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Air Sampling
Difficult because ever changing concentrations
Large sample is required
Automatic online sampling and detection
High sampling rate (0.003-3 m3/min)
Duration
No of samples
Size of samples
Duration
Air and Gas Analysis
Air Sampling methods
Cryosampling
Absorption on to solvents
Partitioning the pollutants in solvents
Absorption on to solids
SPE
SPME
Passive air samplers
Denuders
Use of diffusion to separate air from particles
Diffusion scrubbers
Use of diffusion filters to separate air from particles
Air and Gas Analysis
SPME adsorption
Denuders
Diffusion scrubbers
Air and Gas Analysis
Methods of analysis
Available techniques
Flame photometry
Gas chromatography
Spectrophotometry
Electrochemical methods
Air and Gas Analysis
+SO2 + H+
Air and Gas Analysis
Chemiluminescent
Spetrophotometry (azodye formation)
Spetrophotometry
Gasphase spectroscopy
NO +O3 NO2* + O2
Carbon monoxides
By non dispersive IR spectrometry
Air and Gas Analysis
Carbon monoxides
By non dispersive IR spectrometry
Air and Gas Analysis
Carbon monoxides
By flame ionization GC
Air In
Air and Gas Analysis
Determination of hydrocarbons.
By flame ionization detector
By nondispersive IR technology
Use stripper column to remove water, CO2 and non methane
hydrocarbons to separate from CH4 and CO.
Air and Gas Analysis
Particle analysis :
Appropriate digestion/extraction for chemical analysis
Wave length dispersive x-ray fluorescence spectrometer
Mass spectral analysis (Drift tube ion mobility mass
spectrometry)
Air and Gas Analysis