Documente Academic
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Documente Cultură
Paul Schiffelbein
ASTM Committee Week
14 June 2006
Overview
Measurement system analysis (Round robin,
Interlaboratory Study (ILS), Interlaboratory
Comparison (ILC), Gage Study) description, definitions
and motivation
Round robin guidelines
Round robin logistics
Data Analysis
Precision and bias statement
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Long-term
Process
Variation
Short-term
Process
Variation
bias
Simple
Measurement
Variation
Variation
within a
Sample
Bias
Linearity
Variation
due to
Gage
Short-term
Stability
Variation
due to
Labs,
Operators,
Devices,
Time
Long-term
precision
Precision can be decomposed into short- and longterm (or narrow and wide) components.
Repeatability and reproducibility are used to
quantify this concept.
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ISO 5725-1
Repeatability: Precision under repeatability conditions
ISO 5725-1
Reproducibility: Precision under reproducibility conditions
ASTM/ISO Usage
Observed Process Variation
Actual Process
Variation
Long-term
Process
Variation
Short-term
Process
Variation
bias
Simple
Bias
Linearity
Measurement
Variation
Variation
due to
Gage
Variation
within a
Sample
Short-term
repeatability
Stability
Variation
due to
Labs,
Operators,
Devices,
Time
Long-term
reproducibility
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Long-term
Process
Variation
Short-term
Process
Variation
bias
Simple
Bias
Linearity
Measurement
Variation
Variation
due to
Labs,
Operators,
Devices,
Time
Variation
due to
Gage
Variation
within a
Sample
Short-term
repeatability
Stability
Long-term
reproducibility
Gage
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12
13
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Sigma 500
Lab A
Austria
Statimat
Lab B
Austria
Pre-twisted
Lab C
Europe
Statimattwisted
Uster
Lab D
USA
Pre-twisted
Lab E
Lab F
Statimattwisted
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Etc.
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paul.a.schiffelbein@usa.dupont.com
302/774-2417
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Instron
T T QRS
T FA
S p ru a n c e
T FA
S p ru a n c e
Ma in s ite
L e n zin g
T T QRS
T FA
250
S p ru a n c e B
260
S p ru a n c e A
B F(N )
310
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15
10
Ins tron
TT QRS
TFA
Spruance
TFA
Spruance
Mainsite
Lenzing
TT QRS
TFA
Spruance B
5
Spruance A
Std Dev
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R = 2L + 2r
Where:
Var Ratio
Device&Random
Laboratory[Device]&Random
Residual
Total
0.6823116
0.4806723
Var
Component
66.35
46.74
97.25
210.36
Repeatability variance
Std Error
95% Lower
95% Upper
Pct of Total
62.607
26.848
18.903
19.480
1854.81
224.123
31.5
22.2
46.2
100.0
Reproducibility variance
(one estimate)
Reproducibility variance
(another estimate)
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observed values are considered significantly different at the 95% probability level
if the difference between them exceeds the appropriate critical difference in the
table.
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13.3 Bias The procedure in this test method produces a test value that can be defined
only in terms of a test method. There is no independent referee method by which bias
may be determined. The test method has no known bias.
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Summary
Explicitly state objectives for your study, and
make sure all participants understand them
Write protocol covering responsibilities, timing,
samples and sample handling, test equipment and
set-up, sampling plan, properties, units, etc.
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Thank you
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