Unit 2 3 4

FATTY ACID
DEPARTMENT
RENITA DYAH A.
UOI TRAINEE
UNIT 2
SWEET WATER PURIFICATION
2
Storing
Crude Sweet Water
Filtering Filter 100µm
Sweet Water Heater

Adding
HCL
Adding Air
from Acid Reactor
compressor
Adding Reaction
FeCl3 Vessel
Adding Filter
Aid Solution
Adding NaOH
Solution
Filtering (filter press)
Treated Sweet
Water Receiving
Filtering Strainer
25µm
Storing Purified
sweet water
3
UTILITIES CONSUMPTION :
Utilities (consumption per ton feed) :
1. POWER : 1.5 kWh
2. LP STEAM : 75 kg
3. INSTRUMENT AIR : 0.5 Nm3
4. COMPRESSED AIR : 40 Nm3
Chemicals (consumption per ton feed) :
1. Hydrochloric acid 100% : 1.8 kg (5 kg 36%)
2. Ferric chloride 100% : 1.8 kg
3. Caustic soda 100% : 2.4 kg
4. Filter aid : 1.2 kg
Waste : solid from filter (2-3 kg : 7% glycerol, 45% water)
5
2-D-1 2-PD-1
TK-1003 A
2-F-1 A/B 2-E-1 2-MX-1
FA to B.L 2-P-1
2-D-2 2-R-1 2-D-7
2-P-4 2-P-5
2-R-2
A/B/C
2-F-2 A
2-P-2
2-F-2 B
Disposal
2-D-5
2-D-6 2-P-3 2-F-3 A/B TK-1004 A/B

7
CRUDE SWEET WATER TANK
Tag Name : TK-1003 A

Function : menyimpan crude sweet water dari Unit 1
Capacity : 500 MT
Location : Tank Farm 2
Op condition : ATM, 55oC
Vendor : Maju Bersama
8
9
PRETREATED SWEET WATER TANK
Tag Name : TK-1004 A/B

Function : menyimpan pretreated sweet water dari Unit 2
Capacity : 250 MT
Op condition : ATM, pH : 6-7.5
10
11
SKIMMED FATTY ACIDS PUMP
Tag Name : 2-P-1

Function : mengalirkan fatty acid dari acid reactor
(2-R-1) menuju ke battery limit
Type : centrifugal
Brand : CDR pump
Capacity : 5 m3/h
Head : 46 m
12
SWEET WATER TO FILTRATION PUMP
Tag Name : 2-P-2

Function : mengalirkan sweet water dari reaction
vessels (2-R-2 A/B/C) menuju ke sweet water
filter (2-F-2 A/B)
Type : centrifugal
Brand : KSB pump
Capacity : 15 m3/h
Head : 45 m
Rotation : 2971 rpm
13
TREATED SWEET WATER PUMP
Tag Name : 2-P-3

Function : mengalirkan sweet water dari precoat vessel
(2-D-6) menuju ke product filter (2-F-3 A/B)
Type : centrifugal
Brand : KSB pump
Capacity : 30 m3/h
Head : 45 m
Rotation : 2972 rpm
14
FERRIC CHLORIDE PUMP
Tag Name : 2-P-4

Function : mengalirkan ferric chloride dari ferric
chloride tank (2-D-2) menuju ke reaction
vessels (2-R-2 A/B/C)
Type : metering
Brand : CDR pump
Capacity : 5 m3/h
Head : 25 m
15
SODA ASH MIXING PUMP
Tag Name : 2-P-5

Function : mengalirkan NaOH dari storage (2-D-7)
menuju ke reactor vessel (2-R-2 A/B/C)
Type : centrifugal
Brand : KSB pump
Capacity : 2 m3/h
Head : 26 m
Rotation : 2936 rpm
16
ACID DOSING PUMP
Tag Name : 2-PD-1

Function : mengalirkan HCl 36% suhu 45oC dari
hydrochloric acid tank (2-D-1) menuju ke mixer
(2-MX-1)
Type : metering
Brand : LEWA
Weight : 46 kg
Power : 0.37 kW
Internal PRV pressure : 7 bar
17
ACID REACTOR
Tag Name : 2-R-1

Function : memisahkan fatty acid terikut dari sweet
water, dengan menambahkan HCl 36%
Type : horizontal prismatic with internals
Brand : YUNKU
Capacity : 24.2 m3 (netto) 31.5 m3 (total)
Dimension : 7 x 3 x 1.5 m (L x W x H)
Temp (op/design) : 80/100oC
Press (op/design) : ATM
Fluid : acidified sweet water
18
REACTION VESSELS
Tag Name : 2-R-2 A/B/C
Function : menetralkan sweet water yang
keluar dari acid reactor, dengan
menambahkan NaOH dan FeCl3
Type : vertical cylindrical with compressed
air distributor
Brand : YUNKU
Dimension : D 2.5 m, H 7.6 m
Press (op/design) : full liquid
Fluid : sweet water
19
SWEET WATER HEATER
Tag Name : 2-E-1

Function : menaikkan suhu sweet water dari 45oC
menjadi 90oC
Type : shell and tubes
Brand : Jutasama
Volume : 0.11 m3 (shell) & 0.06 m3 (tube)
Pressure Temperature (max/min)

Design Operation Design Operation
(barg) (barg) (oC) (oC)
Shell 4.5/FV 3.5 180/14 138
Tube 5 4 150/14 80/30
20
HYDROCHLORIC ACID TANK
Tag Name : 2-D-1

Function : menyimpan chemical hydrochloric acid
Type : vertical
Brand : YUNKU
Dimension : 1 m (D) & 1.6 m (H)
Temp (op/design) : AMB
Fluid : Hydrochloric acid 36%
21
FERRIC CHLORIDE TANK
Tag Name : 2-D-2

Function : menyimpan chemical ferric chloric
Type : vertical
Brand : YUNKU
Dimension : 1 (D) & 1.6 m (H)
Temp (op/design) : AMB
Fluid : ferric chloric
22
PRECOAT VESSEL
Tag Name : 2-D-5

Function : melapisi umpan yang akan masuk
filter press dengan filter aid
Type : vertical with agitator
Manufacturer : Wuxi Chemical Equipment CO.LTD
Volume : 4 m3
Weight (empty) : 1020 kg
Temp (op : design (max/min)) : 70 : 100/14oC
Fluid : process water
Density : 1100 kg/m3 (70oC)
24
TREATED SWEET WATER RECEIVER
Tag Name : 2-D-6

Function : receiver sweet water hasil dari filter
press (2-F-2 A/B)
Type : vertical
Volume : 2.2 m3
Press (op/design) : ATM / 0.45 barg (int/ext)
Fluid : sweet water
25
SODA VESSEL
Tag Name : 2-D-7
Function : storage of NaOH 48%W
Type : vertical
Volume : 6.11 m3
Temp (op : design) : 30 : 50/14oC
Location : EL 0
26
HYDROCHLORIC ACID MIXER
Tag Name : 2-MX-1

Function : mencampur sweet water dengan HCl 36%
Type : static
Brand : AXFLOW
Press. design : 5 barg
Temp. design : 100oC
27
INLET PRODUCT FILTER
Tag Name : 2-F-1 A/B

Function : menyaring sweet water dari TK-
1003 A, yang akan menjadi umpan
heater (2-E-1), ukuran 100 µm
Type : basket
Brand : Fluxa Filtri
Capacity : 29 liter
Press. design : 5 bar
Temp. design (min/max) : 0/100oC
Fluid : body sweet water
28
SWEET WATER FILTER
Function : memisahkan sweet water dengan
cake yang terbentuk setelah
reaksi pada 2-R-2 A/B/C
Type : press (including drip pan)
Brand : PMI
Capacity : 620 liter
Weight : 79 kg (empty) 92.4 kg (operation)
No of filtration chamber : 40
Depth of chamber : 32 mm
Filter area : 41 m2
Filtration pressure : 6 bar
29
PRODUCT FILTER

Function : menyaring sweet water dari proses,
sebelum disimpan di TK-1004 A/B,
ukuran 25 µm
Type : basket
Capacity : 40 liter
Press. design : 7 bar
Fluid : body sweet water
30
UNIT 3
SWEET WATER EVAPORATION
31
Storing Purified sweet water
Heat Recovery
Exchanger
Evaporasi 1
Evaporasi 2
Evaporasi 3
Evaporasi 4
Storing
Crude
Glycerine
32
UTILITIES CONSUMPTION :
Utilities (consumption per ton feed) :
1. STEAM : 205 kg
2. POWER : 0.5 kWh
3. COOLING WATER : 24 m3
4. INSTRUMENT AIR : 0.5 Nm3
Waste (vacuum system) : 250 kg (BOD : 2000 ppm)
Glycerine content in liquid effluent : 0.15%
34
MS 3-J-3
3-J-2 3-E-3
3-J-1
3-E-2
3-D-1 3-D-2 3-D-3 3-D-4
3-D-6 3-D-7
3-E-1
1-D-6 3-P-1 3-D-5 3-P-3 1-D-6
TK-1004 A/B
3-P-2 TK-1005 A/B

PRETREATED SWEET WATER TANK

Function : menyimpan pretreated sweet water dari Unit 2
Capacity : 250 MT
Op condition : ATM, pH : 6-7.5
37
38
CRUDE GLYCERINE TANK

Function : menyimpan crude glycerine 88% dari Unit 3
Capacity : 500 MT
Op condition : ATM, 65-75oC, pH : 6-7.5
39
40
CONDENSATE PUMP
Tag Name : 3-P-1

Function : memindahkan condensate dari vessel 3-D-5
menuju ke vessel 1-D-6 untuk digunakan splitter
Type : centrifugal
Brand : KSB pump
Capacity : 9 m3/h
Head : 40 m
Rotation : 2966 rpm
41
CRUDE GLYCERINE PUMP
Tag Name : 3-P-2

Function : memindahkan crude glycerine 88% dari
fourth calandria ke TK 1005 A/B
Type : centrifugal
Brand : KSB pump
Capacity : 5 m3/h
Head : 40 m
Rotation : 2966 rpm
42
CONDENSATE RECOVERY PUMP
Tag Name : 3-P-3

Function : memindahkan hot water dari hot well (3-D-6)
menuju vessel (1-D-6)
Type : centrifugal
Brand : KSB pump
Capacity : 4 m3/h
Head : 25 m
Rotation : 2927 rpm
43
HEAT RECOVERY EXCHANGER
Tag Name : 3-E-1
Function : menaikkan suhu pretreated sweet
water dari 50oC menjadi 108oC
Brand : AMC
44
Dimension :
Parameter
Diameter Shell side Tube
OD. mmside
D. 150oC 120oC
508
Temperature
Height/length 5500 mm
W. Heating
Pressuresurface
3 bar(g)
area 6 bar(g)
63 m2
D. Weight
Pressure 8/FV bar(g)1764.4
(empty) 8/FV
kgbar(g)
FIRST SURFACE CONDENSER
Tag Name : 3-E-2

Function : mengkondensasi uap dari calandria
Brand : AMC
Dimension :
Diameter
Parameter Shell side ID.
Tubemm
side
1150
D. 130oC 80oC
Height/length
Temperature 4000 mm
Heating surface 2
W. Pressure -0.9area
bar(a) 293 m
3 bar(a) 45
SECOND SURFACE CONDENSER
Tag Name : 3-E-3

Function : mengkondensasi uap dari 3-J-2
Brand : AMC
Dimension :
Diameter OD. 273.1 mm
Parameter Shell side Tube side
D. 220oC 135oC
Heating Temperature
surface area 4.54 m2
Weight (empty)
W. Pressure 351.2 kg 2 bar(g)
0.3 bar(g)
46
D. Pressure 1/FV bar(g) 6/FV bar(g)
FIRST CALANDRIA
Tag Name : 3-D-1
Function : memekatkan sweet water dari 30%
menjadi 35%
Type : vertical with heat exchanger
circulation loop
vapor disengaging section
Brand : WCE
Dimension : 508 mm (OD-shell)
42.2 mm (OD-tube)
2500 mm (L)
2 mm (tw)
Heat surface area : 124.3 m2 47
Pressure Temperature (max/min)
Shell 7/FV 5 190/14 170/160
Tube 5/FV 2 170/15 130 48
SECOND CALANDRIA
Tag Name : 3-D-2
menjadi 41.5%
Type : vertical with heat exchanger, circulation
loop, vapor disengaging section
Brand : WCE
42.2 mm (OD-tube)
2500 mm (L)
2 mm (tw)
Heat surface area : 125.1 m2
Operating fluida : steam/condensate (shell)
vapour (tube) 49
Pressure (max/min) Temperature (max/min)
Shell 5/FV 170/14 130
Tube 3/FV 160/14 120 50
THIRD CALANDRIA
Tag Name : 3-D-3
Function : memekatkan sweet water dari 41.5%
menjadi 54%
Brand : WCE
42.2 mm (OD-tube)
2500 mm (L)
2 mm (tw)
vapour (tube) 51
Shell 3/FV 0.8 160/14 114
Tube 1.5/FV -0.2 145/14 101 52
FOURTH CALANDRIA
Tag Name : 3-D-4
menjadi 88%
Brand : WCE
42.2 mm (OD-tube)
2500 mm (L)
2 mm (tw)
vapour (tube) 53
Shell 1.5/FV -0.2 145/14 96
Tube 0.5/FV -0.9 130/14 90 54
CONDENSATE VESSEL
Tag Name : 3-D-5

Function : menampung condensate dari calandria
Type : vertical
Volume : 3.4 m3
Press (op/design) : -0.2 / 1.5/FV barg
Fluid : hot water
55
HOT WELL
Tag Name : 3-D-6
Function : menampung condensate dari 3-E-2
dan 3-E-3
Type : vertical
Volume : 0.5 m3
Temp (op/design) : 40/ 100/14oC
56
HOT WELL
Tag Name : 3-D-7

Function : menampung condensate dari 3-J-3
Type : vertical
Volume : 0.5 m3
Temp (op/design) : 40/ 100/14oC
57
STEAM COMPRESSOR
Tag Name : 3-J-1

Function : membuat vacuum system pada calandria
Type : steam jet
Manufacturer : GEA Wiegand GmbH
Volume (1/2) : 7.2/5.1 liter
Temp. design (1/2) : -10/220oC / 10/220oC
Press. design (1/2) : FV/8 / FV/18
58
EJECTORS
Tag Name : 3-J-2

Type : steam jet
Volume : 2.3 liter
Weight : 35 kg (empty) 37.3 kg (full)
Press. design : -1/1 barg
59
EJECTORS
Tag Name : 3-J-3

Type : steam jet
Volume : 0.1 liter
Weight : 10.7 kg (empty) 10.8 kg (full)
60
UNIT 4
GLYCERINE DISTILLATION
& REFINING
61
Storing
Crude Glycerine
Adding
NaOH
Solution
pre-Heating
Deaerator
Reboiler
Glycerine Distillation
Column
Secondary Adding
Distiller Deodoriser Low

Steam
Scrubber Cooling
cooling
Adding
Bleaching Activated
carbon
Storing Industrial
Storing Crude Grade Glycerine
Pitch Filtering Filter 5 µm
Sweet Water Glycerine
Cooling
Storing Pharma
Grade Glycerine
62
UTILITIES CONSUMPTION (USAGE/TON FEED) :
Utility UoM STD KPI STD DBI
Medium Steam Ton 1.2 1.25
Cooling Water m3 85 85
Soft Water m3 0.015 -
Filter Water m3 0.015 -
Power kWh 31.9 27
Compressed Air Nm3 - 1
Instrument Air Nm3 - 1
Nitrogen Nm3 3.5 -
Chemical
Caustic Soda kg 4.2 2
Activated Carbon kg 2 2
Waste :
Water vacuum system : 600 kg (BOD : 3000 ppm)
Glycerine content in liquid effluent : 0.25%
Exhausted carbon : 2-3 kg
64
pH : 4.5-7.5
Flow NaOH
(FIQ 0410)
16-64 kg/h
BOD : 3000 ppm (STD)

% gly : 0.3%
source : Quality date 3 Jan-1 Feb 2016
66
Exhausted carbon
2-3 kg (STD)
67
TK-1005 A/B
4-MX-1 4-E-1 4-D-1 4-P-1 4-E-2 4-C-1 4-D-3
4-P-4
4-PD-1
4-E-6 3-E-1
4-D-2
68
4-C-2 4-P-3 4-E-5 TK-810
4-C-1 4-C-3 4-P-5 4-E-7 4-D-4/5/6 4-F-1 A/B 4-E-8
TK-809 A/B
4-E-4 A/B 4-E-3 4-P-7 Recycle to TF
Pitch
69
S
4-J-1 4-J-2 4-J-3 4-J-4
4-D-1 4-C-2 4-E-9 4-E-10
4-D-10
70
CRUDE GLYCERINE TANK
Function : storage of crude glycerine 88%
Capacity : 500 MT
Dimension : Dia : 7.994 mm
Height : 12.200 mm
Weight (kg) : 34450 (empty), 634450 (full water)
MOC : SA 516 GR.70
Fluid : crude glycerine
Specific gravity : 1.2
Pressure (kg/cm2) Temperature (oC)

Parameter pH
Vessel Coil Vessel Coil
Design ATM 3.5 80-100 100 -
Operating ATM 3.06 70 90 -
Quality
ATM - 65-75 - 6-7.5
Plant
71
73
PHARMA GLYCERINE TANK
Function : storage of pharma grade glycerine
Capacity : 250 MT
Height : 10.650 mm
MOC : SA 240 304
Fluid : 1st grade glycerine
Parameter
Design 0.05 3.5 80-100 100
Operating 0.025 3.06 65 90
Dia : 5.997 mm Quality

ATM - 45-55 -
Height : 10.650 mm Plant
Product Specification (source : Quality Plant) :
Flowrate : 1500-7700 kg/h
APHA color : 10 max
Moisture : 0.2% max
Glycerine : 99.5% min
pH : 6-7.5
74
75
SECOND GRADE GLYCERINE TANK
Function : storage of second grade glycerine
Capacity : 15 MT
Height : 3.025 mm
MOC : SA 240 304
Fluid : 2nd grade glycerine

Parameter
Design 0.05 3 80-100 120
Operating 0.025 2 60 90 Dia : 2.504 mm

Quality Height : 3.025 mm
ATM - 40-55 -
Plant
Product Specification (Resource : Quality Plant) :

Flowrate : 50-225 kg/h
APHA color : 40 max
Moisture : 7% max
Glycerine : 93-95%
76
77
COLUMN FEED PUMP
Tag Name : 4-P-1
Function : transfer crude glycerine from deaerator (4-D-1) to reboiler (4-E-2)
Type : centrifugal
Brand : KSB pump
Capacity : 180 m3/h
Head : 25 m
Rotation : 1470 rpm
Location : EL 0
78
SECOND GRADE GLYCERINE PUMP
Tag Name : 4-P-3
Function : transfer second grade glycerine from scrubber (4-C-2) to cooler (4-E-5)
Type : centrifugal
Brand : KSB pump
Capacity : 45 m3/h
Head : 35 m
Rotation : 2970 rpm
Location : EL 0
80
PUMPAROUND PUMP
Tag Name : 4-P-4
Function : transfer crude glycerine from pumparound receiver (4-D-3) to heater (3-E-1)
Type : centrifugal
Brand : KSB pump
Capacity : 110 m3/h
Head : 37 m
Rotation : 1484 rpm
Location : EL 0
81
FIRST GRADE GLYCERINE PUMP
Tag Name : 4-P-5
Function : transfer first grade glycerine from deodoriser (4-C-3) to cooler (4-E-7)
Type : centrifugal
Brand : KSB pump
Capacity : 5 m3/h
Head : 55 m
Rotation : 2963 rpm
Location : EL 0
82
SODA DOSING PUMP
Tag Name : 4-PD-1
Function : mentransfer NaOH dari storage 4-D-2 menuju mixer 4-MX-1
Type : reciprocating
Brand : LEWA
Flow (max) : 48.20 liter/h
Power : 0.37 kW
Weight : 81 kg
Fluid : NaOH 50% (45oC)
Location : EL 0
84
RECYCLING GLYCERINE PUMP
Tag Name : 4-P-7
Function : recycle to tank farm from stripped glycerine condenser (4-E-3)
Type : gear
Brand : LEWA
Flow (max) : 616 liter/h
Power : 2.20 kW
Fluid : stripped glycerine (max 80oC)
Location : EL 0
85
DISTILLATION TOWER
Tag Name : 4-C-1
Function : distilled from crude glycerine into glycerine pharma min 99.5%
Type : structured packing (tw : 0.15 mm)
Manufacturer : Jutasama
Pressure Temperature
MOC : SS 304L Parameter
(bar) (oC)
Volume : 85.5 m 3
Design FV/0.45 (g) 15/205
Location : EL 12.000 Operating 0.004 (a) 155
86
SCRUBBER
Tag Name : 4-C-2
Function : separate second grade glycerine product with vapour
Manufacturer : Jutasama
MOC : SS 304L Parameter Pressure (barg) Temperature (oC)
Volume : 15.1 m3
shell coil shell coil
Location : EL 24.000 Design 0.45/FV 5/FV 140/14 159
Operating FV 3 60 145
87
DEODORISER
Tag Name : 4-C-3
Function : reduce odor in pharma glycerine
Manufacturer : Jutasama]
MOC : SS 304L
Volume : 2.12 m3
Temp (op/design) : 145 /160oC
Press (op/design) : 3 mmHG barg / 1.5/FV barg
Location : EL 6.000
88
CRUDE GLYCERINE HEATER
Tag Name : 4-E-1
Function : menaikkan suhu crude glycerine 70oC menjadi 90oC
Type : shell and tubes (SS 316L)
Brand : AMC
Location : EL 18.000 Parameter Shell side Tube side
Dimension : D. Temperature 180oC 150oC
Diameter OD. 356 mm
W. Pressure 3.5 bar(g) 3.0 bar(g)
D. Pressure 4.5/FV bar(g) 3.5/FV bar(g)
Heating surface area 19.93 m2
Fluid LP steam/LP crude
Weight (empty) 863.3 kg condensate glycerine
89
REBOILER
Tag Name : 4-E-2
Function : increase temperature of crude glycerine, before entered 4-C-1
Brand : AMC
Location : EL 12.000
Dimension : Parameter Shell side Tube side
Diameter OD. 508 mm D. Temperature 220oC 205oC
Height/length 4000 mm W. Pressure 14 bar(g) 0.5 bar(g)
Heating surface area 72.8 m2 D. Pressure 18/FV bar(g) 1.5/FV bar(g)

Weight (empty) 2060.2 kg Fluid MP steam/condensate glycerine
90
STRIPED GLYCERINE CONDENSER
Tag Name : 4-E-3
Function : decrease temperature of stripped glycerine from 4-C-2
Brand : AMC
Dimension :
D. Temperature 205oC 80oC
Diameter OD. 550 mm
W. Pressure 0.07 bar(g) 4 bar(g)
D. Pressure 0.45 bar(g) 9 bar(g)
Weight (empty) 922.9 kg Fluid Stripped glycerine Tempered water
91
SECONDARY DISTILLERS
Tag Name : 4-E-4 A/B
Function : separate pitch after distilled
Type : vertical with steam coil and sparger (SS 316L)
Brand : AMC
Location : EL 6.000
Parameter Shell side Coil side
Dimension :
Diameter ID. 1650 mm
W. Pressure FV bar(g) 13 bar(g)
D. Pressure 0.45/FV bar(g) 18/FV bar(g)
Heating surface area 22 m2
Weight (empty) 2291.4 kg Fluid Glycerine/pitches Steam
92
SECOND GRADE GLYCERINE COOLER
Tag Name : 4-E-5
Function : decrease temperature of 2nd grade glycerine up to 60oC
Type : plate (welded type)
Brand : API-Schmidt
Volume chamber (1/2) : 13/14 liter
Press chamber (1/2) min/max : -1/7.5 bar
Temp chamber (1/2) min/max : 5/140oC
Location : EL 6.000
93
PUMPAROUND COOLER
Tag Name : 4-E-6
Function : decrease temperature and back to 4-C-1
Brand : API-Schmidt
Press chamber (1/2) min/max : -1/9 bar
Location : EL 6.000
94
DISTILLED GLYCERINE COOLER
Tag Name : 4-E-7
Function : decrease temperature of distilled glycerine from 146oC using
tempered water
Brand : API-Schmidt
Press chamber (1/2) min/max : -1/9 bar
Location : EL 6.000
95
FIRST GRADE GLYCERINE COOLER
Tag Name : 4-E-8
Function : decrease temperature of 1st grade glycerine from 80oC to 65oC
using tempered water
Brand : API-Schmidt
Press chamber (1/2) min/max : 0/9.5 bar
Location : EL 6.000
96
FIRST SURFACE CONDENSER
Tag Name : 4-E-9
Function : condensing vapour from 4-J-1, 4-J-2, and 4-D-1
Brand : AMC
Dimension :
Diameter ID. 1050 mm
W. Pressure 88 mbara 2 bar(g)
D. Pressure 1/FV bar(g) 6/FV bar(g)
Weight (empty) 8349.6 kg Fluid Inert & water Cooling water
97
SECOND SURFACE CONDENSER
Tag Name : 4-E-10
Function : mengkondensasi uap dari 4-J-3
Type : shell and tubes (A 516 GR 70)
Brand : AMC Parameter Shell side Tube side
Dimension : D. Temperature 220oC 150oC
Diameter OD. 324 mm W. Pressure 0.3 bar(a) 2 bar(g)
Height/length 2000 mm D. Pressure 1/FV bar(g) 6/FV bar(g)
Heating surface area 8.11 m2 Fluid Inerts & water Cooling water
Weight (empty) 426 kg
98
DEAERATOR
Tag Name : 4-D-1
Function : remove dissolved gasses
Type : vertical (SS 304L)
Volume : 3.61 m3
Press (op/design) : FV / 0.45/FV barg
Fluid : glycerine
99
PUMPAROUND RECEIVER
Tag Name : 4-D-3
Function : receiver to return 4-C-1
Volume : vessel : 1.7m3, coil 0.01 m3
Design. Press : vessel 1.5/FV barg, coil 4.5/FV barg
Design. Temp (max/min) : shell 150/14oC, coil 180oC
Op. Press : vessel FV, coil 3 barg
Op. Temp : vessel 120oC coil 150oC
Fluid : vessel : glycerine, coil : steam
100
BLEACHER
Tag Name : 4-D-4/5/6
Function : reduce odor and color using activated carbon
Manufacturer : AMC
Capacity : 17.4 m3
Dimension : ID 1700 mm, H 7100 TL mm
Weight (empty) : 5920.8 kg
Temp (design) : 100oC
Press (op/design) : 6 bara / 8.5/FV barg
Fluid : glycerine pharma grade
101
HOT WELL
Tag Name : 4-D-10
Function : receiver of hot water
Type : vertical (SA 240 316L)
Volume : 0.5 m3
Location : EL 0
103
BOOSTER
Tag Name : 4-J-1
Function : supply steam to system
Type : steam jet
Volume (1/2) : 920/535 liter
Weight (empty/full) : 1044/2511 kg
Temp. design (1/2) : 220oC / 220oC
Press. design (1/2) : -1/1 / -1/0.5 barg
104
BOOSTER
Tag Name : 4-J-2
Function : supply steam to system
Type : steam jet
Volume : 480 liter
Weight (empty/full) : 489/972 kg
105
STEAM EJECTORS
Tag Name : 4-J-3
Function : vacuum system
Type : steam jet
Volume : 3 liter
Weight : 44 kg (empty) 47 kg (full)
106
STEAM EJECTORS
Tag Name : 4-J-4
Function : vacuum system
Type : steam jet
Volume : 0.5 liter
Weight : 22 kg (empty) 22.5 kg (full)
107
POLISHING FILTER
Function : filter 5µm of pharma grade glycerine
Type : catridge
Capacity : 16 liter
Press. design : 9.5 bar
Fluid : body glycerine
Location : EL 6.000
108
CHEMICAL
FOR UNIT 2, 3, & 4
109
CAUSTIC SODA (NaOH)
Supplier : AKR dan Lautan Luas
Test Specification
Parameter Result
Methods min max
Purity, % wt JIS K 1200-1968 48.00 - 48.47
Density at 30 deg C, g/ml JIS K 1200-1968 1.500 - 1.505
Carbonate as Na2CO3, % wt JIS K 1200-1968 - 0.12 0.0540
Sulphate as SO4, % wt ASTM E 1787-96 - 0.01 0.00170
Chlorate as NaClO3, ppm ASTM E 1787-96 - 65 7.886
Chloride as NaCl, % wt JIS K 1200-1968 - 0.01 0.00552
Iron as Fe, ppm JIS K 1200-1968 - 5 1.087
Silica as SiO2, ppm JIS K 1200-1968 - 20 1.797
Heavy metal as Pb, ppm ICP OES NA 0.112
Appearance By visual Clear & NSM Clear & NSM
110
HYDROCHLORIDE ACID (HCl)
Supplier : AKR dan Lautan Luas
Test Specification
Parameter Result
Methods min max
Purity, % wt ASTM E 224-96 32.00 - 33.44
Density at 30 deg C, g/ml ASTM E 224-96 1.150 - 1.161
Free Chlorine, ppm ASTM E 224-97 - 75 0.0019
Iron as Fe, ppm ASTM E 224-99 - 10 0.135
Color, APHA ASTM E 224-99 NA 10.405
Appearance Visual - - Light Yellow
111
FERRY CHLORIDE (FeCl3)
Supplier : Lautan Luas dan Bintang Mitra
Parameter Specification Result

Appearance Dark Brown Liquid Dark Brown Liquid
Specific Gravity 1.43 min 1.44
FeCl3 % (W/W) 40.00 min 41.41
FeCl2 % (W/W) 0.25 max 0.19
Free HCl Acid % (W/W) 0.25 max 0.01
112
Parameter Limit Result
FILTER AID
Color White to off-White White
Supplier : Perlite Makmur Mandiri
G.E. Brighteness 76 min 90
Specific Gravity 2.20-2.45 2.34
Density, kg/m3
Dry Loose (bulk) 110-130 119
Dry Tamped 185-220 188
Wet 210-250 217
Water Permeability 0.65-0.91 0.80
pH Value 6.0-7.8 7.67
Organic Mater N N
Hygroscopicity N N
Particle Size Distribution, % wt retention
100 mesh 5 max 1.0
140 mesh 10 max 3.6
200 mesh 5 max 5.0
325 mesh 15-30 20.6
>325 mesh 55-80 66.8 113

ACTIVATED CARBON
Supplier : Calgon Carbon, Cabot Norit, Ikaindo
Property STD DBI Result
Apparent density dry (gr/ml) 0.50 0.49
Iodine number (mg/l) 1020 min 1019
Molasses number 230 min 233
Abrasion number 75 min 80
Mean particle diameter (mm) 0.9 to 1.1 1.2
% moisture (as packaged) 2% max 1
% +10 mesh 5% max 2
% -40 mesh 4% max 0.0
Acid sol. Ash, % - 0.2
Acid sol. Iron, % as Fe - 0.01
pH - 5.9
Total surface area (m2/g) 1000 to 1100 -
Pore volume (ml/g) 0.95 -
114

Unit 2 3 4

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FATTY ACID

Filtering Filter 100µm

Sweet Water Heater

2-D-6 2-P-3 2-F-3 A/B TK-1004 A/B

Tag Name : TK-1003 A

Tag Name : TK-1004 A/B

Tag Name : 2-P-1

Tag Name : 2-P-2

Tag Name : 2-P-3

Tag Name : 2-P-4

Tag Name : 2-P-5

Tag Name : 2-PD-1

Tag Name : 2-R-1

Tag Name : 2-E-1

Pressure Temperature (max/min)

Tag Name : 2-D-1

Tag Name : 2-D-2

Tag Name : 2-D-5

Tag Name : 2-D-6

Tag Name : 2-MX-1

Tag Name : 2-F-1 A/B

Tag Name : 2-F-3 A/B

3-D-1 3-D-2 3-D-3 3-D-4

3-P-2 TK-1005 A/B

Tag Name : TK-1004 A/B

Tag Name : TK-1005 A/B

Tag Name : 3-P-1

Tag Name : 3-P-2

Tag Name : 3-P-3

Tag Name : 3-E-2

Tag Name : 3-E-3

Tag Name : 3-D-5

Tag Name : 3-D-7

Tag Name : 3-J-1

Tag Name : 3-J-2

Tag Name : 3-J-3

Distiller Deodoriser Low

BOD : 3000 ppm (STD)

4-MX-1 4-E-1 4-D-1 4-P-1 4-E-2 4-C-1 4-D-3

4-C-1 4-C-3 4-P-5 4-E-7 4-D-4/5/6 4-F-1 A/B 4-E-8

4-E-4 A/B 4-E-3 4-P-7 Recycle to TF

4-J-1 4-J-2 4-J-3 4-J-4

4-D-1 4-C-2 4-E-9 4-E-10

Pressure (kg/cm2) Temperature (oC)

Design ATM 3.5 80-100 100 -

Operating ATM 3.06 70 90 -

Design 0.05 3.5 80-100 100

Operating 0.025 3.06 65 90

Dia : 5.997 mm Quality

Pressure (kg/cm2) Temperature (oC)

Design 0.05 3 80-100 120

Operating 0.025 2 60 90 Dia : 2.504 mm

Product Specification (Resource : Quality Plant) :

Dimension : Parameter Shell side Tube side

Diameter OD. 508 mm D. Temperature 220oC 205oC

Height/length 4000 mm W. Pressure 14 bar(g) 0.5 bar(g)

Heating surface area 72.8 m2 D. Pressure 18/FV bar(g) 1.5/FV bar(g)

Weight (empty) 922.9 kg Fluid Stripped glycerine Tempered water

Weight (empty) 2291.4 kg Fluid Glycerine/pitches Steam

Weight (empty) 8349.6 kg Fluid Inert & water Cooling water

Diameter OD. 324 mm W. Pressure 0.3 bar(a) 2 bar(g)

Height/length 2000 mm D. Pressure 1/FV bar(g) 6/FV bar(g)

Weight (empty) 426 kg

Purity, % wt JIS K 1200-1968 48.00 - 48.47