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Name : Name : C1 to C4 Hydrocarbon Instrument : C1 to C3 Hydrocarbon on
Name
:
Name
:
C1 to C4 Hydrocarbon
Instrument
:
C1 to C3 Hydrocarbon on PLOT COLUMN
Chemito GC with FID
Instrument
: Chemito GC with FID
Analytical Conditions
Analytical Conditions
Col
:
Col
: Porapak N 6 Ft
Inj.
:
100° C
100° C
40° C
10 ppm each.
Hydrocarbon.
Inj.
:
50 Mtr 0.32 ID
Al2O3/KCL PLOT COLUMN
100° C
Det.
:
Det.
:
150°C
Oven
:
4
Oven
:
5
Sample
:
Sample Qty. :
Split
:
50° C
25 ul.
1 : 125
1 2
6
3
1
3
1.
Methane
2
1.
Methane
2.
Ethane
2.
Ethylene
4
5
6
3.
Ethylene
3.
Acetylene
4.
Propane
4.
Porpane
5.
Propylene
5.
Propylene
6.
Acetylene
6.
Butane
0
5
10
15
0
1
2
3
Code No.: L_201
Code No.: L_202
Name
:
Name
:
Instrument :
C1 to C5 Hydrocarbon
Chemito GC with FID
Instrument :
Ethylene Gas Purity
Chemito GC with FID
Analytical Conditions
Analytical Conditions
Col
:
20% SEBACONITRILE, 20 Ft
Col
:
Inj.
:
50° C
Inj.
:
Det.
:
100° C
Det.
:
Oven
:
40° C
Oven
:
50 Mtr GS-ALUMINA PLOT
100° C
150° C
70° C
1
9
6
8
10
1.
Air Methane
1. Methane
5
7
2.
Ethane
2. Ethane
3
4
3.
Propane
10
3. Ethylene
4.
Propylene
3
2
4. Propylene
5.
iso Butene
5. Acetelene
5
6.
n Butene
4
6. C2H2
2
7.
iso Butene
6
7
7. NC4
8
1
8.
T 2 Butene
11
8. +C4
9
9.
iso Pentane
9. 1C4
10.
N Pentane
10. 0
cis C4
5
10
15
0
5
10
15
11. PPDN
Code No.: L_203
Code No.: L_204
Name
:
C2 Hydrocarbon Stream
Chemito GC with TCD
Name
:
Instrument :
Instrument :
Ethylene & Propylene Stream
Chemito GC with FID
Analytical Conditions
Analytical Conditions
Col
:
Col
:
Inj.
:
Inj.
:
Det.
:
20% BEEA, 20 Ft
50° C
100° C
40° C
Det.
:
20% BEEA, 20 Ft
50° C
100° C
Oven
:
Oven
:
40° C
2
8
3
2
5
7
3
1
4
9
1. CH4
2. C2H2
3. C2H4
4
4. C2H6
6
1
1. Air
5. C3H6
2. Ethane
6. C3H8
3. Ethylene
5
7. 1C4
4. Propane
8. 1C4
5. Propylene
9. 0
nC4
2
4
6
8
10
0
5
10
15
Code No.: L_205
Code No.: L_206
Name : Name : C3 Stream Impurities Chemito GC with FID & Methanator Instrument :
Name
:
Name
:
C3 Stream Impurities
Chemito GC with FID & Methanator
Instrument :
Propylene Stream
Chemito GC with FID
Instrument :
Analytical Conditions
Analytical Conditions
Col
:
Inj.
:
Inj.
:
30% TBP, 40'X ¼'' s.s
50° C
Det.
:
Det.
:
Oven
:
Oven
:
100° C
40° C
Col
:
50° C
100° C
40° C
With CSV & Porapak Q & Molecular Sieve 13X
2
1
3
5
1
2
4
1.
Propylene ( 99%)
3
1. AIR
2.
Propadiene (75 ppm)
2. CH4
3.
Methyl Acetylene (75 ppm)
3. CO2
4. C2H4
5
10
15
20
25
5. 0
C2H6
2
4
6
8
10
Code No.: L_207
Code No.: L_208
Name
:
Name
:
Instrument :
C4 Stream Impurities
Chemito GC with FID
Instrument :
C4 Hydrocarbon
Chemito GC with FID
Analytical Conditions
Analytical Conditions
Col
:
0.19% Picric Acid on Carbopak
Col
:
Inj.
:
50° C
Inj.
:
Det.
:
50° C
Det.
:
Oven
:
25° C
Oven
:
20% Sebaconitrile 30'x1/8 ”
50° C
100° C
35° C
2
3
6
Quantity
:
50 ul
1
4
4 5
3
1. isobutene
1
2. Butane
1. isobutane
3. iso Butane
2. n-Butane
2
4. n-Butane
3. 1- Butane
5. cis Butane
4. isobutane
5
6. Trans Butane
5. Trans-2 Butane
6
7
6. 2-Butane-CIS
7. isopentane
0
5
10
15
0
10
20
30
Code No.: L_209
Code No.: L_210
Name
:
Instrument :
C4 Hydrocarbons
Chemito GC with Cryo Acc.
Name
:
Instrument :
LP Gas with GS Alumina Plot Column
Chemito Capillary GC with FID
Analytical Conditions
Analytical Conditions
Col
:
Inj.
:
Det.
:
Oven
:
20% BEEA, 20 Ft
30° C
30° C
00° C
Col
:
Inj.
:
Det.
:
1234 56
67
Oven
:
Quantity
:
50 Mtr.x0.53 mm ID
GS Alumina Plot
100° C
100° C
70° C
25 ul
3
9
2
4
1
5
8
1. Propane
2. Propene
9 10
1. Propane
3. iso Butene
7 8
2. Propylene
4. n Butane
3. i- Butane
5. Trans 2 Butane
4. n-Butane
6. Butane
5. 1 Butene
7. iso Butane
6. Trans 2 butene
8. 2 Butane Cis
7. isobutene
9. iso Pentane
8. cis-2 butene
10. 0
n Pentane
9. 1,3 Butadine
5
10
15
5
10
15
20
25
Code No.: L_211
Code No.: L_212
Name : Natural Gas with Back Flush Chemito GC with TCD & Back Flush Valve
Name
:
Natural Gas with Back Flush
Chemito GC with TCD & Back Flush
Valve with Gas Sampling Valve
Name
:
Instrument :
Instrument :
Natural Gas by Temp. Programming
Chemito GC
Analytical Conditions
Analytical Conditions
Col
:
Col
:
30% DC_200, 30 Ft
TCD
40° C
Inj.
:
Det
:
Det.
:
Oven
:
Oven
:
Porapak Q 10'
100° C
TCD
50° C (2 min.)
(Temp. Prog.)
12°c/min
150° C
2
2
4
1
5
1. N2
3
5
3 4
2. CH4
1. N2
3. CO2
6
1
2. CH4
7
4. C2H6
3. CO2
8
5. C3H8
4. C2
6. i C4
6
7
5. C3
7. n C4
6. C4
8
9
8. i C5
7. C5
9. n C5
8. 0
C6+
5
10
15
20
25
0
5
10
15
20
25
Code No.: L_213
Code No.: L_214
Name
:
RGA Test Mixture
Name
:
Instrument : Chemito 8500 RGA with CSV, BFV
Instrument :
RGA Mat Sample
Chemito 8500 RGA with CSV, BFV
Analytical Conditions
Analytical Conditions
Col
:
Col
:
Det.
:
:
Sample
:
20% SEBN, Mol. Seive
5A & 13X, Porapak Q
Dual TCD
40° C
0.5 ml of RGA Std. Gas
Det.
Oven
:
Oven
:
Sample
:
20% SEBN, Mol. Seive
5A & 13X, Porapak Q
Dual TCD
40° C
0.5 ml of RGA Std. Gas
15
1. H2
2. CO2
3
11
3. C3
3 4
1. Hydrogen
10.
iso Pentane
4. i C4
2
5
2. Carbondioxide
11.
cis Butene2
5
5. n C4
3. Propane
12.
n Pentane
6. i C5
10
1
1
9
4. Propylene
13.
Ethylene
4
7. n C5
12
5. iso Butane
14.
Ethane
8. C2
2
13
8 9
11
6
13
6. n Butane
15.
Nitrogen
9. C2
16
8
7. I Butane
16.
Methane
10. O2
12
6
17
10
7
14
7
8. CO
iso Butane
17.
11. Methane
9. Trans 2 Butane
12. N2
0
5
10
15 20 25
30 35 40
45
13. 0
CO
10
20
30
40
50
Code No.: L_215
Code No.: L_216
Name
:
Natural Gas by Satellite Refinery Gas Analyser
Name
:
Instrument
: Chemito Refinery Gas Analyser with FID & TCD
Instrument :
Natural Gas by Satellite Refinery Gas Analyser (TCD)
Chemito Refinery Gas Analyser with FID & TCD
Analytical Conditions
Analytical Conditions
Col
:
Mol. Seive 13X, Sebaconitrile
Col
:
Mol. Seive 13X, Sebaconitrile
Inj
:
& Porapak Q
100° C
200°C (FID)
40° C
Inj
:
Det
:
Det
:
2 3 4
5
Oven
:
Oven
:
& Porapak Q
100° C
200° C (FID)
40° C
1
1
6
2
1. Methane
7
2. Ethane
3. Propane
1. Nitrogen
3
4. isobutane
4
2. CO2
5. n-Butane
3. Ethane
6. isopentane
4. CO
7. n-Pentane
0
2
4
6
8
9
0
2
4
6
8
9
Code No.: L_217
Code No.: L_218

Name

:

C1 to C6 Analysis by Plot Column

 

Instrument :

Chemito Capillary GC with FID

Analytical Conditions

 

Col

:

50 mtr x 0.53 ID GS Alumina Plot

 

Inj

:

250° C

Det

:

250° C

Oven

:

70° C (5 min)

Oven : 70° C (5 min) 5° c/min 100° C (20 min)

5° c/min

Oven : 70° C (5 min) 5° c/min 100° C (20 min)

100° C (20 min)

Quantity

:

(Temp. Prog) 25 ul

Split

:

1 : 100

1.

2.

3.

4.

5.

6.

7.

8.

9.

Methane

Ethane

Ethylene

Propane

Propylene

isobutane

n-Butane

Acetylene

Trans-2-Butene

10.

11.

12.

13.

14.

15.

16.

17.

18.

Butene

isobutylene

cis-2-Butene

isopentane

n-Pentane

1.3 Butadiene

Propyne

trans-2-Pentene

Pentene-1

19.

20.

21.

22.

23.

24.

25.

cis-2-Pentene

n-Hexane

1 Butyne

2 Butyne

Trans-2-Hexene

Hexene 1

cis-2-Hexene

18 20 9 10 15 12 24 11 21 22 8 13 16 17 7
18
20
9 10
15
12
24
11
21
22
8
13
16 17
7
14
6
4
2
25
19
1 5
3
23
0
5
10
15
20
25
30
35
40
45
50
55
60
65

Code No.: L_219

Name : Natural Gas by Capillary & Back Flush Name : Green Oil in Propylene
Name
:
Natural Gas by Capillary & Back Flush
Name
:
Green Oil in Propylene
Instrument :
Instrument :
Chemito GC with FID, LSV &
Back Flush Valve
Chemito Capillary GC with FID & TCD
Back Flush
Analytical Conditions
Analytical Conditions
Col
:
Col
:
30% DC 200, 6 ft.
Porapak N, 6 ft. &
Inj
:
Det
:
30% TBP, 30 ft. X ¼” S.S
150° C
200° C
40° C
2 ml of propylene by LSV
Inj
:
Oven
:
Det
:
50 mtr. Pona Cap. Col.
100° C
200° C (TCD)
2
Sample
:
Oven
:
40° C (4min)
4° C/min
1
130° C (Temp. Prog.)
4
1. N2
2. CH4
3. Ethane
5
1. Propylene
4. C3
6
2
7 8
2. Green Oil - 10 ppm
in Propylene
5. I-C4
1
3
6. N-C4
7. I-C5
8. N-C5
0
5
10
15
20
0
5
10
15
Code No.: L_220
Code No.: L_221
Name
:
L-P-Gas
Chemito Refinery Gas Analyser
Name
:
Instrument :
Instrument :
C4 Olefin Stream by Plot Column
Chemito Capillary GC with FID
Analytical Conditions
Analytical Conditions
Col
:
Set of Analytical Col. With Chemito RGA GC
Col
:
Inj
:
Det
:
Oven
:
Sample
:
75° C
75° C
45° C
250 ul. Gas
Inj
:
Det
:
50 mtr. Alumina Plot Column
180° C
200° C
1
Oven
:
90° C (3 min)
15° C/min
3
4
Sample
:
Spilt
:
180°C (Temp. Prog.)
10 ul of Gas
1 : 100
1. C6+
2. Propane
3. iso-Butane
4. n-Butane
5
4
5. Butene -1
6. isobutene
1. isobutane
8
7. Trans-2-Butene
2. n-butane
8. I Pentane
2
3. trans-2-Butane
2
9. cis-Butene-2
4. 1 Butene
9 10
3
10. n-Pentane
6 7
1
5 6 7
5. iso-Butene
11 12
11. Oxygen
6. cis-2-Butene
12. Nitrogen
7. iso-Pentane
0
5
10
15
0
5
10
15
20
25
30
Code No.: L_222
Code No.: L_223