
ied from 1.33 to 1.34. Recently, externally-metal-coated PCF SPR holes in the second ring. The size of the air holes in the second ring
sensors have gained increased attention because of their straight- is larger than first ring for obtaining better light confinement in the
forward detection and ease of fabrication. The PCF based SPR sensor desired direction [37]. In the first ring, air holes are arranged at 60
proposed by Hassani et al. was used for the detection of biolayer anticlockwise progressive rotations and in second ring air holes are
thickness [29]. Plasmonic gold and biolayer were deposited outside arranged at 30 anticlockwise rotations. In the second ring, four air
the PCF surface. The proposed bimetallic SPR sensor shows holes are missing, which accumulates the evanescent electromag-
maximum wavelength sensitivity of 4750 nm/RIU and 4300 nm/ netic field at the four sides of the PCF, and it can easily move to-
RIU for quasi TM and TM fundamental core modes, respectively. wards the metal surface. Here, L is the center-to-center distance
Recently, a multichannel PCF-based sensor has been proposed by between two adjacent air holes, d is the diameter of air holes in the
Hameed et al. [30], where plasmonic silver is coated by the gold. first ring and d1 is the diameter of air holes in the second ring. The
The proposed bimetallic SPR sensor shows maximum wavelength thickness of silver layer is ts. Outside of silver layer an analyte layer
sensitivity of 4750 nm/RIU and 4300 nm/RIU for quasi TM and TM is placed, which acts as the dielectric medium (sensing medium). In
fundamental core modes, respectively. The PCF SPR sensor pro- the proposed sensor, we used fused silica as the background ma-
posed by Otupiri et al. consists of elliptical air holes and four terial. The RI of fused silica can be obtained by using the Sellmeier
microfluidic channels [31], which can detect multi-analytes having equation [38]. The complex RI of silver can be obtained from the
different refractive indices. It is reported that maximum wave- Palik [39]. Finite element method (FEM) with circularly perfectly
length sensitivity of 4600 nm/RIU and amplitude sensitivity of 425 matched layer (PML) boundary condition has been used to simulate
RIU1 can be achieved for a gold layer thickness of 50 nm. A single- the proposed structure. We used finer element meshing, which
ring hexagonal PCF SPR sensor with four microfluidic channels has took 64,475 elements to represent the full structure. The PML
been demonstrated, where four modes are separately studied for thickness and analyte layer thickness were 2.5 mm and 3.5 mm,
multi-analyte detections [32]. The proposed sensor shows respectively. The RI of analyte (na) is varied from 1.33 to 1.37.
maximum wavelength sensitivity of 2400 nm/RIU in y-polarized The sensing performance of a SPR sensor greatly depends on the
HE11 mode. Although multichannel SPR sensors are useful for plasmonic material employed in the design. Current plasmonic
multi-analyte detections, obtaining such microfluidic channels is sensors mostly use gold because of several advantageous proper-
difficult from a fabrication point of view. ties. Gold is chemically inert, long-term stable, and easy to struc-
In D-shaped PCF sensors, the top of the cladding is etched out in ture [19]. However, it has higher optical damping and has wider
order to obtain a flat surface. The plasmonic material and analyte resonance wavelength peak leading to false positive analyte de-
sample are both placed on that flat surface. Most of the internally tections [33]. Copper is another potential plasmonic material hav-
and externally metal-coated PCF sensors are based on the metal ing almost the same optical damping and interband transition as
coating on the circular surface. In general, obtaining a uniform gold. Compared to gold and copper, aluminum has not attracted
circular surface is difficult since it associates with unwanted surface much attention due to its high optical damping, and high interband
roughness. Taking advantage from the flat surface, D-shaped PCF transition loss [19]. From the optical point of view, silver can be
sensors provide possibilities for homogeneous coating with mini- regarded as one of the potential candidates for plasmonic material.
mal surface roughness [33]. Very recently, a D-shaped PCF sensor The positive attributes of silver are no interband transition in the
has been proposed using gold as the plasmonic material and tita- visible wavelength spectrum, low optical damping, narrow
nium di-oxide (TiO2) for shifting the resonance wavelength from
visible to near infrared [34]. In the sensing range between 1.33 and
1.43, the D-shaped sensor shows maximum amplitude sensitivity
of 1086 RIU-1 with sensing resolution of 9.2 106 RIU. Although
D-shaped PCF sensors provide high sensitivity and eliminate the
issue of uniform thickness, they require accurate polishing of the
predefined section. Very recently, a quasi D-shaped PCF SPR sensor
has been proposed by An et al. [35] using graphene and indium tin
oxide (ITO) layers operating in the near-infrared wavelengths.
Another D-shaped PCF sensor has been reported having rectangular
lattice air-holes [36]. Two larger air holes are placed near the core of
the PCF to create birefringence, which yields a higher figure-of-
merit (FOM) of about 478.3 RIU1.
In this paper, a hollow-core PCF SPR sensor with circular lattice
air holes is proposed. A thin layer of silver is used in the outer
surface of the PCF structure, which simplifies the detection mech-
anism. The performance of the sensor is investigated in terms of
amplitude sensitivity, wavelength sensitivity, sensor resolution,
and linearity. Compared to other designs in the literature, the
proposed sensor exhibits lower confinement loss. Due to such low
confinement loss, the length of the sensor can be extended to Fig. 1. Cross-section view of the proposed circular lattice PCF sensor with L ¼ 2 mm,
centimeter scale. We also discuss the fabrication tolerance in order d ¼ 0.57L, d1 ¼ 0.78L and ts ¼ 30 nm.
M.R. Momota, Md.R. Hasan / Optical Materials 76 (2018) 287e294 289
Fig. 3. (a) Loss spectra with increasing analyte RI from 1.33 to 1.37, and (b) amplitude sensitivity with increasing analyte RI from 1.33 to 1.37 with L ¼ 2 mm, d ¼ 0.57L, d1 ¼ 0.78L
and ts ¼ 30 nm.
Fig. 4. (a) Loss spectra with increasing silver layer thickness from 30 to 50 nm at analyte RI of 1.35 and 1.36, and (b) amplitude sensitivity for silver layer thickness of 30, 40 and
50 nm with na ¼ 1.35, L ¼ 2 mm, d ¼ 0.57L, d1 ¼ 0.78L and ts ¼ 30 nm.
Fig. 5. (a) Loss spectra with increasing pitch from 1.8 to 2.1 mm at analyte RI of 1.35 and 1.36, and (b) amplitude sensitivity for different pitch values with na ¼ 1.35, d ¼ 0.57L,
d1 ¼ 0.78L and ts ¼ 30 nm.
Fig. 6. Performance comparison using gold as the plasmonic material (a) Loss spectra with increasing analyte RI from 1.33 to 1.37 and (b) amplitude sensitivity with increasing
analyte RI from 1.33 to 1.37 with L ¼ 2 mm, d ¼ 0.57L, d1 ¼ 0.78L and tg ¼ 30 nm.
case, confinement loss peak varies about ±0.47 dB/cm and ±1 dB/ figure, there is a negligible fluctuation of amplitude sensitivity due
cm due to ±5% and ±10% variations for analyte RI of 1.35. Unlike to the variation of d. Fig. 9(c) shows the impact on confinement loss
variations of ts, small blue shift occurs due to 5% and 10% increase of due to the ±5% and ±10% change of d1 from the optimum value. As
L and small red shift occurs due to 5% and 10% decrease of L. illustrated in the figure, there is a noticeable change of loss depth
Fig. 8(d) shows the effect on the amplitude sensitivity due to ±5% when d1 is varied. Due to 10% decrease of d1 from the optimum
and ±10% variations of L. Amplitude sensitivity does not change value, confinement loss is increased from 2 dB/cm to 4.73 dB/cm.
significantly with respect to variations of L. 10% change of L re- We found a red shift due to this variation. 5% and 10% increases of d1
sults in amplitude sensitivity of 228 RIU1 whereas the optimum result in a blue shift. It can be seen from Fig. 9(d) that amplitude
value is 215 RIU1. sensitivity is almost independent to ±5% and ±10% variations of d1
Fig. 9(a) shows the effect of varying d on the confinement loss by from the optimum value.
±5% and ±10% from the optimum value. Due to ±5% and ±10% The distance between second ring and silver coating layer of the
variations of d, confinement loss varies about ±0.41 dB/cm and proposed hollow-core PCF sensor plays a significant role in the
±0.8 dB/cm for analyte RI of 1.35. Moreover, it is apparent that small manufacturing process. Initially we kept the distance between
blue shifting occurs due to 5% and 10% decrease of d and small red second ring and silver coating fixed to 50 nm. In practice, it is
shifting occurs due to 5% and 10% increase of d. Dependence of difficult to maintain such small distance between second ring and
amplitude sensitivity due to the variation of d by ±5% and ±10% silver coating layer. Therefore, we increased this distance to 100,
from the optimum value is shown in Fig. 9(b). According to the 150, and 200 nm to investigate the effect on sensing performance.
292 M.R. Momota, Md.R. Hasan / Optical Materials 76 (2018) 287e294
second ring and silver coating layer can be enlarged to facilitate the
fabrication.
The proposed PCF consists of circular lattice air holes. The cir-
cular pattern can be realized by employing stack-and-draw, die-
cast and capillary stacking methods [45]. Note that the diameter of
standard PCF is 125 mm; therefore, an extra polishing would be
required to etch out the uncladded silica surface formed outside the
cladding air holes [45]. Moreover, the proposed PCF can be obtained
by using the tapered technique [46]. Due to surface roughness of
the externally-deposited silver nanofilm, it is difficult to obtain a
very smooth surface. The thin silver can be deposited by using
thermal evaporation, sputtering technique, and wet-chemistry
technique [33]. However, minimal surface roughness can be ach-
ieved by employing chemical vapor deposition (CVD) technique
[47]. Due to corrosive nature of the silver and oxidation issue, the
proposed sensor may not be suitable for long-term stability.
However, using graphene on the top of the silver can eliminate
Fig. 7. Linear fitting of resonance wavelength with analyte RI from 1.33 to 1.37. those issues [48,49]. Fused silica has ultra low thermal sensitivity,
which is used as the background material. The RI change of fused
silica with temperature is only 1.28 105/ C. Due to such low RI
The effects due to increasing this distance on the loss depth and change, the effect of temperature variation can be neglected when
amplitude sensitivity are shown in Fig. 10. According to Fig. 10(a), the sensor is used in common environments [50]. For instance, the
loss depth increases by increasing the distance between second self-referencing method can be used to eliminate the impact of
ring and silver coating layer. The minimum and maximum loss instrumental noise and temperature fluctuations [31]. In practical
depth of about 2.435 and 7.74 dB/cm can be obtained when the applications such as in remote sensing, the length of the sensor
distance between second ring and silver coating layer is increased should be long. Generally, the sensor length is restricted to milli-
from 50 to 200 nm for an analyte RI of 1.36. The distance between meter scale due to high propagation loss [31,34]. The proposed
second ring and silver coating layer can be further increased, which sensor shows comparatively lower confinement loss, which
results in a significant increase of confinement loss. As a result, it potentially allows extending the sensor length. Additionally, using
will be difficult to obtain a measurable signal at the output end to three dimensional translation stages and special designed fiber
detect the sample. To maintain the confinement loss lower than holder, the sensor length can be further extended to centimeter
7 dB/cm, the distance between second ring and silver coating layer scale [51].
should not be longer than 200 nm. It can be observed from Table 1 compares the performance of the existing PCF SPR
Fig. 10(b) that amplitude sensitivity is reduced from 215 to 203 sensors with the proposed hollow-core sensor. It can be seen from
RIU1 when the distance between second ring and silver coating the table that the proposed PCF SPR sensor shows improved results
layer is increased from 50 to 200 nm for an analyte RI of 1.35. Due to in terms of amplitude sensitivity, wavelength sensitivity and sensor
such low variation of amplitude sensitivity, the distance between resolution.
Fig. 8. Investigation of fabrication tolerance on the performance of the sensor (a) Effect on loss spectra due to maximum ±10% variation of ts from the optimum value at analyte RI
1.35 and 1.36, (b) effect on amplitude sensitivity due to maximum ±10% variation of ts from the optimum value at analyte RI 1.35, (c) effect on loss spectra due to maximum ±10%
variation of L from the optimum value at analyte RI 1.35 and 1.36, (d) effect on amplitude sensitivity due to maximum ±10% variation of L from the optimum value at analyte RI
1.35.
M.R. Momota, Md.R. Hasan / Optical Materials 76 (2018) 287e294 293
Fig. 9. Investigation of fabrication tolerance on the performance of the sensor (a) Effect on loss spectra due to maximum ±10% variation of d from the optimum value at analyte RI
1.35 and 1.36, (b) effect on amplitude sensitivity due to maximum ±10% variation of d from the optimum value at analyte RI 1.35, (c) effect on loss spectra due to maximum ±10%
variation of d1 from the optimum value at analyte RI 1.35 and 1.36, (d) effect on amplitude sensitivity due to maximum ±10% variation of d1 from the optimum value at analyte RI
1.35.
Fig. 10. Effect on (a) loss depth and (b) amplitude sensitivity due to the variation of distance between second ring and silver layer.
Table 1
Comparison with the existing SPR PCF sensors in the literature.
Ref. Wavelength range (nm) RI Range Wavelength sensitivity (nm/RIU) Amplitude sensitivity (RIU1) Wavelength resolution (RIU) Amplitude resolution (RIU)
4. Conclusions analytes. The plasmonic material and sensing layer are placed
outside the PCF surface, which facilitate both fabrication and ana-
A hollow-core circular lattice PCF-based SPR refractive index lyte detection. The proposed sensor shows a maximum wavelength
sensor is proposed for the detection of biological and biochemical sensitivity of 4200 nm/RIU with a wavelength resolution of
294 M.R. Momota, Md.R. Hasan / Optical Materials 76 (2018) 287e294
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