UNIVERSITATEA DE STIINTE AGRICOLE SI MEDICINA VETERINARA

LABORATOR CONTROLUL CALITATII PRODUSELOR APICOLE SI

DIAGNOZA APICOLA
STR. CALEA MNTUR 3-5, INSTITUTUL DE STIINTELE VIETII
400372 CLUJ-NAPOCA
Tel 0264/596384/386, Fax: 0264/593792
http://usamvcluj.ro/APHIS-DIA/index.html
e- mail: obobis@usamvcluj.ro
Laborator Autorizat Sanitar Veterinar
Nr. 111/26.06.2014

Pagina: 1/4
ANALIZA COMENZII NR....... din ....................
Solicitant :

Nume client/firm...
Persoana de contact..
AdresaTel/Fax:.
e-mail ..
Date privind proba:
Tip prob...
Prelevarea a fost efectuat de .....
Nr. probeAnul produciei...
Proba este sigilat

DA

NU

Proba reprezint eantion dintr-un lot de ............kg

Perioada de execuie a analizelor.........................................................................
Observaii:
Cerine speciale ale clientului.......

Pagina: 2/4

Cod
Parametrul
pro
determin
ceat
dura
Miere de albine

UM

Metoda de
determinare/
Referential

Tarif
(l
*
ei
)

Refractrometric/

PO-01

Apa

g/100g

International Honey
Commision Harmonised
Methods of International
Honey Commision (2009)

10

Conductometric/

PO-02

Conductivitate
electric

PO-03

Aciditate
liber, a
lactonelor si
total, pH
Hidroximetil-

PO-04 furfural (HMF)

mS/cm

International Honey
Commision Harmonised
Methods of International
Honey Commision (2009)

Poteniometric/

meq/kg

International Honey
Commision Harmonised
Methods of International
Honey Commision (2009)

mg/kg

International Honey
Commision Harmonised
Methods of International
Honey Commision (2009)

Schade/g

International Ireland Ltd.

Diastase activity in honey.
Assay Procedure K-AMZHY
04/05

PO-06

Analiza
palinologic

SR 784/3-2009 Miere de
albine. Metode de analiz

Zaharuri

PO-08

Tetracicline
(tetraciclina,
oxitetraciclina)

PO-09

PO-10

PO-20

Examen microscopic/

40

55

Cromatografie de lichide
(HPLC-RI)/

g/100g

ppb

Sulfamide
(sulfanilamida,
sulfadiazina,
sulfatiazol,
sulfamerazina,
sulfametazina)

50

Spectrofotometric
(Amilazyme)/Megazyme

Indicele
diastazic

PO-07

40

Cromatografie de lichide
(HPLC-PDA)/

PO-05

(Fructoz,
glucoz,
zaharoz,
maltoz,
turanoz)

15

ppb

Cloramfenicol

ppb

Cenusa

International Honey
Commision - Harmonised
Methods of International
Honey Commision (2009)

Cromatografie de lichide
(HPLC-PDA)/ metod
adaptat dup AOAC Official
Methods of Analysis 1995,
(33.2.62)

Cromatografie de lichide
(HPLC-FLD)/ metod
dezvoltat n laborator dupa
Poszniak A. i colab., 2007,
Bull.Vet.Inst.Pulawy,52:87-91

Cromatografie de lichide
(LC-MS)/ metod dezvoltat
n laborator dupa Shen si
Jiang, 2005, Analitica
Chimica Acta, 535:33-41

Gravimetric, calcinare/
SR 784/3-2009

100

100

100

100

30

Nr.
pr Valoare
ob
(lei)
e

Cod
pro
cedura
Polen
PO-11

Parametrul
determin
at
Apa/
Substan
uscat

UM

PO-12 Proteine totale

PO-13

Lipide totale

Zaharuri

PO-07
PO-20

(Fructoz,
glucoz,
zaharoz,
maltoz,
turanoz)

Metoda de
determinare/
Referential
Gravimetric, uscare la
etuva/S.T.R.-55; N.I.55/88
ACA Romania, Combinatul
Apicol
Kjeldahl/metoda dezvoltata
in laborator dupa Campos
M.G.R. i colab., 2008,
Journal of Apicultural
Research and Bee World
47(2):156-163
Extractie Soxhlet/ metoda
dezvoltata in laborator dupa
L.B. Almeida-Muradian i
colab., 2005, Journal of Food
Composition and Analysis 18:
105-111

Tarif
(l
*
ei
)

15

50

40

Cromatografie de lichide
(HPLC-RI)/ metod adaptat

g/100g

Cenusa

Reziduu la
extractie

dup International Honey

Commision - Harmonised
Methods of International
Honey Commision (2009)

Gravimetric, calcinare/
metod adaptat dup
784/3-2009

SR

100

30

Propolis
PO-14
PO-15
PO-13

Polifenoli si
flavonoide din
tinctura de
propolis
Ceara
(substante
extractibile)

Gravimetric/ S.T.R.-55;
N.I.55/88 ACA Romania,
Combinatul Apicol

15

Spectrofotometric/

metod dezvoltat n
laborator dupa Singleton si
col., Methods in Enzymology,
1999, 299, 152-178

Extractie Soxhlet/ S.T.R.55; N.I.55/88 ACA Romania,

Combinatul Apicol

50x2

40

Ceara
PO-16
PO-17

PO-18

Indicele de
aciditate si
saponificare
Punctul de
topire
Reziduuri de
acaricide
(amitraz, 2,4dimetilanilin,
brompropilat,
cumafos,
fluvalinat)

mg
KOH/g
o

ppb

Titrimetric/
STAS 3064/3-74 Cear de
albine. Metode de analiz

STAS 3064/3-74 Cear de

albine. Metode de analiz
Cromatografie de gaze
(GC-MS)/ metod
dezvoltat n laborator dupa
Lodesani si col.,2008,
Apidologie, 39:324-333

60
10

100

Pagina: 3/4
Nr.
pr Valoare
ob
(lei)
e

Cod
Parametrul
pro
determin
ceat
dura
Lptior de matc
PO-11

Apa/
Substan
uscat

UM

PO-12 Proteine totale

PO-13

Lipide totale
Zaharuri

PO-07

PO-19
PO-20

(Fructoz,
glucoz,
zaharoz,
maltoz,
turanoz)

Tarif *
(l
ei
)

Metoda de
determinare/
Referential
Gravimetric, uscare la
etuva/ Caiet de sarcini

Pagina: 4/4
Nr.
pr Valoare
ob
(lei)
e

15

46/1977 Asociatia
Crescatorilor de Albine din
Romania
Kjeldahl/metoda dezvoltata
in laborator dupa Campos
M.G.R. i colab., 2008,
Journal of Apicultural
Research and Bee World
47(2):156-163
Extractie Soxhlet/ metoda
dezvoltata in laborator dupa
L.B. Almeida-Muradian i
colab., 2005, Journal of Food
Composition and Analysis 18:
105-111

50

40

Cromatografie de lichide
(HPLC-RI)/ metod adaptat
dup International Honey
Commision - Harmonised
Methods of International
Honey Commision (2009)

g/100g

100

Cromatografie de lichide
(HPLC-PDA)/ metod

Acidul
10-hidroxi
decenoic
(10-HAD)

dezvoltat n laborator dup

Liu i col., J. Agric Food
Chem., 2008, 56(23):1144752

Cenusa

metod adaptat dup

784/3-2009

100

Gravimetric, calcinare/

30

SR

Valoare totala (lei).................

* - se bifeaz prin X analiza solicitat
Acordul clientului privind:
Metodele si procedurile de analiza utilizate

DA

NU

Tarifele aplicate ncercrilor solicitate

DA

NU

Perioada de execuie a ncercrilor solicitate (durata

estimat n zile lucrtoare)

DA

NU

Data:

Semntura client

FS-APHIS-02-01 Editia 2/19.05.2014 Revizia 1/21.12.2015