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Bitumen (Asphalt)
- Two main categories: Natural asphalt & Petroleum asphalt
Natural Asphalt
Occurs naturally in natural deposits (as native asphalt e.g. in
Trinidad lake, etc; or rock asphalt in sandstone or limestone)
Petroleum Asphalt
Also known as refinery asphalts. It is produced by industrial
(fractional) distillation of crude petroleum (crude oil)
It is the heaviest fraction and the one with the highest boiling
point, boiling at 525 °C (977 °F).
3.3 PHYSICAL PROPERTIES
• Those which directly affect the performance of asphalt
in a mixture while being mixed, laid and in service.
Distillation of Cutbacks
4.0 ASPHALT MIX TYPES AND DESIGN
• Methods of preparing asphalt mixtures for
pavements include
- Hot Mix Asphalt (HMA) – heated asphalt + heated aggreg.
- Cold Mix Asphalt – cutback or emulsion mixed with aggreg.
and laid at ambient temperature.
- Penetration Method – heated asphalt sprayed over and
allowed to penetrate compacted crushed aggregates
- Inverted Penetration Method – spreading asphalt binder
over the roadway surface and laying selected aggregates to
penetrate the asphalt.
• Asphalt mixes so produced include
(i) Asphalt concrete (AC); (ii) Rolled asphalt; (iii) Mastic
asphalt; (iv) Surface treatment (slurry seals, dressing);
(v) Bituminous macadam; (vi) Penetration macadam
Principal Bituminous Mix Types
1. Asphalt Concrete: A high quality, thoroughly controlled
mixture of hot asphalt binder and hot mineral aggregates
2. Rolled Asphalt: A high quality mortar type produced using
fine aggregate and penetration grade asphalt. These mixes
are more flexible and durable than asphalt concrete
3. Mastic Asphalt: A mortar type of bituminous mix usually
cast into blocks, with 14-17% hard asphalt binder (10-25 pen).
For crack sealing, to prevent attrition of aggregates, etc.
4. Bitumen Macadams: They contain coarsely graded
mineral aggregates coated with asphalt in premix plants. They
have higher air voids than AC
5. Penetration Macadams: Produced by spraying heated,
dissolved or emulsified asphalt over compacted crushed
aggregate in-situ.
6. Surface Treatments: Inc. surface dressing, tack coats etc
5.1 Types of Bituminous Surfacing
OTTA SEAL CONSTR.
Spreading of aggregate
over cutback asphalt spray
4) Fatigue resistance
- Resistance to pavement failure due to repeated
traffic loading (failure in form of alligator cracking)
- Dense-graded mixtures offer higher fatigue resist.
5) Skid resistance
- Controlled by aggregate physical characteristics
(texture, shape & resistance to polish)
- Also, low asphalt content & open-graded aggregate
6) Impermeability
- Resistance to penetration of water and air
- Improves pavement durability and stability
- Facilitated by high asphalt content, dense gradation
and sufficient compaction (→ imperviousness)
7) Workability
- Ease of AC placement and compaction (with
reasonable effort)
- Factors that promote high stability cause workability
problems (→ a compromise required)
Stability X X X
Durability X X X
Flexibility X X X
Fatigue resist X X X
Skid resist. X X X
Impermeab. X X X
Workability X X X
4.2 ASPHALT MIX DESIGN
• Two primary properties desirable in design of asphalt
concrete mixtures are stability and durability (i.e.
getting a stable AC mix that is durable)
• Factors to also consider are economy and workability
• Aim is therefore “to find an economical gradation and
blend of aggregate and asphalt that will yield a mix
having:-
1. Sufficient asphalt binder to ensure a durable pavmnt
2. Sufficient mix stability to serve without distortion or
displacement at the anticipated traffic load
3. Sufficient voids in the compacted mix to avoid bleeding
4. Sufficient workability to facilitate proper compaction”
Addit. requirements: Flexibility, fatigue- & skid resistance
4.2.1 MARSHALL MIX DESIGN
• Developed by Bruce Marshall in the US
• Aims at obtaining a dense mix of high stability but with
adequate void content to allow sufficient binder
content for good durability and flexibility
• Standardized in ASTM D1559 and AASHTO T245
• Standard procedure involves:
(i) Prep. of test specimens, h ≈ 63.5 mm, Ф ≈ 101.5 mm
- heating, drying, mixing and compacting in mould
- both faces of sample receives same number of
compaction blows, determined by the traffic levels
Traffic level Number of blows/face
Light (ESAL < 104) 35
Medium (ESAL = 104-106) 50
Heavy (ESAL > 106) 75
Marshal Mix Design cont…
(ii) Bulk density test
Determined on compacted cooled specimens by
the water displacement method, with a thin coat of
paraffin wax on it
(iii) Stability and flow test
Specimens are conditioned for 30-40 min in water
bath at 60ºC. They are compressed in the Marshall
test machine (rate 51mm/min) for determination of
Stability and Flow
NB: Stability is the max load resistance (kN) that the test
specimen will develop at 60ºC in the Marshall test.
:Flow is the total deformation (in 0.25 mm units) of
the specimen at failure when subjected to
compression in the Marshall stability test
Marshall Mix Design Test Set-up
Marshal Mix Design cont…
(iv) Density-voids analysis
- This involves determination of voids using known
and computed density (specific gravity) values
- Three types of voids are considered, namely:
VMA = Voids in Mineral Aggregates
VTM = (Air) Voids in Total Mix
VFB = Voids Filled with Binder (also VFA - asphalt)
(v) Interpretation of test results
The obtained data are used to prepare plots which
are used to determine the optimum binder content
(vi) Determination of the optimum binder content
The content that fulfills the requirements
Density-Voids Analysis
• Mineral aggregates are porous; can absorb water and
asphalt to a var. degree.
• For Marshall mix design, we consider Bulk SG and
Effective SG
1. Bulk Specific Gravity, Gsb
• This includes the volume of the water permeable voids
in the aggregate (often termed the “”saturated surface
dry” or SSD volume of the aggregate.
2. Effective Specific Gravity, Gse
• Includes the volume of the water permeable voids in
the aggregate that cannot be reached by the asphalt.
IMPORTANT DEFINITIONS
1. Voids in Total compacted Mix (VTM)
Total volume of the small pockets of air existing between the
coated aggregate particles in a compacted asphalt paving
mixture, expressed as a percentage of the bulk volume of the
compacted mixture
VTM = (Va/Vm)* 100%
2. Asphalt binder content (Pb)
Pb = (Mb/Mm)* 100%
3. Effective asphalt binder (volume) (Vbe)
The volume of total asphalt (content) minus the portion of
asphalt „lost‟ by absorption into the aggregate particles
Vbe = Vb – Vba
NB: Absorbed binder: Pba = (Mba/Mg)*100%
IMPORTANT DEFINITIONS cont…
4. Voids in Mineral Aggregate (VMA)
The volume of inter-granular void space between the aggregate
particles of compacted paving mixture that includes the air voids
(VTM) and effective asphalt binder content (Pbe), expressed as
a percent of total volume of the mixture specimen
VMA = [(Va + Vbe) / Vm] *100%
5. Volume Filled with Binder (VFB)
The percentage of the voids in the mineral aggregates (VMA)
that is „occupied‟ by the effective asphalt binder (i.e. voids in
mineral aggregate minus voids in the compacted total mix,
expressed as a percent of the voids in mineral aggregates)
VFB = (Vbe/VMA)*100%
= [(VMA-VTM)/VMA] * 100%
SUMMARY OF RELATIONSHIPS
1) M m = M b + Mg
= Mbe + Mba + Mg
2) Vm = Vg + Vbe + Va
= Vg + (Vb - Vba) + Va
3) ρmb = Mm/Vm ; (Gm = ρmb/ ρw)
4) Vgb = Mg/ ρgb = Mg/(Ggb*ρw)
5) Mb = Pb * Mm ; Vb = Mb/ρb = Mb/(Gb* ρw)
6) Mba = Pba * Mg ; Vba = Mba/ ρba = Mba/(Gb* ρw)
7) Vbe = Vb - Vba
8) Va = Vm - (Vg + Vbe) = 1 - (Vg + Vbe), cons. unit volume
SUMMARY OF RELATIONSHIPS cont…
9) VTM = (Va/Vm)*100% = (Va/1)*100% if Vm = 1 m3
Therefore:
= 89.5%
INTERPRETATION OF DATA
From the test results, prepare the following plots:
weak asphalt
layer
SUPERPAVE MINERAL AGGREGATE
Rounded Aggregate
When a mass of aggregate is loaded, aggregate particles
begin to slide by or “shear” with respect to each other,
which results in permanent deformation of the mass.
shear plane
= c + (tan
shear strength normal
stress
asphalt binder aggregate
contribution contribution
shear shear
stress () stress ()
large “c”
small “c”
small large
funnel
fine aggr sample (190 g)
suspended clay
sand reading
sedimented
aggregate
Superpave Clay Content
Requirements
Traffic, million Sand Equivalent,
ESALs minimum
< 0.3 40
0.3 to < 3 40
3 to < 10 45
10 to < 30 45
> 30 50
6.3 Superpave Binder Tests
Three ‘new’ tests are used to measure the
physical properties of Superpave binders:
• Dynamic shear test, which measurer the
binder's stiffness and phase angle at
intermediate and high temperatures.
• Bending beam test, which measures the low-
temperature stiffness of the binder.
• Direct tension test, which measures the low-
temperature tensile and fracture properties.
DTT RV
DSR
BBR
- 20 20 60 135
Pavement Temperature, C
SUPERPAVE BINDER PURPOSE
TEST
Dynamic Shear Rheometer Measure properties
(DSR) at high and
intermediate
temperatures
Rotational Viscometer (RV) Measure properties
at high temperatures
Bending Beam Rheometer Measure properties
(BBR) at
Direct Tension Tester (DTT) low temperatures
Rolling Thin Film Oven Simulate hardening
(RTFO) (durability)
Pressure Aging Vessel characteristics
(PAV)
Fatigue Low Temp
Cracking Cracking
Construction Rutting
[DTT]
[RV]
[DSR] [BBR]
Pavement Age
RTFO - aging
No aging
PAV - aging
Superpave Binder Tests cont…
6.3.1 The Rolling Thin-Film Oven (RTFO) Test
• The test simulates short-term aging by heating a
moving film of asphalt binder in an oven for 85
minutes at 163° C (325° F).
• The effects of heat and air are determined from
changes incurred in physical properties measured
before and after the oven treatment by other test
procedures.
• The moving film is created by placing the asphalt
binder sample in a small jar (figure next slide) then
placing the jar in a circular metal carriage that rotates
within the oven.
The Rolling Thin-Film Oven Test
RTFO Samples
(left - after aging in the RTFO,
The Rolling Thin-Film Oven
center - before aging in the RTFO,
right - empty sample jar)
6.3.2 The Pressure Aging Vessel (PAV)
• The test was adopted by Superpave to simulate the
effects of long-term asphalt binder aging that occurs
as a result of 5 to 10 years HMA pavement service.
• The PAV is an oven-pressure vessel combination
that takes RTFO aged samples (figure next slide)
and exposes them for 20 hours to high air pressure
(2070 kPa) and temp. (90° C, 100° C or 110° C),
depending upon expected climatic conditions.
Rotational Viscometer
Rotational Viscometer (Schematic)
6.3.4 The Dynamic Shear Rheometer (DSR)
• The test is used for testing medium to high temper.
viscosities (it is conducted between 46° C and 82° C).
• The actual temperatures anticipated in the area where
the asphalt binder will be placed determine the test
temperatures used.
• The basic DSR test uses a thin asphalt binder sample
sandwiched between two plates. The lower plate is
fixed while the upper plate oscillates back and forth
across the sample at 1.59 Hz to create a shearing
action.
• These oscillations at 1.59 Hz (10 radians/sec) are
meant to simulate the shearing action corresponding
to a traffic speed of about 90 km/hr
Dynamic Shear Rheometer Test
• Pavement Temperature
• Adjust for Speed of Traffic
• Adjust for Axle Load
PG SPECIFICATIONS
*the highest possible pavement temperature in North America is about 70°C but
two more high temperature grades were necessary to accommodate transient and
stationary loads.
Sample Preparation
The Superpave gyratory compactor
• It was developed to improve mix design's ability to
simulate actual field compaction particle orientation
with laboratory equipment
• Compaction pressure = Typically 600 kPa (87 psi)
• Simulation method - The sample is inclined at 1.25°
and rotates at 30 revolutions per minute as the load is
continuously applied. This helps to achieve a sample
particle orientation that is somewhat like that achieved
in the field after roller compaction
• Number of gyrations at three levels of compaction are
used for determination of opt. binder content (Ninitial,
Ndesign & Nmax.)
Gyratory Compactor cont…
Key parameters of the gyratory compactor are:
• Sample size = 150 mm (6-inch) diameter
cylinder approximately 115 mm (4.5 inches) in
height (corrections can be made for different
sample heights). Note that this sample size is
larger than those used for the Hveem and
Marshall methods (see the figure).
Selection of Optimum Asphalt Binder Content
< 0.3 70 - 80
0.3 to < 3 65 - 78
10 to < 30 65 - 75
30
Selection of Optimum Asphalt Binder Content – Contd…
THANK YOU!!