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JEFCOR L ORATORIES, INC~

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Qjia[ity Servi1:e is Our ~usiness
. Metro Manila . Cavite it Davao

I BISA Bldg.. Perpetual Village, East S~rvice Road


Paraiiaque City. Metro Manila
Tel. No.: (632) 838-8433/84 Telel;,..: (632) 838-8483
E-rnail: jercor@skyineLnC!
Enghlccring BllIg.. Main S1.. FifOt Cavitc Industrial ESlale
Lanekaan. Dasrnarifias. Cavilc
TcL-No.: (046) 402-1318
E-rnaii: jcfcor@skyincLncl
Rill. c IJ GRDC Building
1":lIlang. D"vao City
Tel. Nil.: (082) 235-3544
E~mail: jcfcor@skyincLnct

Poly Aromatic Hydrocarbon Analysis

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FiDfA.(Q2iii1i7PMIliEOiiDj)

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PESTICIDE

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Recognized LaboratCl)' . AUTHORJTY,
C.R. No. 0$12005
..- "; RoCogn1ZOOI.abcratory
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JEFCOR LABORATORIES, INCa
Quafity Service is Our 'Business
.. Metro Manila . Cavite .. Davao
BISA Bldg., PerjJetuaJ Village. East Service Rood Engineering Bldg., Main St.. Firsl Cavile Industrial Estale Rm.213 GRDCDuildillg
Parmiaque CilY, MelrO Manila Lallgkaan. Da5mariiias, Cavitt: L.1I13nl1Davao City
Tel. No.: (632) 838-8483/84 "Ie(ela." (632) 838-8483 Tel. No.: (046)40:2-/3111 Tel. N~~: (082) 235-3544
E-mail: jeli:or@skyinel.llet E-mail: jefcor@skyiIlCt.net E-mail: jcfcor@skyillct.l1el

. 07CA-0135
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Recognized laIIaratcxy
C.R. No.'039/2OO5

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.- ._- -.. ..-

CALIBRATION CERTIFICATES

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.:,'.~..... I TEAM NO.3 - METER BOX CALIBRATION

USING FIVE CRITICAL ORIFICES


-

Console Model 04-Jan-07 i Time 1300H 5td Temp 2!


Number 5721Date
Console Serial Barometric Pressure 756.2 Std Press 7f
0210064 mmHg
Number
DGMModel K.. 0.392'
SK25 Theoretical Critical Vacuum 357mm Hg or 141nHg
Number
DGMSerial Previous O.
8000573 Calibration Technician CJG
Number calibration

I! DGM
Elapsed Orifice
Metering Console
Volume Outlet Temp. Coef.
Critical Orifice

Ambient Temp. Critical


TH'fiG
. .10 Vi\JUUIU

I j',-
-- J--
e
- min.
AM
Pm
IRltl1
VmI
mm H2O ------mL
Final
Vmf
- m3.-
elf
Vm
>0.14iri3- "--'De'
InitlElI
tml
F-IFlal
tmf
DC
....-0
;'flil!
#
K'
.'- - .----- .----- .-
mebic units
Initial
-. t.mb.
"c
Final
. - .f8n1b-.------' .
.C
Hg.
or
mmHg
..

I
;
16.0 8.0 455.7670 0.147 25.0 25.0 40 2.07929 26.0 26.0 15.0
455..91361 I
i
26.0 15.0
~ 11.0 17.0 455.9190 456.0654 0.146
I
25.0 25.0
4. 3,00839 26.0
..

, 9.0

7.0

5.0
:30.0

50.0

90.0
456.0730

456.2420

456.4070
456.2314

456.3992

456.5619
0.158

0.157

0.155
25,0

25.0

25.0
25.0

25.0

25.0
55

63

73
3.99715

5.11189

7.08081
26.0

26.0

25.0
26.0

25.0

25.0
15.0

15.0

15.0
I
Standardized Data .
I Dry Gas Meter
I
CaUbration Factor Flowrate AHg
, Dry Gas Meter Critical Orifice
Value Varn Std & corr 0.0212 m3.tJmln Varlat

Vin(aIdI 'QII1Cstd) Vet(Sld) Qet(Std) dY Omcstd)(CGII) dHc MH


Y
m3 m3/min m3 m3/min %2% m3/min mm H2O :t5.1mn

0.1460 0.OQ91 . 0.1455 0.0091 0.9966 0.11 0.0091 43.4905 -0.5


-.
J I
0.1459 0.0133 0.1447 0.0132 ! 0.9919 -0.37 0.0132 44.2257 0.2
~ !
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t

, 0.1581 0.0176 0.1573 0.9953 ! 0.0175 44.3209 0.3


0.0175 -0.03
r
0.1572 0.0225 0.1566 0.0224 0.9965 0.09 . 0.0224 45.2640 1.3

If 0.1555 0.0311
. 0.1551 0.0310 0.9975
-
0.20 0.0310 42.7217 -1.3

. Y Average 0.9955 44.0045

I
6.HGAverage

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L Signature: Date: 4-Jan


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:~~.; TEAM NO.3 - METER BOX CALIBRATION
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USING FiVE CRITICAL ORIFICES

"~~I
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Meter Gamma vs Flow Rate


1.020 - -
1.015 ""'-

1.010
-
~
1"11 1.000
.1.005
<;.,<0 - - .. ._. n
<tJ
_.
E - ._,, . ......
'''crt' .-
k' r;..9>0P ..
-
. g
C!
0;995 _. ""-
--" .....
Q? .
-

;
.... 0.990
Qj
, :
::i1: 0.985
...:
.
., I
0.980

0.975 - .- -- .- -- -- -- -- -- e- - - -- . - -- - . -- - - - -
0.970 ...I- -
0.005 0.010 0.015 0.020 0.025 0.030 0.1
Flow Rate m3/min

1- ~ - Upper Umit . Meter Box - - - -:- Lower Umit I

Meter Pressure vs Flow Rate


100.0
90.0
80.0

~ 70.0
60.0
50.0
... 40.0
.$
~ 3Q.0

,I
.

20.0
10.0.
6.0 .
0.0050 0.0100 0.0150 ) 0.0200 0.0250 0.0300 0.035(
r- Flow Rate m3/min

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TEAM NO. :; . CRITICAL ORIFICE

DETERMINATION OF ORIFICE COEFFICIENT K'

Std
1200H 298 .K
Console Model Number
572 i
Date
04.Jan-07ITlme
I Temp
,
111
Conaole Serial Number 0210064 Barometric Pressure 756.2 mm Hg Std Press 760 mmHg

IIt
(
DGM M"del NUJ:l1ber SK25 Theoretical CrItical Vacuum 357mm Hg or 14in Hg K1 0.3921

Previous
DGM Serial Number 8000573 Calibration Technician EOA 0.9981
calibration

fI Metering Console Critical Orifice


i PGM
I Actual
i
I Elapsed Volume Outlet Temp Coeff. Dlff
Orifice I Ambient Temp Critical Vacuum
TIme Vacuum x104 %
Run l1H Initial Final Final Orifice Initial Final - .. . ._-- -.. -.-.-
(Initial . -. -. ._._- -- 'n
# . . ..10 or
._-- - 9 .. - Pm' V'- ..' '-Vmi" .. -i..v I.nr t.m.. tomb In Hg <
1.- . or 2tS-50mm K'
. mln mm H2O m3 m3 .C .c .c .c mmHa )0 Critlcal :1:0.5

-- 1 6 7 454.6060 454.6610 24.0 24.0 40 24.0 24.0 15 16 2.08308


-
0.18.

2 6 7 454.6610 454.7158 21.0 4.0 40 24.0 24.0 1.5 16 : 2.07550 0.1e .


.\ Average 2.07929
1 6 15,4 454.7210 454.8004 I 24.0 25.0 48 24.0 24.0 15 16 3.00460 0.13
2 6 15.4 I 454.8004 454.8800 25.0 25.0 I 48 25.11 25.0 15 16 3.01218 0.13
Average 3.00839
1 6 2B 454.8890 454.9948 25.0 25.0 55 25.0 :is.o 15 16 4.00852 0.28
2 6 28 454.9948 455.1000 25.0 25.0 55 25.0 25.0 15 16 3.98579 . 0.28
Average 3.99715
1 . 6 45 455.1070 455.2414 25.0 I 25.0 63 25.0 25.0 15 16 5.10050 0.22
2 , 6 45 455.2414 455.3764 ! 25.0 25.0 I 63 25.0 25.0 15 16 5.12327 0.22
Average 5.11189
1 6 86 455.3920 455.5780 I 26.0 ! 25.0
73 25.0 25.0 15 16 7.07488 0.08
2 6 86 455.5780
455.7640 I 25.0 25.0 I 73 25.0 25.0 15 16 7.08675 0.08

Average 7.oa081
.

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BERKf/lANSYSTErv1S~
INC.
£111'irOllmel1la[.\.Jal1agemellF Service Pro\:ider

TEMPE'RATURE DISPLAy- CALIBRATION


lYIeterConsole No. BSI - T3 Personnel EOA, CJG
Reference Calibration Maker ALTEK Pretest OK
Model Series 22 TC Source P osttest OK
Serial No. -' Date 04 January 2007

TC Refernce Temp. ..Qritria Reference ---.Temp. Criteria Criteri;'


-.-CHANNEL- - Temp 1,-'- Readhig' ... Criteria Met Temp. 2, Reading Met
ID °c 1,oC °c 1,oC
PROBE 0 -2 -0.733 Y 50 .. 50 0.619 Y
FILTERl- ... 0 -1 -0.366 Y' 50 " .- 50 0.619 Y
EXIT' "\0 '.. -2 50 50 0.619 Y
-0.733 Y
AUX 0 -2 -0.733 Y 50 50 0.619 Y
STACK O. 2 -0.733 Y 250 346 0.765 Y
STACK 50 48 -0.619 Y 300 298 0.349 Y
TC Reference Temp. Criteria Reference Temp. Criteria Criteria
HANNEL Temp. 3, Reading Criteria Met Temp. 4, Reading Met
ID °c 1,oC °c 1,oC
PROBE 100 99 0.268 Y 150 147 0.709 Y
FILTER 100 98 0.536 Y 150 147 0.709 y
EXIT 100 98 0.536 y 150 147' 0.709 y
AUX 100 99 0.268 Y 150 147 0.709 Y
STACK 350 349 0.161 Y 450 449 0.138 Y
STACK 400 399 0.149 Y 600 600.. 0.000 Y
. CRITERIA: Percent difference between the Reference Temperature and the average Temperature can be only 1:1.5%°.

.EQUATION: [CRef.Temp. + 273). (Temp. Readlnq + 273)1 x 100


(Ref.Temp. +273)

Calibrated By : Checked By:

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~ Environmental Alanagement Service Provider


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It TEMPERATURE SENSOR CALIBRATION DATA SHEET,


I, Date 04 JANUARY2007 Thermocoucle No. TMC- T3
Personnel EOA. CJG Reference
Ambient Temperature 29.20 e ASTM Mercurv-in-alass ID# SILBER
I '.
NIST Reference Te 10#
._._---- -.- n- . - --
._- ."
- ._- ---
I Date
Reference Reference Thermocouple Absoiute
Point Number Source (Specify) Thermometer Display Temp., Temperature
, '" Teme., °e ' e '.' ! Differonce, % .
., ..
04 JAN.
,
ZOO7
-
"
1
-'f '(
''q;OTWATER 90.2 90 0.2
2 AMBIENT 30.2 30 0.2
3 ICED WATER 2 2 0
1
2
3
1
2
3
2
'.- - .
3

Ghecked By:
Calibrated By: Signa
COV;:(t ",h!lS-
e OverPrintedName

Date:
Over Printed Name

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El1virol1mentallvlal1agement Sen.-ice Provider

-
POST TEST THERMOCOUPLE CALIBRATION CHECK
EPA Approved Alternative Method (Alt-Q11)
Single Point Calibration.

Thermocouple ill .. TMC- T3 Personnel EOA, CIG.


Probe I Pitot Tube ill SPA-T3-36/ PT-T3-3 Probe T e Stainless Steel
-.- - ~.
_'H' . .-- --
' -------
. ..-.--.- - .-

DATE Calibrated Reference Thermocouple


; .
Difference 2 Continuity
\
.-PASS I
.
.. By: Temp. °c 1 Temp. °c lithi' + 1oC) . Check 3 FAIL
4 JAN.2Qof EOA 30.0 30.0 0.5 OK PASSED

-- "
i.'

. 1 Referenc~ Thermometer is mercury-in-glass and ASTM certified. unl~ss otherwise noted. . i..".:
2 After each test run series, check the accuracy (and, hence, the calibration) of each thermocouple system at ambient
temperature. The temperature of the thermocouple and reference thermometers shall agree with:!:1°C. . .
3 The continuity check involves subjecting the tip of the thermocouple to a change in temperature ~eck
.
the crimps, loose
i
,i-

~;
connections. Thermocouples with crimps a~ose connections will not immediatelyrespond to t~~erajure c;ha~nd th.ose
with wrong connectiona will ,how an opppfsltq,j:hange In temperature.. -','

Calibrated By : 'BJVI~ C). /\'SI( . Checked By:


Signature Over Printed Name

Date:
e Over Printed Name
.-.01
1
'

:.'- :~.'~: -,

Environmental ,\{al1agelllem Service Provider

DIGITAL BALANCE CALIBRATION


Digital Balance ID DB - T3 Personnel EOA, CJG
Manufacturer Acculab Date 04 Januarv 2001
Model VI-1200' Calibration Standard 1000 g
Serial Number 0435BZ041 TVDe Weif!hts
- -- -~
0."'-- -

TEST
. DATE Calibration Digital Differenc 1,2 PASS/
--:'
POINT ~,
"',
NUMBER Calibrated Weights, <g} Response, (Q) { Qrams FAIL
1 04 Jan. 2007 1000 999.9 0.1 PASS
2
3'
4
5
6
7
8 '.
9
10 t,
1
Acceptable EPA Method 4 tolerance must be less than 0.5 gram.
2 Ac;:eptable EPA Method 5 tolera~ce mJJ.!itless than 0.5 gram.

Calibrated By : ~DD Q. 11.31!:. Checked By:


Signature Over Printed Name

Date: '

"
BERKMAN
SYSTffIlS,nu~.
Environmental Manogemenl Service Provider

NOZZLE CALffiRATION SHEET


Date EMV,OTR
Nozzle Box ID INCONEL
, -- -. -., -_.'.--.-. ..-- - -"--- - "-
- . u-

10 01 (mm) 02 (mm) D3 (mm) D (mm) Average


'>-..... . -(mm)
.-I
T4 NS-1 - 3..1(f 3.10 3.10 0.000 "3.10
T4 NS-2 4.76 4.76 4.76 0.000 4.76
,
T4 NS-3 6.36 6.35 6.35 0.010 6.35
T4 'NS-4 7..94 7.95 7.94 0.010 7.94
T4 NS-5 9.53 9.53 9.53 0.000 9.53
T4 NS-6 11.11 111.11 11.12 0.010 11..11
T4 N$-7 . 12.69 12.70 12.71 0.020 12.70

,
=
D Maximum difference in any two measurements. Tolerance-= 0.1 mm -.
. Average= Averageof D1.2.~ .

~~
Calibrated By: EN11.-M. V1u.A"'',/\:'\IA Checked By:
Sisnature Over Pnnted Name

Date:
BERKMANSYSTEMS,
INC.
Environmental NJanllgement Service Provider

TYPE-S PITOT TUBE CALIBRATION


I PITOT TUBE ID I PT-TA-16 J Probe Assembly ID I IPA,.T4-16

PARAlVIETER - . VALUE ALLOW ABLE RANGE


-
Assembly Level YES YES
HolesDamaaed.. NO NO
Obstructed NO NO
;,--
al 0° ..... - --.. -100a.1.+100 . - -.--.- u- ?
-.
- a2 .... . - --.. 0° -10°< a2<+100
r-
81 00
0"
-5°< 61<+5°
-5°< 6?-:+5°
L-
(32 ' .
'f
y ". 0" j l r-:-
6
.. ~
e .0" i;;.; ;.
t.
A 0.915" For X" OD, 0.526 to 0.750" ~
For3/" 00.0.788 to 1.125" ~
I.
Z =Asin Y 0.0 Z = oS0.125"
W = A sin e 0.0 w = s 0.031"
For X" 00, 0.263 to 0.375" F
PA 0.428"
For %" 00, 0.394 to 0.563"
0.487". For X" 00, 0.263 to 0.375"
PB For 3/8"OD 0.394 to 0.563"
PA - PB 0.059" -0.063 to 0.063" ~ ~.~
DT 0.372" 0.188 to 0.375"
Where: cx.1& a.2 = angles between the pitot tube opening and the horizontal plane when viewed from the end
~1& ~2 = angles between the pitot tube opening and the horizontal plane when viewed from the side
y= the angle measured when calculating the difference in length belweenthe two pitat tube legs
e =the angle measuredwhen calculatingthe distancethatthepitot tubes are rotated
. A =the distance between the tips of the pitot tube opening
Z =the difference in length between the two pitot ~ube legs.
W= the distance that the pitot tube legs are rotated '.
P A&PIF vertical distance between each pitot tube opening plane &the center line of the pitot tube
=
c.r the tube external diameter
Certification
I certIfythat the Type S pitot tl,lbemeets or exceeds allspecifications, criteria and lor applicable design
features and is hereby assigned a pitottube calibrationfactor (Cp) of 0.84.

Certified By: -~em,t.- ro. ,JViEV


Jr
SignatureOverPrintedName

Date: . tJ/-tY;-d7
J

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ANNEX E ~
~ ---. -~--. -- --- - . ,- . _..- .- .- --" n --- --- - q.-- ,.'.'-~.
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TEST PARTICIPANTS
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TEST PARTICIP ANTS

INTEGRATED WASTE MANAGEMENT, INC.


Engr. Bong Rivera Plant Administrator
Engr. Stephen C. Tronco Pollution Control Officer

JEFCOR LABORA TORI~S,INC.


Edna Callejas-Mijares PresidentlManaging Director
- - --,---Edgar H. RamirezU - -- -- n ,-, -,--
"',_n,~ nLaboratory,Manager--, " ,------

Engr. Ramer P. Bautista Environmental Officer


Adrian L. Furing Chemist
.~ >- .O&-'!::.
)~

Berkman Systems, Inc.


Jose VictorC.DelaAlas Operations Supervisor
Edindo C. Fernando Operations Asst. Supervisor
Joseph Rensis A. Rabago Field Technician
Eduardo O. Asis Field Technician
William T. Yumul Field Technician
Rolando S. Salazar Field Technician
Henry R. Bencito Field Technician
Jerry T. Somblingo Driver

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