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La coloanele cu talere, fazarichidase gaseste in miscare turbulenta, p"":fT.ltistemul in care vitezatransferuluile masa este determinata de rezistenta razel llchlde.

Eficacitatea: La coloanele cu umplutura, dar si la cele cu talere, valorile eficacitatii sunt in limite largi. Functionarea discontinua:
Coloanele cu umplutura cu diameter mari au masa foarte mare si prezinta probleme deosebite larcalizarea unei distributii uniforme a celor doua faze. La diameter mai mici de 400 mm coloanele cu talere sunt mai ieftine decat cele echivalente cu umplutura.

ll ll -

c) Caracteristicile fazelor participante

Sisteme corozive:
Este mai usor si mai ieftin sa se construiasca o coloana cu umplutura din material rezistent la coroziune, decat o coloana cu talere care presupune un cost

foarte ridicat.

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-

Sisteme care contin solid sau slamuri: Coloanele cu umplutura sunt sisteme care nu contin solide sau slamuri, iar coloanele cu talere sunt sisteme care contin solide sau slamuri in concentratie mare. Sisteme care spumeaza: La coloanele cu umplutura pentru sistemele care spume aza datorjtabarbotarii in lichid se formeaza pe talere o emulsie fina G L formata picaturi din de lichid si spuma' cate va determina o uniformizare a concentratiei in coloana si prin urrnare
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Sisteme termostabile: Coloanele cu umplutura sunt sisteme stabile din punct de vedere termic, iar coloanele cu talere sunt sisteme care nu prezinta stabilitate din punct de vedere

Sisteme vascoase: Coloanele cu umplutura sunt sisteme cu vascozitate mare, iar coloanele cu talere sunt sisteme cu vascozitate mica. Sisteme cu degajari de caldura: Daca efectul termic al procesului este mare la coloanele cu umplutura se monteaza dispositive pentru colectare si redistribuire. In cazul coloan.lor.u talere se monteaza serpentine de racire pe talere care favorizeaza absorbtia. Exista sisteme cu degajari mari de caldura la absorbtie, iar coloanele cu umplutura sunt sisteme cu degajari neinsemnate de caldura la absorbtie.

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Umpluturi pentru coloane:

Umpluturile utilizate pentru coloane se pot imparti in 3 categorii: - corpuri de umplere de forma neregulata; - corpuri de umplere de forma definita;

agatare.

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fi eficiente, umpluturile trebuie

sa indeplineasca urmatoarele

conditii:

sa prezinte o suprafata sa

catmai uniforma raportata la unitatea de volum; prezinte o rezistenta mica la curgerea fluidelor; sa realizeze o amestecare buna a celor 2 faze; sa fie ieftina; sa prezinte o rezistenta mecanica si chimica corespunzatoare.

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Corpurile de umplere de forma neregulata sunt in general foarte rar utilizate. Corpurile de umplere pot fi asezate in mod regulat in coloana sau pot fi turnate. La umpluturile asezate in vrac distributia lichidului depinde de forma si marimea corpurilor de umplere, diamtrul coloanelor, inaltimea straturilor si distributia initiala. Umpluturile mici duc la formarea unor purje de lichid datorita efectelor capilare ce apar la punctele de contact intre corpuri, ceea ce determina micsorarea suprafetei udate a umpluturii si prin urrnare scaderea eficacitatii coloanei. In scopul realizarii unei bune distributii a lichidului in coloana, in sectiunea transversal a straturilor de umplutura, se recomanda ca diametrul nominal al corpurilor de umplere sa fie de cel putin 8 ori mai mic decat diametrul coloanei. Evitarea formarii canalelor se face prin turnarea uniforma a umpluturii in strat, distributia uniforma a fazei lichide, impartirea umpluturii in mai multe straturi in care se interpun dispositive interioare pentru redistribuirea lichidului. Gratarele se construiesc din lemne, material ceramic, metalice, plastic, in forma simpla de bare paralele sau forme complexe, care permit dirijarea celor doua fluide. In timp ce gratarele simple se demonteazansot, se rcalizeaza o scadere de presiune si nu se infunda cand lichidul contine particule solide in suspensie. Gratarele complexe asigura o umezire aproape complete a umpluturii, preintampina aparitia unor curgeri partiale si a pungilor cu lichid.

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V

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