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1. Gravare acidă
2. Primer
3. Bonding
Generaţia 4
All-Bond 2, Scothbond MP
Adezivi în 2 paşi
1. Gravare acidă
2. Primer
Primer şi bonding într-un
singur recipient
3. Bonding
Generaţia 5
One-Step,Optibond, Prime & Bond, Singlebond
Adezivi în 2 paşi
1. Acid Primer
autogravant
2. Primer
3. Bonding
Generaţia 5
Liner Bond II (V), SE Bond
Adezivi de unică aplicare
1. Acid
H2O
Adezive autodemineralizante
2. Primer A + B (Mix) (L/C)
3. Bonding
Sisteme cu 2 componente
Prompt L-Pop, One-Up Bond F
Grabado
total
Studiu asupra forţei adezive
Sanares et al., Dent Mater 2001; 17:542-556
Adhesion Compatibility
15
pH
10with Self-Cured Composites
3.6
Self-Cured
5
2.8
0 2.6
PB2.1 OptS SB OS
Adezivii auto-demineralizanţi în relaţie cu
răşinile foto sau auto polimerizabile
Tay et al. J Dent 2002; 30:371-382
Adeziv auto- pH
60 demineralizant
Light-Cured Mode Chemical-Cured Mode
Touch & Bond (AQ) 2.6
50
i-Bond 2.4
Micro-TBS (MPa)
10
0
All-Bond
All-Bond 2 2 One-Up
One-Up Etch
Bond F Etch &
& Prime AQ
AQ Bond Prompt
Prompt L-Pop Futura-
Futura-Bond
Control Bond F Prime3.0 3.0 Bond L-Pop Bond
Incompatibilitatea chimică
cu compozitele
autopolimerizabile Strat inhibat O 2d
Aci
Se datorează acidităţii stratului
Acid
superficial al bondnig-ului care nu
polimerizează, fiind inhibat de Bonding
oxigenul atmosferic
Implicaţii clínice
Hydrophilic Hydrophobic
MDP during Poly’n after
BisGMA application polymerization
pH=3.2 (Less permeable)
Resin for Composite Log P Functional Monomers Log P
for Adhesive
Adhesive
Hydrophilic: Hydrophobic:
Uncured All-Bond U Cured All-Bond U
• Good wetting to tooth • more durable bond
• less permeable
• better seal, less chance of sensitivity
• more compatible with s/c or d/c
materials
Phase Separation of SE Adhesives
• All SE adhesives contain water & ethanol
• Water evaporates slower than ethanol*
Water bubble
Initial Azeotropic
Mixture of
Water/Ethanol
5-minute No Phase-separation
evaporation
Clinical Significance
Adhesives w/ no phase separation:
= easier to evaporate solvent & water
Cured composites w/
a.k.a
water-soluble blue dye Dream Bond
Immersed in water
for 4 hrs/37ºC Water
Blue-dye release
Self-Etch
Total-Etch
Bonds to Ceramics
For Direct / Indirect
• Apply Adhesive (LC)
B I S
CO
All-Bond Universal
Shear bond strength on dentin with different moisture level, MPa
“Desiccated” indicated that dentin was desiccated by using a strong stream of air for 10 seconds.
“Moist” as stated in the instructions for use
“Over-wet” indicated that dentin was very wet with a pool of water left on dentin.
28
Dentin SBS (MPa) with Direct L/C Composites
Self-Etch Mode
Shear Bond Strength, MPa
Composite (L/C) All-Bond Universal ScotchBond Universal
Aelite APB 36.9(6.7) n=9 34.7 (10.8) n=6
Z100 (3M) 34.1(6.7) n=8 44.9 (4.4) n=6
Filtek Supreme Ulta (3M)
(3M) 30.2 (4.7) n=6 35.6 (5.7) n=6
Empress Direct (Ivoclar) 31.2 (5.3) n=10 35.5 (6.9) n=8
Ultradent Jig Method
SonicFil (Kerr) 32.5 (5.6) n=8 34.5 (4.8) n=6
Core-Blue (u-TBS)
Micro-Tensile
53.7(16.4) n=15
Method
38.6 (13.1) n=11
B I S
CO
Universal Adhesive - ABU vs SBU
Bonding with D/C Resin Luting Cements for Indirect
Cement
Curing All-Bond ScotchBond
Substrate Mode Universal Universal /DCA
w/ Duolink with RelyX ARC
Dentin (SE) L/C
L/C, 31.0 (3.0) n=7 33.2(4.7), n=6
Dentin (SE) 4d/80C 22.7 (4.5) n=8 13.6(4.1), n=6
Dentin (SE) S/C 29.4(4.7) n=8 20.3 (6.2) n=6
Dentin (TE) L/C 33.2(7.8) n=8 30.1 (3.2), n=6
S/C Compatibility Incompatible!
Dentin (TE) S/C 33.7 (5.6) n=8 21.5 (5.6), n=6
B I S
CO
Universal Adhesive - ABU vs SBU
Bonding with D/C Resin Luting Cements for Indirect
Cement
Curing All-Bond ScotchBond
Substrate Mode Universal Universal /DCA
w/ Duolink with RelyX ARC
Cement
Curing All-Bond ScotchBond
Substrate
28.7 MPa Mode
(Z-Prime)Universal Universal /DCA
w/ Duolink with RelyX ARC
Zirconia L/C 26.9 (5.1) n=8 22.3(6.7) n=7
Alumina L/C 33.7 (8.2) n=8 25.2(7.8)n=6
Stainless Steel L/C 39.8 (6.8), n=8 33.3(5.6)n=6
RexIII L/C 37.8 (6.0) n=8 31.7(9.9)n=6
SureFire A L/C 17.8 (2.3) n=8 15.4(1.8)n=6
B I S
CO
Gold L/C 21.7 (4.6) n=8 25.8 (8.3), n=6
Bond to Zr? “Yes”
Water Contact angle on Sandblasted Zr (n=10)
pH = 3.2 pH = 2.8
Bisco 3M/ESPE
B I S
CO