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II
Matrix - '-Ni2AlTi
dislocations in superalloy
Foils 3 mm diam. disk very thin (<0.1 - 1 micron - depends on material, voltage)
if d = 2.5, = 0.288
= 2d sin d (2)
R/L = /d Rd = L
specimen
image plane
Get pattern of spots around transmitted beam from one grain (crystal)
[111] in cubic
[001] in hexagonal
l = +1 level
Some 0-level patterns thus exhibit higher rotational symmetry than structure has
0-level
l = -1 level
Ewald sphere
Find crystal system, lattice parameters, index pattern, find zone axis ACTF!!! Note symmetry - if cubic, what direction has this symmetry (mm2)? Reciprocal lattice unit cell for cubic lattice is a cube
Hafnium ()
See channels through foil Channels may be light or dark in image Usually do image simulation to determine features of structure
M23X6 (figure at top left). L21 type '-Ni2AlTi (figure at top center). L12 type twinned 'Ni3Al (figure at bottom center). L10 type twinned NiAl martensite (figure at bottom right).