Documente Academic
Documente Profesional
Documente Cultură
www.elsevier.com/locate/foodqual
a,*
Laboratorio de Analisis Sensorial, Facultad de Farmacia, Universidad del Pas Vasco/Euskal Herriko Unibertsitatea,
Paseo de la Universidad, 7, 01006 Vitoria, Gasteiz (Alava), Spain
Consejo Regulador de la Denominacion de Origen Queso Idiazabal, Granja Modelo de Arkaute, Apartado 46, Arkaute (Alava), Spain
Available online 20 May 2006
Abstract
The standardization and accreditation of sensory quality evaluation methods is a pressing need for the certication of food products,
particularly for foods and beverages with specic sensory characteristics, such as those with a protected designation of origin (PDO).
This study describes a proposal for the development of accredited sensory evaluation methods, showing as an example an application
from a specic certied product (PDO Idiazabal cheese). A training and qualication process for expert panelists is required. In cheese,
panelists score quality of overall sensory parameters (shape, rind, paste colour, eyes, odour, texture, avour and aftertaste) on a scale,
based on how close the product lies to a specic quality standard. Panelists justify the quality scores given on the basis of the absence/
presence of specic characteristics in the product and/or the presence of defects. Training requires the prior establishment of references
for both characteristics and defects. Qualication trials determine whether or not the expert panelists (both individually and as a panel)
are appropriately qualied to carry out the sensory evaluation. This work also shows the quality control maintenance of qualications
for the expert panellist. This approach could be generalized to any type of food and beverage as a reference for the accreditation of sensory quality evaluation methods according to ISO 17025. In this way, each product manufacturer would be able to dene its quality
standard and, on the basis of this standard, carry out the sensory evaluation using a panel specically trained for this purpose.
2006 Elsevier Ltd. All rights reserved.
Keywords: Sensory quality evaluation; ISO 17025 sensory method accreditation; Food quality certication; Protected designation of origin (PDO);
Idiazabal cheese
1. Introduction
The scientic strategy most acceptable for sensory quality evaluation takes into account the relation from two
types of data: tests with consumers (aective class, hedonic
type test) and trained analytical panels (descriptive class,
analytic type test). The relation between the two makes
it possible to determine sensory proles best adapted to
the concept of the product quality in the target market,
q
426
F.J. Perez Elortondo et al. / Food Quality and Preference 18 (2007) 425439
In laboratories that only use descriptive techniques, typically the number of positive descriptors is limited (key
attributes) and it is doubtful that it is even possible to
achieve a product more in line with a given sensory prole,
but where quality is insucient due to the presence of a
defect.
Finally there are some products, which, although they
should be market orientated to ensure successful sales, their
sensory attributes are inuenced by certain origins or processing factors. This is the case of PDO products that need
to gain the acceptance of consumers while at the same time
respecting their sensory typicalness. In many cases, these
producers are small enterprises, where it is economically
impossible for them to develop and introduce systematic
quality control on the end product from hedonic and analytical information.
Questions arise such as the followings: Apart from the
opinion of the consumer, should the inuence of technical,
cultural, social and environmental factors be taken into
account to obtain dierentiated products? Would it be
appropriate to propose a sensory analysis method validated and recognised (accredited), allowing a direct evaluation of the quality previously dened for a product, by
means of a panel of expert panelists trained specically
for the purpose? Using this method, should we take into
account the possible defects known in the product that
are important for its identity? How do we integrate said
possible defects in the quality evaluation?
Generally, in quality certication of PDO products,
regulations underline the fact that these products should
present sensory characteristics in accordance with the
judgement of a Sensory Committee. These panelists,
who may be labelled expert judges of a specic product,
Fig. 1. Main activities for the accreditation of a sensory quality evaluation method on a specic food product.
F.J. Perez Elortondo et al. / Food Quality and Preference 18 (2007) 425439
to the European Community regulations for PDO products, the certifying organizations of these food products
have to comply with the European Standard EN45011
(DOCE, 1992). Consulting the mentioned standard, it
becomes obvious that the analysis for certifying these products, sensory included, should be carried out in laboratories
according to the standard ISO 17025. One of the most
important documents nowadays for standardization of sensory activity is the European publication reference EA-4/09
Accreditation for sensory testing (ENAC, 2003) that
supplements ISO 17025 and provides specic guidance on
the accreditation of sensory laboratories. This document
gives detailed guidance for the interpretation of ISO
17025 for those undertaking sensory examinations. Accreditation bodies will only accredit laboratories for sensory
methods that have been fully documented and validated.
Some laboratories have accredited general discriminative,
descriptive and consumer sensory tests, but there is no previous experience in the accreditation of sensory quality
evaluation methods of specic products.
The aim of this study is to describe, for example, a sensory evaluation method that serves as a basis for the sensory quality certication of a specic product (PDO
Idiazabal cheese), as well as the training and qualication
process for expert panelists required for implementation.
The paper presents the experience of four years of work
and shows a general perspective across all the activities
(Fig. 1) developed in an accredited sensory laboratory
(June, 2005) according to ISO 17025:http://www.enac.es/
html/anx/le/UPV_EHU_LE1020_REV1.pdf.
2. Material and methods
2.1. Expert panelists for sensory quality evaluation
of a specic product
ISO standards on the selection and basic training of
panelists may be used as a reference during the initial training stages of experts, although such standards do not establish the required level needed to pass these preliminary
tests. Afterwards, expert judges should be trained specically on the sensory quality of the product under study
(characteristics and defects) and for the specic application
of the evaluation method.
2.2. Installations, equipment, chemical and foodstus
specic references
An accredited sensory analysis laboratory (SAL) should
have a meeting room according to the ISO standard, standardized booths and an isolated sample preparing area.
The other equipment in a SAL is not sophisticated, in order
to comply with the accreditation standards. This equipment is basically limited to thermo hygrometers and continuous read-out thermometers, refrigerators, tempered
sample chambers, weighing scales, distilling equipment
and/or water deionisation and volumetric material, chemi-
427
428
F.J. Perez Elortondo et al. / Food Quality and Preference 18 (2007) 425439
Table 1
Sensory standard denition of Idiazabal cheese used in quality evaluation
(adapted from Perez Elortondo, 1993)
Variable
Shape
Rind
Paste colour
Eyes
Odour
Texture
Flavour
Aftertaste
F.J. Perez Elortondo et al. / Food Quality and Preference 18 (2007) 425439
429
Table 2
Tests and criteria for selection of panelists
Table 3
Tests and criteria for basic training of panelists
F.J. Perez Elortondo et al. / Food Quality and Preference 18 (2007) 425439
430
tory management personnel decides, which of the candidates continue in future tests, based upon interest, availability and training results.
SAL considers these judges (food panelists) to be qualied to conduct simple standardized sensory analysis, basically discriminating tests, and to participate in the
development of descriptive sensory methods for specic
foods.
3.3. Specic training of panelists: PDO Idiazabal cheese
as example
So that a panelist can evaluate the sensory quality of
Idiazabal cheese, he must be given specic training and
Table 4
List of defects in appearancea
Shape
Rind
Paste colour
Holes
Blowing
Low
Convex
Sunken
Inclined
Colouring
Not developed
Cracks
Extraneous agents
Marks
Mouldy
Dirty
Caverns
Large
Cracks
Badly distributed
Numerous
Rounded
Table 5
Denition and references for characteristics of odour, avour and aftertaste
Characteristic
Odour
Sheeps milk
Sharp
Pungent
Acid
Sweet
Smoky (only smoked
cheeses)
Flavour
Sheeps milkd
Natural rennetd
Pungent
Sweet
Acid
Bitter (absence)
Salty
Smoky (smoked
cheeses)d
Aftertaste
Continuity
Persistent
Notable
a
Denition
Reference
Not applicable
To 2.35 g anhydrous sodium chloride add 50 mL H2O. Add 2.4 mL
BS to 100 g curd
Dissolve 5 lL commercial phenolic type liquid smoke aroma to
10 mL with H2Ob
Not applicable
Not applicable
Not applicable
F.J. Perez Elortondo et al. / Food Quality and Preference 18 (2007) 425439
431
Table 6
Denition and references of texture characteristics
Characteristic
Denition
References
Elasticity
Firmness
Granularity
Table 7
Group of defects and references for odour, avour and aftertaste
Defects
Denition
Reference
Vinegar
Rancid
Animal
Cowshed
Odour
Acid
Faecal
Putrid
Flavour/aftertaste
Acidic
Vinegar
Animal
Cowshed
Natural rennet
(in excess)c
Faecalc
Putridc
Bitter
Pungent
Abrasive
Pungent
5 g sheep dung
5 g putrid cheese. Add 3.5 mL BS to 100 g curd
5 g putrid cheese
F.J. Perez Elortondo et al. / Food Quality and Preference 18 (2007) 425439
432
representatives of each of the parameters. Once the panelists acquire sucient theoretical knowledge, they participate in two types of training sessions:
Denition
Reference
Elastic
Frankfurter
sausage
Soft
Hard
Floury
Sandy
Lumpy
Crystals
Coarse
Melting
Moist
Liquid
Doughy
Plastic
Brittle
Dry
Soluble
Melted cheese
Raw carrot
Potato puree
Breadcrumbs
Medium
grained
couscous
Sugar
Pippin apple
Melted cheese
Boiled white
of egg
Granny Smith
apple
Boiled egg yolk
Soft toee
Toast
Toast
Sugar
F.J. Perez Elortondo et al. / Food Quality and Preference 18 (2007) 425439
433
Table 9
Means, standard deviation, reproducibility, repeatability and discriminating capacity of one panelist
Shape
Rind
Paste colour
Eyes
Texture
Odour
Flavour
Aftertaste
ICh 2
ICh 1
ICh 2
ICh 1
ICh 2
ICh 1
ICh 2
ICh 1
ICh 2
ICh 1
ICh 2
ICh 1
ICh 2
Mean (N = 3)
S sample
3.25
0.50
3
0
3.75
0.50
2
0
4
0
3
0
3
0
1
0
4
0
4
0
4
0
4
0
4
0
3.50
0.58
4
0
3.25
0.50
Day 2
ICh 1
ICh 2
ICh 1
ICh 2
ICh 1
ICh 2
ICh 1
ICh 2
ICh 1
ICh 2
ICh 1
ICh 2
ICh 1
ICh 2
ICh 1
ICh 2
Mean (N = 3)
S sample
3
0
4
0
4
0
2
0
3
0
3
0
3
0
2
0
5
0
4
0
4.25
0.5
3
0
4
0
2.25
0.50
4
0
2
0
S
S
S
S
S
0.50
0
0.25
0.35
0.43
0
0
0
0
0
0.50
0
0.25
0.35
0.43
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0.50
0.25
0.35
0.43
0
0
0
0
0
0
0
0
0
0
0.58
0.50
0.54
0.05
0.54
0
0
0
0
0
0.50
0
0.25
0.35
0.43
session 1
session 2
repeatability
between session
reproducibility
% Reproducibility
% Repeatability
94
94
ICh 1
ICh 2
ICh 1
ICh 2
ICh 1
ICh 2
ICh 1
ICh 2
ICh 1
ICh 2
ICh 1
ICh 2
ICh 1
ICh 2
Mean
Ic
3.12
0.53
3.87
2.65
3.5
0.70
3
2.12
1.5
4.5
0.70
4.12
0.88
3.5
4
1.59
2.87
4
1.94
2.62
% Discriminating
67
3.5
ICh 2
ICh 1
ICh 2
ICh 1
ICh 2
ICh 1
ICh 2
ICh 1
ICh 2
ICh 1
ICh 2
ICh 1
ICh 2
Mean (N = 10)
S panelists
3.10
0.22
1.61
0.49
3.37
0.46
2.43
0.72
3.07
0.33
1.29
0.33
3.77
0.57
3.45
0.38
4.27
0.42
3.82
0.43
3.77
0.58
2.96
0.46
3.86
0.76
2.97
0.40
t calculated
t tabulated
1.09
2.23
3.36
0.73
3.56
0.72
7.06
2.10
3.47
2.10
11.97
2.10
OK
OK
OK
1.49
2.10
2.35
2.10
3.45
2.10
3.25
2.14
OK
OK
OK
ICh 1: Idiazabal cheese 1; ICh 2: Idiazabal cheese 2; N: Number of times that every kind of cheese is evaluated during each session; S: Standard deviation;
Ic: Compatibility race.
434
F.J. Perez Elortondo et al. / Food Quality and Preference 18 (2007) 425439
F.J. Perez Elortondo et al. / Food Quality and Preference 18 (2007) 425439
435
No
Yes
No
Yes
No
Yes
7
One absent-inappropriate?
No
3
Do you consider this/these defect/s to be medium?
Yes
No
Yes
6
Various absent-inappropriate?
No
2
Do you consider this/these defect/s to be serious?
Yes
Yes
Yes
4
Fig. 2. Tree diagram for evaluating sensory quality (evaluation criteria).
Mean (N = 14)
S panelists
t calculated
t tabulated
Idiazabal
cheese
4.14
0.86
2.95
2.064
3.36
0.50
OK
ICh 1: Idiazabal cheese 1; ICh 2: Idiazabal cheese 2; S: Standard deviation;
N: Number of times the sample has been evaluated.
0.20
0
0.10
0.43
0.44
3,43
2.86
0.10 3.71
0.10 2.86
0.10
0.42
0.43
3.71
3
0.10 3.86
0
3.14
0.05
0.37
0.38
3.57
2.86
0
3.43
0
2.86
0
0.33
0.33
3.57
3
0
3.57
0
3
0
0.25
0.25
2
2.43
0
2
0
2.43
0
0.08
0.08
2.86
2.71
0.40 2.86
0.20 2.71
0.30
0.27
0.41
4.57
4
Aftertaste
Flavour
ICh 1 ICh 2 Ss
ICh 1 ICh 2 Ss
Odour
Texture
ICh 1 ICh 2 Ss
ICh 1 ICh 2 Ss
Eyes
Paste colour
ICh 1: Idiazabal cheese 1; ICh 2: Idiazabal cheese 2; Ss: standard deviation of each session; Sbs: standard deviation between sessions.
Discriminating capacity
0
4
0.20 4.28
0.10
0.15
0.17
0.258
3.14
3.43
S session
0.142
0.082
0.082
0.103
0.237
3.14
3.14
ICh 3
Mean day 1
Mean day 2
S repeatability
Sbs
S reproducibility
ICh 2
3.43
3.57
4
4
4.14
4
S repeatability
S between
session
S
reproducibility
ICh 1 ICh 2 Ss
ICh 1
3.71
3.86
4
Rind
Session 1
Session 2
Session 3
ICh 1 ICh 2 Ss
Table 11
Quality control for quantication on scale of sensory parameters
Table 10
Example of results of validation (mean of the seven panelists as a whole)
for the parameter avour
ICh 1 ICh 2 Ss
ICh 1 ICh 2 Ss
F.J. Perez Elortondo et al. / Food Quality and Preference 18 (2007) 425439
Shape
436
F.J. Perez Elortondo et al. / Food Quality and Preference 18 (2007) 425439
437
tied in previous routine sessions. If the results of repetition show fewer than ve members of the panel to
identify the defect, then it will be openly discussed to
achieve consensus as to whether or not the specic defect
is found in the cheese. To back this up, by means of harmonization tasting, cases where panelists were not unanimous
(34 panelists noting down the defect) are investigated in
order to reduce the frequency of these situations as much
as possible.
3.8.2. Follow-up and monitoring the panelists
To ensure the individual qualication of the panelists
and the panel as a whole, it is essential to follow up and
monitor each one of the expert judges and the panel. To
do so, the SAL has standardized procedures:
Follow-up and routine monitoring of the panelists. An
individual report is drawn up comparing the results
given by each the judges in each session with the average
results from the panel as a whole. In those cases where
the standard deviation of the panel is P1, an analysis
of the data from panelists responsible of this dispersion
is conducted. Panelists who stand at a distance from the
rounded o average obtained by the panel as a whole by
one unit are noted as a deviation for these parameters.
This report is drawn up for each session, and is to be
shown to the judges so that they can see where there
were deviations. Where a panelist, in a given session,
Table 12
Individual report of a panelist after a session
Data
Judge
Cheese code
Shape
Rind
Paste colour
Eyes
Texture
Odour
Flavour
Aftertaste
256
Deviation?
Panel mean
5
Yes
3
4
Yes
2
789
Deviation?
Panel mean
123
Deviation?
Panel mean
951
Deviation?
Panel mean
632
Deviation?
Panel mean
6
Yes
4
701
Deviation?
Panel mean
No. cheeses:
No. parameters:
No. deviations:
% Deviations:
No. deviations:
% Deviations:
6
48
3
6.25
4
8.3
Panelist
Panel
Defects
Defects identied by the panel:
Defects not identied by the panelist:
Defects identied by the panelists:
% Identied:
82.14
28
5
23
OK
F.J. Perez Elortondo et al. / Food Quality and Preference 18 (2007) 425439
438
presents more than 15% deviations for all the parameters evaluated, one of the following measures is taken:
the panelist is interviewed to evaluate any possible
causes, re-training on the characteristics aected, temporary withdrawal and/or personal re-qualication. As an
example, Table 12 shows the individual (each panelist)
report appearance after a session where six cheeses were
analysed.
Follow-up and routine monitoring of the panel. If during a
given session the panel as a whole presents 15% deviations for all the attributes evaluated, then the following
measures are to be taken: re-training of the panel and/or
temporary withdrawal from participating.
Table 13
Cross-reference table showing ISO 17025 Standard items and the quality
manual (QM) and operative quality procedures (OQP)
ISO 17025:1999
standard section
QM
01
4. Management requirements
4.1. Organization
4.2. Quality system
management
4.3. Monitoring documents
OQP
4. Conclusions
02
03
04
F.J. Perez Elortondo et al. / Food Quality and Preference 18 (2007) 425439
439