ANEXA 1 DETERMINAREA CLORALCANILOR DIN PROBELE DE APA METODA CLOALC.

M PREGATIREA PROBEI Intr-o fiola de proba (de 25 ml) se introduc 25 ml proba (masurati cu o pipeta de 25 ml). Se introduce in proba Gerstel Twister( 10 mm cu 0.5 mm P !S) si se mentine sub a"itare #0 minute. APARATURA: -T S -Gas $%romato"rap% &'(0 ()"ilent) -$oloana * +P- 5!S, 0.25 mm -.0m -250/m -0.25/m -Split0Splitless Inlet ()"ilent) -$ooled In1ections S2stem ($IS,Gerstel) -!S 5(3.()"ilent) CONDITII DE ANALIZA: Inlet *mode4split 5ate split4 1001 6low 43 ml0min T S mode4standard Tinit.700$(0.10 min), &00$0min, 2#50$, (5 min) $IS4 T initiala7-#5 0$,(0.#0 min), 120$0sec, 2&0 0$ 89en4 .00$ (&min), #0$0min,300$, 100$0min, 1500$ (5 min) $olumn 6low 0.3 ml0min (+e) :elocit2 .0 cm0s !S mode4S$); .0-250 amu.